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Laser powder bed fusion of NiTiFe sha.e memory alloy via premixed powder:microstructural evolution,mechanical and functional properties

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Rare Metals 2024年第5期43卷 2300-2316页

作者： Bo Yuan Jin-Guo Ge Liang Zhang Hong-Jun Chen Long-sha.Wei Yu-Duo Zhou Run-Hua Song Institute of Intelligent Manufacturing Technology Shenzhen PolytechnicShenzhen 518055China School of Mechanical and Electrical Engineering Guilin University of Electronic TechnologyGuilin 541004China Guangdong Advanced Polymer Composite Engineering Technology Research Center Shenzhen Academy of Aerospace TechnologyShenzhen 518057China Jihua Laboratory Testing Center Jihua LaboratoryFoshan 528000China

High-cost pre-alloyed powder is the bottleneck problem that limits the widespread application of additivemanufactured sha.e memory *** this work,the lowcost ternary NiTiFe sha.e memory alloy is fabricated by laser powder bed fusion(LPBF)technique via mechanically mixed pre-alloy NiTi powder and varying contents pure Fe powder(1,2,3 wt%).All NiTiFe alloys show a relative density of up to 99.8%by optimizing the LPBF processing *** to the heterogeneous nucleation effect of micron-sized Fe particles,both grain refinement and texture weakening are generated in the NiTiFe alloys,accompanied by the reduction of dislocation *** the room-temperature mechanical properties,the NiTi-3Fe alloy shows the highest microhardness of HV370,but the fracture strength and elongation reduce to1701 MPa and 23%*** evolution of mechanical properties is attributed to the high internal defects,low dislocation density and the incoherent ***,the NiTi-3Fe alloy shows the quasi-linear superelasticity behavior;the superelastic recoverable strain of NiTi-1Fe and NiTi-2Fe decreased with the increase in Fe *** study provided a new-fangled insight for the development of multi-component NiTi-based sha.e memory alloys by additive manufacturing.

关键词： Additive manufacturing sha.e memory alloy Metal matrix composite Microstructure Mechanical properties

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PbGIF1 promoting cell-proliferation in pear fruit is transcriptionally activated by Pb RR1

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Horticultural Plant Journal 2024年第3期10卷 689-697页

作者： Huibin Wang Guangya sha.Rui Gao Jianwen Pang Rui Zhai Chengquan Yang Zhigang Wang Lingfei Xu College of Horticulture Northwest A&F UniversityYanglingShaanxi 712100China College of Life Science Hebei Agricultural UniversityBaodingHebei 071000China

As a cell proliferation regulator involved in wide biological processes in plants,GRF-INTERACTING faCTOR(GIF)controls different tissues ***,whether GIF participates in fruit development remains *** to transcriptome data,we identified PbGIF1was highly expressed during fruit development in cytokinins induced parthenocarpy *** the present study,the biofunction of PbGIF1 was initially *** of PbGIF1 promoted fruit size of transgenic *** size of flesh fruit was not affected by cell expansion but the cell proliferation was promoted by overexpressing Pb *** accelerated cell proliferation process was also observed in PbGIF1-overexpressed transgenic pear fruit *** transcriptional regulation of cytokinins on PbGIF1 was further confirmed by exogenous CPPU treatments in pear *** investigate the underlying mechanism,the cytokinins-responded factor,PbRR1,was further focused *** results of Yeast-one-hybrid assay suggested that PbRR1 can bind to the promoter sequence of *** transcriptional activation of PbRR1 on PbGIF1 was also confirmed by Dual-Luciferase *** together,the results showed that cytokinins control pear fruit development via the transcriptional activation of PbGIF1 by PbRR1.

关键词： PbGIF1 Cell proliferation Pear Fruit development Cytokinins PbRR1

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Flexible mille-feuille structure electromagnetic interference shielding film with excellent thermal conductivity and Joule heating

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Nano Research 2024年第5期17卷 4544-4554页

作者： Dingwen Yin Huijuan Xiu Simin Wang Yanfei Pan Na Li Rui Cheng sha.yan Huang sha.fan Jinbao Li College of Bioresources Chemical&Materials Engineering Shaanxi University of Science&TechnologyXi'an 710021China National Demonstration Center for Experimental Light Chemistry Engineering Education Shaanxi Provincial Key Laboratory of Papermaking Technology and Specialty Paper DevelopmentXi'an 710021China College of Material Science and Art Design Inner Mongolia Agricultural UniversityHohhot 010018China

The intelligent electronic devices have urgent demands for electromagnetic interference(EMI)shielding films with excellent heat dissipation ***,it is challenging to obtain excellent EMI shielding and thermal conductivity performances ***,inspired by mille-feuille structure,the multifunctional EMI shielding films developed by a layer-by-layer self-assembly and hot-pressing *** ingenious introduction of silver nanoparticles(AgNPs)with large specific surface area and highly conductive into the network formed by TEMPO-oxidized cellulose nanofibrils(TOCNFs)with large aspect ratio to form the TOCNFs/*** the graphene nanoplates(GNPs)with high conductivity loss distributed alternately with TOCNFs/AgNPs to construct mille-feuille structure,which had highly efficient conductive network,complete thermally conduction pathway and rich heterogeneous ***,the designed films presented high electrical conductivity of 8520 S/cm,superb EMI effectiveness(SE)of 98.05 dB,and excellent thermal conductivity of 18.82 W/(m·K).Furthermore,the films possessed outstanding Joule heating performances with low voltages,including high heating temperature(100℃),fast response time(fascinating thermal conductivity and Joule heating performances have substantial application in flexible electronics,electromagnetic waves shielding and thermal management.

关键词： TEMPO-oxidized cellulose nanofibrils/silver nanoparticles(TOCNFs/AgNPs) mille-feuille structure electromagnetic interference shielding thermal conductivity Joule heating

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Synergistic Brønsted Base/Photoredox-Catalyzed Three-Component Coupling with Malonates to Synthesize δ-Hydroxy Esters and δ-Keto Esters

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Chinese Journal of Chemistry 2024年第9期42卷 957-962页

作者： Ting Li Wei Wang Ming Dong Zhije Zhang sha.Yu Zhengchu Chen Siping Wei Dong Yi Green Pharmaceutical Technology Key Laboratory of Luzhou City Central Nervous System Drug Key Laboratory of Sichuan ProvinceSchoolof PharmacySouthwestMedicalUniversityLuzhouSichuan 646000China Nuclear Medicine and Molecular Imaging Key Laboratory of Sichuan Province LuzhouSichuan 646000China

Multicomponent alkene 1,2-dicarbofunctionalizations(DCFs)have emerged as a powerful strategy to rapidly incorporate both two carbon subunits across one C-C double bond in one step for enhancing molecular complexity and *** the best of our knowledge,there is only one report on photoredox-catalyzed three-component DCFs with malonates through the radical−radical cross-coupling,while photoredox-catalyzed radical-polar crossover(RPC)-type DCFs with malonates were still ***,we describe a redox-neutral RPC-type 1,2-dialkylation of styrenes with malonates and aldehydes through the synergistic Brønsted base/photoredox catalysis *** transition-metal-free strategy provides an efficient and clean approach to a broad variety ofδ-hydroxy esters and also features exceptionally mild conditions,wide compatibility of substrate scope and functional groups,and high atomic ***,three-component 1,2-alkylacylation from the same starting materials was achieved in one-pot manner through such RPC-type coupling and subsequent two-electron oxidation process,providing a set ofδ-keto esters of interest in pharmaceutical research.

关键词： Alkene difunctionalization Photoredox catalysis Malonates Radical reactions C-C coupling Synthetic methods Aldehydes Alkylation Multicomponentreactions

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Synergetic pathways of water-energy-carbon in ecologically vulnerable regions aiming for carbon neutrality:a case study of sha.nxi,China

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Frontiers of Environmental Science & Engineering 2024年第9期18卷 1-15页

作者： Yingying Liu Hanbing Li sha.Chen Lantian Zhang Sumei Li He Lv Ji Gao Shufen Cui Kejun Jiang Department of Environmental Science Key Laboratory of Beijing on Regional Air Pollution ControlBeijing University of TechnologyBeijing 100124China China Metallurgical Industry Planning and Research Institute Beijing 100711China Environmental Defense Fund Beijing 100007China Department of Financial Management Lishui UniversityLishui 323000China Energy Research Institute Beijing 100038China

Synergetic energy-water-carbon pathways are key issues to be tackled under carbon-neutral target and high-quality development worldwide,especially in ecologically vulnerable regions(EVRs).In this study,to explore the synergistic pathways in an EVR,a water-energy-carbon assessment(WECA)model was built,and the synergistic effects of water-energy-carbon were comprehensively and quantitatively analyzed under various scenarios of regional *** Province was chosen as the representative EVR,and Lower challenge(LEC)and Greater challenge(GER)scenarios of zerocarbon transition were set considering the technological maturity and regional energy *** results showed that there were limited effects under the zero-carbon transition of the entire region on reducing water withdrawals and improving the water *** the LEC scenario,the energy demand and CO2 emissions of sha.nxi in 2060 will decrease by 70.9%and 99.4%,respectively,whereas the water withdrawal and freshwater aquatic ecotoxicity potential(faETP)will only decrease by 8.9%and 1.6%,*** could be attributed to the stronger demand for electricity in the energy demand sector caused by industrial transition *** GER scenario showed significant growth in water withdrawals(16.0%)and faETP(36.0%)because of additional biomass *** promote the synergetic development of regional transition,EVRs should urgently promote zero-carbon technologies(especially solar and wind power technologies)between 2020 and 2060 and dry cooling technology for power generation before *** particular,a cautious attitude toward the biomass energy with carbon capture and storage technology in EVRs is strongly recommended.

关键词： Carbon neutrality Water withdrawals Water environment quality Ecologically vulnerable region Typical regional transition

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Gastrointestinal problems in a valproic acid-induced rat model of autism: From maternal intestinal health to offspring intestinal function

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World Journal of Psychiatry 2024年第7期14卷 1095-1105页

作者： sha.Li Nan Zhang Wang Li Han-Lai Zhang Xiao-Xi Wang Institute of Acupuncture and Moxibustion China Academy of Chinese Medical SciencesBeijing 100000China Institute of Basic Theory for Chinese Medicine China Academy of Chinese Medical SciencesBeijing 100000China

BACKGROUND Autism spectrum disorder(ASD)is a developmental disorder characterized by social deficits and repetitive ***(GI)problems,such as constipation,diarrhea,and inflammatory bowel disease,commonly occur in patients with ***,GI problems of ASD patients were attributed to intestinal inflammation and vertical mother-to-infant microbiome *** To explore whether GI problems in ASD are related to maternal intestinal inflam-mation and gut microbiota *** An ASD rat model was developed using valproic acid(VPA).Enzyme-linked immunosorbent assay and fecal 16S rRNA sequencing were used to test GI *** VPA exposure during pregnancy led to pathological maternal intestinal changes,resulting in alterations in maternal gut ***,the levels of inflammatory factors also ***,prenatal exposure to VPA resulted in impaired duodenal motility in the offspring as well as increased levels of infla-mmatory *** GI problems in ASD may be associated with maternal intestinal inflammation and microbiota *** research is required to find more evidence on the etiology and treatment of GI problems in ASD.

关键词： Autism spectrum disorder Gastrointestinal problems Gut microbiota Intestinal inflammation Intestinal motility

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Carbene-catalyzed enantioselective seleno-Michael addition as access to antimicrobial active Se-containing heterocycles

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Science China Chemistry 2024年第7期67卷 2199-2205页

作者： Hongyan Long sha.Zhao Chunyan Jian Xiuli Wu Fengfei Lu Minghong Liao Fengrui Che Xingxing Wu Yonggui Robin Chi State Key Laboratory of Green Pesticide Key Laboratory of Green Pesticide and Agricultural BioengineeringMinistry of EducationGuizhou UniversityGuiyang 550025China School of Chemistry Chemical Engineeringand BiotechnologyNanyang Technological UniversitySingapore 637371Singapore

Organoseleniums exhibit a diverse set of biological activities that are pivotal for drug discovery and are widely explored in synthetic chemistry and material *** many transformations have been developed for non-enantioselective C–Se bond formations,the catalyst-controlled stereoselective preparation of chiral organoseleniums continues to be of considerable *** particular,there are limited studies on the enantioselective seleno-Michael addition reactions to access chiral selenium functional ***,we disclose a carbene-catalyzed highly enantioselective nucleophilic C–Se bond construction through formal[3+3]annulations between selenocarboxamides and bromoenals,affording seleno-thiazinone products with good yields and excellent *** choice of a weak inorganic base was pivotal to suppressing the unproductive racemization and decomposition of the selenium ***,the catalytically generated chiral selenium-containing heterocyclic products feature remarkable antimicrobial activities that could serve as promising lead scaffolds for further agrochemical development.

关键词： seleno-Michael addition organocatalysis N-heterocyclic carbene seleno-heterocycles antimicrobial activity

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Self-powered stimuli responsive material for dual stimulation of heat and guest molecules

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Chinese Chemical Letters 2024年第2期35卷 590-593页

作者： Jintao Men Ke Xu Taiting sha.Lei He Yan Xu Jie Mu Tijian Yin Qiong Ye Jiangsu Key Laboratory for Science and Applications of Molecular Ferroelectrics and School of Chemistry and Chemical Engineering Southeast UniversityNanjing 211189China

Stimuli-responsive smart materials exhibit reverse chemical/physical changes in response to external stimuli and research on stimuli-responsive smart materials with self-powered properties is still uncultivated ***,we report perovskite crystalline self-powered multiple stimuli-responsive materials triggered by chemical and thermal stimuli.[HMEP]PbI_(3)·(H_(2)O)(1;HMEP is a hydroxytris(1-methylethyl)phosphorus cation)crystallizes in a chiral space group P 21 at 293 K and has the piezoelectric reaction(d_(33)=10 pC/N and output voltage=1 V)of self-powered modes,this value is larger than the value of 3 pC/N for the classical piezoelectric material *** materials can generate energy due to mechanical deformation,and using thermal heating to lose water,[HMEP]PbI_(3)(2)can be obtained.2 crystallizes in the non-centrosymmetric space group,undergoes two reversible phase transitions at 243/255 K and 315/348 K,and shows second harmonic generation ***,2 can return to the hydrated form 1 after absorbing *** work will lay the foundation for self-powered stimuli-responsive compounds and contribute to the construction of novel organic-inorganic hybrid materials with second harmonic generation switching.

关键词： Self-powered Dual stimulation reactive Phase transition SHG switch Organic-inorganic hybrid perovskite

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High-entropy catalysts for electrochemical water-electrolysis of hydrogen evolution and oxygen evolution reactions

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Frontiers in Energy 2024年第3期18卷 265-290页

作者： Simiao sha.Riyue GE Ying LI Julie M.CAIRNEY Rongkun ZHENG Sean LI Bin LIU Jiujun ZHANG Wenxian LI School of Materials Science and Engineering Shanghai UniversityShanghai 200444China School of Chemical and Environmental Engineering Anhui Polytechnic UniversityWuhu 241000China Australian Centre for Microscopy and Microanalysis School of AerospaceMechanical and Mechatronic EngineeringThe University of SydneySydney NSW 2006Australia School of Physics The University of SydneySydney NSW 2006Australia School of Materials Science and Engineering UNSW Materials&Manufacturing Futures InstituteUniversity of New South WalesSydney NSW 2052Australia College of Materials Science and Engineering Fuzhou UniversityFuzhou 350108China

High entropy materials (HEMs) have developed rapidly in the field of electrocatalytic water-electrolysis for oxygen evolution reaction (OER) and hydrogen evolution reaction (HER) due to their unique properties. In particular, HEM catalysts are composed of many elements. Therefore, they have rich active sites and enhanced entropy stability relative to single atoms. In this paper, the preparation strategies and applications of HEM catalysts in electrochemical water-electrolysis are reviewed to explore the stabilization of HEMs and their catalytic mechanisms as well as their application in support green hydrogen production. First, the concept and four characteristics of HEMs are introduced based on entropy and composition. Then, synthetic strategies of HEM catalysts are systematically reviewed in terms of the categories of bottom-up and top-down. The application of HEMs as catalysts for electrochemical water-electrolysis in recent years is emphatically discussed, and the mechanisms of improving the performance of electrocatalysis is expounded by combining theoretical calculation technology and ex-situ/in situ characterization experiments. Finally, the application prospect of HEMs is proposed to conquer the challenges in HEM catalyst fabrications and applications.

关键词： high-entropy electrocatalysis synthetic methods water-electrolysis hydrogen and oxygen evolutions

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Spin-orbit torque effect in silicon-based sputtered Mn_(3)Sn film

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Chinese Physics B 2024年第10期33卷 394-399页

作者： sha.Lu Dequan Meng Adnan Khan Ziao Wang Shiwei Chen Shiheng Liang School of Physics Hubei UniversityWuhan 430062China Key Laboratory for Intelligent Sensing System and Security of Ministry of Education Wuhan 430062China

Noncollinear antiferromagnet Mn_(3)Sn has shown remarkable efficiency in charge-spin conversion,a novel magnetic spin Hall effect,and a stable topological antiferromagnetic state,which has resulted in great interest from researchers in the field of spin-orbit *** research has primarily focused on the spin-orbit torque effect of epitaxially grown noncollinear antiferromagnet Mn_(3)Sn ***,this method is not suitable for large-scale industrial *** this study,amorphous Mn_(3)Sn films and Mn_(3)Sn/Py heterostructures were prepared using magnetron sputtering on silicon *** spin-torque ferromagnetic resonance measurement demonstrated that only the conventional spin-orbit torque effect generated by in-plane polarized spin currents existed in the Mn_(3)Sn/Py heterostructure,with a spin-orbit torque efficiency of ***,we prepared the perpendicular magnetized Mn_(3)Sn/CoTb heterostructure based on amorphous Mn_(3)Sn film,where the spin-orbit torque driven perpendicular magnetization switching was achieved with a lower critical switching current density(3.9×10^(7)A/cm^(2))compared to Ta/CoTb *** research reveals the spin-orbit torque effect of amorphous Mn_(3)Sn films and establishes a foundation for further advancement in the practical application of Mn_(3)Sn materials in spintronic devices.

关键词： spintronics noncollinear antiferromagnetism spin-orbit torque

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