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Integrated high-performance and accurate shaping technology of low-cost powder metallurgy titanium alloys: A comprehensive review

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International Journal of Minerals,Metallurgy and Materials 2024年第3期31卷 413-426页

作者： Xuemeng Gan shaofu li Shunyuan Xiao Yafeng Yang State Key Laboratory of Mesoscience and Engineering Institute of Process EngineeringChinese Academy of SciencesBeijing 100190China University of Chinese Academy of Sciences Beijing 100049China Key Laboratory of Science and Technology on Particle Materials Chinese Academy of SciencesBeijing 100190China

The practical engineering applications of powder metallurgy (PM) Ti alloys produced through cold compaction and pressure-less sintering are impeded by poor sintering densification, embrittlement caused by excessive O impurities, and severe sintering deforma-tion resulting from the use of heterogeneous powder mixtures. This review presents a summary of our previous work on addressing the above challenges. Initially, we proposed a novel strategy using reaction-induced liquid phases to enhance sintering densification. Near- complete density (relative density exceeding 99%) was achieved by applying the above strategy and newly developed sintering aids. By focusing on the O-induced embrittlement issue, we determined the onset dissolution temperature of oxide films in the Ti matrix. On the basis of this finding, we established a design criterion for effective O scavengers that require reaction with oxide films before their dissol-ution. Consequently, a ductile PM Ti alloy was successfully obtained by introducing 0.3wt% NdB6 as the O scavenger. Lastly, a powder- coating strategy was adopted to address the sintering deformation issue. The ultrafine size and shell-like distribution characteristics of coating particles ensured rapid dissolution and homogeneity in the Ti matrix, thereby facilitating linear shrinkage during sintering. As a result, geometrically complex Ti alloy parts with high dimensional accuracy were fabricated by using the coated powder. Our fundament-al findings and related technical achievements enabled the development of an integrated production technology for the high-performance and accurate shaping of low-cost PM Ti alloys. Additionally, the primary engineering applications and progress in the industrialization practice of our developed technology are introduced in this review.

关键词： powder metallurgy titanium sintering densification oxygen scavenging accurate shaping

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基于反向传播神经网络PID的高功率微波炉温度控制

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强激光与粒子束 2024年第1期36卷 55-61页

作者：王威李少甫吴昊蒋成唐颖颖西南科技大学信息工程学院四川绵阳621010

针对现有10 kW高功率工业微波炉,采用继电器作为控制执行器,在使用传统控制方法加热时,温度存在较大超调和明显振荡,系统温度稳定性较低,为解决上述问题将反向传播神经网络PID(BPNNPID)控制引入到该装置微波加热温度控制中,并以自来水... 详细信息

针对现有10 kW高功率工业微波炉,采用继电器作为控制执行器,在使用传统控制方法加热时,温度存在较大超调和明显振荡,系统温度稳定性较低,为解决上述问题将反向传播神经网络PID(BPNNPID)控制引入到该装置微波加热温度控制中,并以自来水为加热对象进行仿真对比与实验验证。首先,利用现有输入输出实验数据,建立工业微波炉温度控制模型;其次,运用MATLAB/SIMUliNK搭建高功率工业微波炉温度控制系统并进行仿真对比实验;最后,实验验证BPNNPID控制方法在加热5 kg自来水时工业微波炉的温度控制性能,实验结果表明,较常规PID、模糊PID控制,该方法在微波加热过程中对媒质温度控制超调更小且未发生明显温度振荡,有效改善了高功率工业微波炉工作时的系统温度稳定性,有助于提高产品质量和安全性能。

关键词：高功率微波加热反向传播神经网络 PID 温度控制

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Highly ductile hypereutectic Al-Si alloys fabricated by selective laser melting

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Journal of Materials Science & Technology 2022年第15期110卷 84-95页

作者： Yafeng Yang Kang Geng shaofu li Michael Bermingham R.D.K.Misra State Key Laboratory of Multiphase Complex Systems Institute of Process EngineeringChinese Academy of SciencesBeijing 100190China University of Chinese Academy of Sciences Beijing 100049China School of Mechanical and Mining Engineering University of QueenslandSaint LuciaQueensland 4072Australia Department of Metallurgical Materials and Biomedical EngineeringUniversity of Texas at El Paso500 W University AvenueEl PasoTX 79968USA

In the endeavor to maximize the refinement effect of primary Si and alleviate the inherent brittleness of hypereutectic Al-Si alloy,the approach of coating P as a modifier on powder was *** ultimate aim was to create more heterogeneous fine Al P nucleus and enhance the nucleation efficiency of primary Si on Al P to refine the coarse primary Si to nano-scale during 3D *** the combination of large undercooling and high density of nucleation sites,the size of primary Si was successfully refined to 200–300 nm and the divorced eutectic was also induced to modify the microstructure of *** the presence of nano-scale primary Si,the melting pool boundary(MPB)feature disappeared and the fracture mechanism also changed from load transfer to interfacial *** with the pristine alloy,the ductility was increased four times without significantly changing the ultimate tensile strength(UTS)and wear *** improvement of ductility is attributed to the refinement of primary Si,the disappearance of MPB features and the formation of divorced *** optimal tensile properties were:UTS-482 MPa,yield strength-320 MPa and ductility of 8.1%at 0.05 wt.%*** are comparable to those for high-strength Al alloys.

关键词： Al-Si alloys Heterogeneous nucleation Ductility Powder processing Selective laser melting

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高功率微波加热三维温度模型仿真与验证

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强激光与粒子束 2024年第1期36卷 84-93页

作者：吴昊李少甫王威蒋成唐颖颖西南科技大学信息工程学院四川绵阳621010

微波加热不均匀性一直以来都是从事微波加热控制方向研究人员心目中的热点问题。根据微波加热装置的物理结构建立了炉内各层表面的温度静态差分模型结合实验以求得微波加热的实际功率。再基于传热学的有限差分法建立三维空间中的温度分... 详细信息

微波加热不均匀性一直以来都是从事微波加热控制方向研究人员心目中的热点问题。根据微波加热装置的物理结构建立了炉内各层表面的温度静态差分模型结合实验以求得微波加热的实际功率。再基于传热学的有限差分法建立三维空间中的温度分布模型,利用MATLAB以及COMSOL仿真对比验证了模型的有效性。假定微波均匀加热求得被加热介质的平衡温度与不均匀加热时的温度进行比对以找出微波加热过程中介质的部分温升平衡点,最后互相比对找出最优点为控制对象进行专家PID(proportion-integral-derivative)微波加热。实验结果表明,该方法能较为精确地测量出被加热介质任何时刻的平衡温度,使得微波加热在工业生产上有着更加广泛的应用。

关键词：微波加热静态差分有限差分 COMSOL仿真温升平衡点

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Integrating dual-role variables in data envelopment analysis

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Journal of Systems Engineering and Electronics 2010年第5期21卷 771-776页

作者： Feng Yang liang liang Zhaoqiong li shaofu Du School of Management University of Science and Technology of China Hefei 230026 P. R. China

Traditional data envelopment analysis（DEA） theory assumes that decision variables are regarded as inputs or outputs,and no variable can play the roles of both an input and an output at the same *** fact,there exist some variables that work as inputs and outputs simultaneously and are called dual-role *** DEA models cannot be used to appraise the performance of decision making units containing dual-role *** paper analyzes the structure and properties of the production systems comprising dual-role variables,and proposes a DEA model integrating dual-role *** the proposed model is illustrated to evaluate the efficiency of university departments.

关键词： data envelopment analysis efficiency evaluation dual-role variable.

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Polymeric hollow fiber membrane for cooling crystallization seeding:On the mechanism of induced nucleation based on thermal transfer Author links open overlay panel

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Particuology 2024年第8期91卷 38-49页

作者： Zeman He shaofu Du Guanying Shao Peiyu li Lei Sheng Gaohong He Xiaobin Jiang Wu Xiao State Key Laboratory of Fine Chemicals School of Chemical EngineeringEngineering Laboratory for Petrochemical Energy-efficient Separation Technology of Liaoning ProvinceDalian University of TechnologyDalian 116024China

Cooling crystallization is an important separation process and particuology technology that requires accurate nucleation control ***,we introduced the polymeric hollow fiber membrane with proper thermal properties as the effective nucleation induction interface during cooling *** heterogeneous nucleation control mechanism was introduced based on classical nucleation theory and the thermal transfer *** properties and the thermal conductivity of two kinds of polymeric membranes,polytetrafluoroethylene(PTFE)and polyethersulfone(PES),were measured and simulated with the developed *** two membranes possessed different nucleation induction periods,nucleation rates and crystallization performances,which validated that the hollow fiber membrane module could effectively accelerate the nucleation process compared to conventional cooling crystallization owing to the shorter nucleation induction period and the reduced solution surface *** to the higher hydrophobicity and the lower roughness of the membrane surface,the PTFE membrane possessed a more moderate performance in generating stable heterogeneous nucleation than the one of PES ***,the adjustable membrane property enabled the hollow fiber membrane-assisted cooling crystallization to possess the accurate nucleation control and desired terminal particle products.

关键词： Cooling crystallization Nucleation Particle process Hollow fiber membrane Induction period Process control

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Preparation of nano-sized tungsten carbide via fluidized bed

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Chinese Journal of Chemical Engineering 2020年第3期28卷 923-932页

作者： Feng Pan Zhan Du shaofu li Jun li Meiju Zhang Maoqiao Xiang Qingshan Zhu State Key Laboratory of Multiphase Complex Systems Institute of Process EngineeringChinese Academy of Sciences(CAS)Beijing 100190China Information Research Institute of Emergency Management Department Beijing 100084China University of Chinese Academy of Sciences Beijing 100049.China

Ultrafine or nano-sized of tungsten carbide(WC)is the key material to prepare ultrafine grained cemented *** this paper,nano-sized WC powders were directly prepared by using industrial nano-needle violet tungsten oxide(WO2.72)as the raw material,a fluidized bed as the reactor,and CO as the carbonization *** relationship between particle sizes and reaction temperatures,residence times,atmospheres has been investigated *** addition,the physical–chemical indexes(such as residual oxygen,total carbon and free carbon)of the products were *** results indicated that the particle size of WC increased with the increase of temperature from 800 to 950°*** the residence time increased,the particle size decreased gradually,and then increased due to slight *** introduction of hydrogen reduced the carbonization rate,and is not beneficial to obtaining nano-sized *** that satisfy the standard were obtained when WO2.72 reacted with CO at 850°C,900°C and 950°C for 3.0 h,2.5 h and 2.0 h,*** particle sizes of the three samples calculated from the specific surface area were 46.4 nm,53.2 nm and 52.1 nm,respectively.

关键词： Nanoparticles Violet tungsten oxide Nano tungsten carbide Fluidized-bed Reduction-carbonization Process control

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Efficient fluidization intensification process to fabricate in-situ dispersed(SiO+G)/CNTs composites for high-performance lithium-ion battery anode applications

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Particuology 2021年第3期19卷 84-90页

作者： Hebang Shi He Zhang Chaoquan Hu shaofu li Maoqiao Xiang Pengpeng Lv Qingshan Zhu State key Laboratory of Multiphase Complex Systems Institute of Process EngineeringChinese Academy of SciencesBeijing 100190China University of Chinese Academy of Science Beijing 100049China College of Materials and Metallurgy Guizhou UniversityGuiyang 550025China Nanjing IPE Institute of Green Manufacturing Industry Nanjing 211135China

An efficient fluidization process intensification method was proposed to prepare carbon nanotube(CNT)-enhanced high-performance SiO anodes for lithium-ion *** introduction of graphite particles decreased bonding among SiO particles,inhibiting agglomerate growth and enhancing ***(SiO+G)/CNTs composites were synthesized by fluidized bed chemical vapor deposition with the CNTs grown in-situ,which ensured uniform dispersion and superior anchoring of the *** in-situ-grown CNTs and stacked graphite ensured excellent structural stability and *** synthesized(SiO+G)/CNTs delivered a stable reversible capacity of 466 mAh g^(−1) after 125 cycles and a capacity of∼200 mAh g^(−1) at 2 A g^(−1).The charging results indicated that the 3D network structure comprising CNTs and graphite not only effectively buffered the electrode expansion but also greatly improved mechanical flexibility.

关键词： Process intensification Fluidized bed chemical vapor deposition Carbon nanotubes Silicon suboxide anode

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高截止频率肖特基二极管仿真模型研究

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电波科学学报 2023年第6期38卷 1040-1047页

作者：余蒋平李少甫唐颖颖西南科技大学信息工程学院绵阳621010

基于表面沟道型平面肖特基势垒二极管基本结构,采用GaAs 0.15μm伪高电子迁移率晶体管(pseudomorphic high electron mobility transistors,pHEMT)工艺制程,提出了一种垂直沟道长跨度空气桥的肖特基二极管模型.研究了不同阳极直径对肖... 详细信息

基于表面沟道型平面肖特基势垒二极管基本结构,采用GaAs 0.15μm伪高电子迁移率晶体管(pseudomorphic high electron mobility transistors,pHEMT)工艺制程,提出了一种垂直沟道长跨度空气桥的肖特基二极管模型.研究了不同阳极直径对肖特基二极管级联电阻的影响,对比分析了不同焊盘间距下肖特基二极管模型的S参数仿真结果,得到最优空气桥长度;仿真了最优焊盘间距下二极管肖特基结的TCAD模型,根据仿真得到的特性曲线提取肖特基二极管的SPICE参数.经实验测试,该二极管具有极低的零偏置结电容,截止频率高达9 THz,仿真结果与实测结果吻合度较高,可用于太赫兹频段上.

关键词：太赫兹肖特基二极管 GaAs 垂直沟道截止频率

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Leaching kinetics of fluorine during the aluminum removal from spent li-ion battery cathode materials

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Journal of Environmental Sciences 2024年第4期138卷 312-325页

作者： Shengjie li Jianxin Zhu Research Center for Eco-Environmental Sciences Chinese Academy of SciencesBeijing 100085China University of Chinese Academy of Sciences Beijing 100049China

The high content of aluminum(Al)impurity in the recycled cathode powder seriously affects the extraction efficiency of Nickel,Cobalt,Manganese,and lithium resources and the actual commercial value of recycled materials,so Al removal is crucially important to conform to the industrial standard of spent li-ion battery cathode *** this work,we systematically investigated the leaching process and optimum conditions associated with Al removal from the cathode powder materials collected in a wet cathode-powder peeling and recycling production line of spent li-ion batteries(liBs).Moreover,we specifically studied the leaching of fluorine(F)synergistically happened along with the removal process of Al,which was not concerned about in other studies,but one of the key factors affecting pollution prevention in the recovery *** mechanism of the whole process including the leaching of Al and F from the cathode powder was indicated by using NMR,FTIR,and XPS,and a defluoridation process was preliminarily investigated in this *** leaching kinetics of Al could be successfully described by the shrinking core model,controlled by the diffusion process and the activation energy was 11.14 kJ/***,the leaching of F was attributed to the dissolution of liPF6and decomposition of PVDF,and the kinetics associated was described by Avrami *** interaction of Al and F is advantageous to realize the defluoridation to some *** is expected that our investigation will provide theoretical support for the large-scale recycling of spent liBs.

关键词： Al removal F leaching Cathode powder Heating alkali leaching Leaching kinetics

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