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Effects of dispersoid preforming via multistep sintering of oxide dispersion-strengthened CoCrFeMnNi high-entropy alloy

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Journal of Materials Science & Technology 2023年第9期140卷 187-200页

作者： seunghyeok chung Ji Ho Shin Ho Jin Ryu Department of Nuclear and Quantum Engineering Korea Advanced Institute of Science and Technology(KAIST)Daejeon 34141Republic of Korea Central Research Institute Korea Hydro and Nuclear Power Co.Ltd.(KHNP)Daejeon 34101Republic of Korea

Dispersoid formation and microstructural evolution in an oxide dispersion-strengthened CoCrFeMnNi high-entropy alloy(HEA)using a newly designed multistep sintering process are *** proposed multistep sintering consists of a dispersoid preforming heat treatment of as-milled 0.1 wt%Y_(2)O_(3)-CoCrFeMnNi high-entropy alloy powders at 800℃,followed by sintering at 800–1000℃ under uniaxial *** the conventional single-step sintered bulk,the coarsened BCC Y_(2)O_(3)dispersoids mainly form with an incoherent interface with the HEA *** contrast,finer FCC Y_(2)O_(3)dispersoids,an atypical form of Y_(2)O_(3),are formed in the matrix region after multistep *** of FCC Y_(2)O_(3)disper-soids is initiated on the favorable facet,the{111}plane of the austenitic matrix,with the formation of a semi-coherent interface with the matrix during the dispersoid preforming heat treatment and it maintains its refined size even after *** is found that dispersoid preforming prior to sintering appears promising to control the finer dispersoid formation and refined grain structure.

关键词： Oxide dispersion strengthening High-Entropy alloy Multistep sintering Dispersoid preforming Microstructure evolution Interfacial structure

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Effects of TiC on the microstructure refinement and mechanical property enhancement of additive manufactured Inconel 625/TiC metal matrix composites fabricated with novel core-shell composite powder

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Journal of Materials Science & Technology 2023年第33期164卷 13-26页

作者： Taegyu Lee Wonjong Jeong seunghyeok chung Ho Jin Ryu Department of Materials Science and Engineering Korea Advanced Institute of Science and TechnologyYu Seong-GuDae Hak-Ro 29134141 DaejeonRepublic of Korea Department of Nuclear and Quantum Engineering Korea Advanced Institute of Science and TechnologyYu Seong-GuDae Hak-Ro 29134141 DaejeonRepublic of Korea

The flexible product shape of additive manufacturing(AM)is attractive,but the process suffers from a lack of material property diversity due to a limited number of printable alloys and post-processing *** overcome this problem,the AM of metal matrix composites(MMCs)is a highly suitable solution because the properties of MMC can be tailored using various ***,extensive research has been conducted on the AM of MMCs;however,the major huddle for this process has been the difficulties in preparing feedstock powder and operating the AM *** study introduces an easily synthesizable core-shell composite powder,which was fabricated by a recently developed process called the SMART *** core-shell powder has a novel morphology,consisting of a metal core and composite shell,distinguishing it from the powders used in conventional AM *** 625/TiCp composites were fabricated using the core-shell composite powder,with various fractions of TiCp up to 10 vol.%.Compared to additive-manufactured Inconel 625,the additive-manufactured MMCs showed enhanced strength with significantly fewer *** results of this study may accelerate the application of MMC fabricated by AM,which offers superior properties and reliability compared to casting and powder metallurgy due to the higher degree of dislocation density and reinforcement dispersion.

关键词： Powder treatment Composite powder Metal matrix composite Additive manufacturing Nickel-based superalloy Directed energy deposition

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The effects of Y pre-alloying on the in-situ dispersoids of ODS Co Cr Fe Mn Ni high-entropy alloy

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Journal of Materials Science & Technology 2021年第26期85卷 62-75页

作者： seunghyeok chung Bin Lee Soo Yeol Lee Changwoo Do Ho Jin Ryu Department of Nuclear and Quantum Engineering Korea Advanced Institute of Science and TechnologyDaejeon 34141Republic of Korea Manufacturing Technology Office Korea Institute for Rare MetalKorea Institue of Industrial TechnologyGet-Pearl TowerGaetbeol-ro 12Yeonsu-guIncheon 21999Republic of Korea Department of Materials Science and Engineering Chungnam National UniversityDaejeon 34134Republic of Korea Neutron Scattering Division Oak Ridge National LaboratoryOak RidgeTN 37831USA

Oxide dispersion strengthened CoCrFeMnNi high-entropy alloys(ODS-HEAs)were prepared using two different powder preparation methods classified by yttrium addition strategy to investigate the effects of in-situ and ex-situ oxide dispersoid formation on the microstructure and mechanical *** micro structural analysis was carried out by X-ray diffraction(XRD),electron backscattered diffraction(EBSD),high-resolution transmission electron microscopy(HRTEM),atom probe tomography(APT),and small-angle neutron scattering(SANS).Cryo-milled powder analysis,grain structure evolution after spark plasma sintering,dispersoid characteristics,and matrix/dispersoid interface structure analysis of the insitu and ex-situ dispersoids within the high-entropy alloy(HEA)matrix were *** in-situ dispersoid formation was dominantly observed in the Y-alloyed ODS-HEA through the construction of a coherent interface relationship with complex chemical composition,leading to an increase in the Zener pinning forces on the grain boundary ***-HEA with in-situ oxide dispersoids enhanced the formation of ultrafine-grained structures with an average diameter of 330 nm at a sintering temperature of 1173 *** study shows that the Y pre-alloying method is efficient in achieving fine coherent dispersoids with an ultra fine-grained structure,resulting in an enhancement of the tensile strength of the CoCrFeMnNi HEA.

关键词： Oxide dispersion strengthened(ODS)alloy High-entropy alloy In-situ oxide dispersoid formation Microstructure Mechanical property

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