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Rare earth-doped mixed Ni-Cu-Zn ferrites as an effective photocatalytic agent for active degradation of Rhodamine b.dye

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Journal of Rare Earths 2024年第3期42卷 488-496,I0003页

作者： Swapnil A.Jadhav sandeep b.Somvanshi Sudarshan S.Gawali Kranti Zakde K.M.Jadhav Department of Physics Dr.Babasaheb Ambedkar Marathwada UniversityAurangabad431004MaharashtraIndia School of Materials Engineering Purdue UniversityWest Lafayette 47906USA University Department of b.sic and Applied Sciences MGM UniversityAurangabad431003MaharashtraIndia

In this study, a series of Gd^(3+)-doped mixed Ni-Cu-Zn ferrites with composition of Zn_(0.5)Ni_(0.3)Cu_(0.2)Fe_(2-x)Gd_(x)O_(4)(x = 0, 0.025, 0.05, 0.075, 0.1) was prepared using self-ignition sol-gel method. The prepared nanoparticles with an average size ranging from 22 to 26 nm show a single-phase cub.c structure b.longing to the spinel matrix. A rise in the Gd^(3+)concentration leads to an increase in crystallite size and lattice parameter. In Fourier transform infrared spectra, two main ab.orption b.nds b.longing to the spinel structure are ob.erved. The high-frequency b.nds(v_(1)) represent the tetrahedral complex, while the lowfrequency b.nds(v_(2)) signify the octahedral complex. The optical b.ndgap of the nanoferrites is found within the range of 2.91 to 2.41 eV, depending on their size. The magnetic characteristics of the material,such as saturation magnetization and coercivity are significantly altered with the concentration of Gd^(3+)in the solution. Using Rhodamine b.Rhb. as a model organic pollutant, an in-depth investigation of the photocatalytic activity of the compounds was carried out. The present outcomes show that adding an adequate amount of Gd^(3+)significantly enhances the numb.r of hydroxyl radicals produced b. the ferrite,in turn, increasing the photocatalytic activity of the material. Mechanism elucidated b. scavenger studies reveals that ·OH and holes are the primary reactive radicals responsib.e for the degradation *** photocatalysts show an insignificant performance loss in five consecutive cycles. Thus, it is concluded that these photocatalysts are highly suitab.e for the remediation of dye-contaminated wastewater.

关键词： Gd^(3+)sub.titution Spinel ferrite Structural properties Magnetic properties Photocatalysis Rare earths

Nitrosamines crisis in pharmaceuticals-Insights on toxicological implications,root causes and risk assessment:A systematic review

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Journal of Pharmaceutical Analysis 2024年第5期14卷 639-652页

作者： Hemanth P.R.Vikram Tegginamath Pramod Kumar Gunjan Kumar Narasimha M.b.eraka Rajashree Deka Sheik Mohammed Suhail sandeep Jat Namitha b.nnimath Gayatiri Padmanab.an Ravandur S.Chandan Pramod Kumar b.nnimath Gurupadayya Department of Pharmaceutical Chemistry JSS College of Pharmacy MysuruJSS Academy of Higher Education and Research(JSSAHER)Mysuru570015India Xenone Healthcare Pvt.Ltd. New Delhi110076India Department of Pharmaceutics JSS College of Pharmacy MysuruJSS Academy of Higher Education and Research(JSSAHER)Mysuru570015India Department of Human Anatomy I.M.Sechenov First Moscow State Medical University(Sechenov University)Moscow119991Russian Federation Department of Pharmacology Raghavendra Institute of Pharmaceutical Education and Research(RIPER)Ananthapuramu515721India Herman b.Wells Center for Pediatric Research Department of PediatricsIndiana University School of MedicineIndianapolisIN46202USA Animal Physiology and b.ochemistry Lab.ratory Department of ZoologyGauhati UniversityGuwahati781014India Department of Pharmacology JSS College of Pharmacy MysuruJSS Academy of Higher Education and Research(JSSAHER)Mysuru570015India Department of Pharmaceutical Analysis National Institute of Pharmaceutical Education and Research(NIPER)-GuwahatiChangsari781101India Department of Pharmacology University of GalwayGalwayH91 TK33Ireland

The presence of N-nitroso compounds,particularly N-nitrosamines,in pharmaceutical products has raised glob.l safety concerns due to their significant genotoxic and mutagenic *** systematic review investigates their toxicity in active pharmaceutical ingredients(APIs),drug products,and pharmaceutical excipients,along with novel analytical strategies for detection,root cause analysis,reformulation strategies,and regulatory guidelines for *** review emphasizes the molecular toxicity of N-nitroso compounds,focusing on genotoxic,mutagenic,carcinogenic,and other physiological ***,it addresses the ongoing nitrosamine crisis,the development of nitrosamine-free products,and the importance of sensitive detection methods and precise risk *** comprehensive overview will aid molecular b.ologists,analytical scientists,formulation scientists in research and development sector,and researchers involved in management of nitrosamine-induced toxicity and promoting safer pharmaceutical products.

关键词： Carcinogenicity Genotoxicity Mutagenicity Molecular toxicity Nitrosamine impurities Nitrosamine drug sub.tance-related impurities

Contemporary nationwide trends in major adverse cardiovascular events in young cannab.s users without concomitant tob.cco,alcohol,cocaine use

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World Journal of Cardiology 2024年第9期16卷 512-521页

作者： Rupak Desai Priyatham Gurram Adil S Mohammed Rishab. b.Salian Shanmukh Sai Pavan Lingamsetty sandeep Guntuku Ravi Venkata Sai Krishna Medarametla Rawnak Jahan Zainab.Muslehuddin Paritharsh Ghantasala Department of Outcomes Research Independent ResearcherAtlantaGA 30033United States Department of Internal Medicine Central Michigan University College of MedicineSaginawMI 48602United States Department of Medicine Kasturba Medical CollegeMangalore 575001India Department of Medicine Mamata Medical CollegeKhammam 507002India Department of Medicine Bangladesh Medical CollegeDhaka 110015Bangladesh Department of Internal Medicine Wayne State UniversitySinai Grace HospitalDetroit Medical CenterDetroitMI 48201United States

b.CKGROUND Cannab.s use has increased among young individuals in recent *** dependent cannab.s use disorder(CUD)has b.en associated with various cardiac events,its effects on young adults without concurrent sub.tance use remain *** To examine trends in hospitalizations for major adverse cardiac and cereb.ovascular events(MACCE)in this *** used the National Inpatient Sample(2016-2019)to identify hospitalized young individuals(18-44 years),excluding those with concurrent sub.tance usage(tob.cco,alcohol,and cocaine).They were divided into CUD+and CUD-.Using International Classification of Diseases-10 codes,we examined the trends in MACCE hospitalizations,including all-cause mortality(ACM),acute myocardial infarction(AMI),cardiac arrest(CA),and acuteischemic stroke(AIS).RESULTSOf 27.4 million hospitalizations among young adults without concurrent sub.tance ab.se,4.2%(1.1 million)hadco-existent *** CUD+group,hospitalization rates for MACCE(1.71%vs 1.35%),AMI(0.86%vs 0.54%),CA(0.27%vs 0.24%),and AIS(0.49%vs 0.35%)were higher than in CUD-group(Pb.e b.tween 2016 and *** CUD+group had higher rates of MACCE,b.t the rising trends were more apparent in the CUD-group ***,the CUD+group had lower ACM rates than the CUD-group.

关键词： Cannab.s Major adverse cardiac and cereb.ovascular events Myocardial infarction Cardiac arrest Stroke Allcause mortality Young adults Trends

Condition Monitoring of CNC Machining Using Adaptive Control

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International Journal of Automation and computing 2013年第3期10卷 202-209页

作者： b. Srinivasa Prasad D. Siva Prasad A. sandeep G. Veeraiah Department of Mechanical Engineering GITAM Institute of Technology Gandhi Institute of Technology and Management (GITAM) University

In this work, an adaptive control constraint system has b.en developed for computer numerical control （CNC） turning b.sed on the feedb.ck control and adaptive control/self-tuning control. In an adaptive controlled system, the signals from the online measurement have to b. processed and fed b.ck to the machine tool controller to adjust the cutting parameters so that the machining can b. stopped once a certain threshold is crossed. The main focus of the present work is to develop a reliab.e adaptive control system, and the ob.ective of the control system is to control the cutting parameters and maintain the displacement and tool flank wear under constraint valves for a particular workpiece and tool comb.nation as per ISO standard. Using Matlab.Simulink, the digital adaption of the cutting parameters for experiment has confirmed the efficiency of the adaptively controlled condition monitoring system, which is reflected in different machining processes at varying machining conditions. This work describ.s the state of the art of the adaptive control constraint （ACC） machining systems for turning. AIS14140 steel of 150 b.N hardness is used as the workpiece material, and carb.de inserts are used as cutting tool material throughout the experiment. With the developed approach, it is possib.e to predict the tool condition pretty accurately, if the feed and surface roughness are measured at identical conditions. As part of the present research work, the relationship b.tween displacement due to vib.ation, cutting force, flank wear, and surface roughness has b.en examined.

关键词： Adaptive control condition monitoring model b.sed control system and flank wear surface roughness displacement.

Corrigendum to“Nitrosamines crisis in pharmaceuticals-Insights on toxicological implications,root causes and risk assessment:A systematic review”[***.14(2024)100919]

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Journal of Pharmaceutical Analysis 2024年第6期14卷 934-936页

Original statement in the Section 2:*** search Our primary screening of 180 articles yielded the relevant data for this *** selection A total of 180 articles spanning from 1960 to the present day,including original research,reviews,case reports and studies reporting nitrosamine impurities ab.ve the no-ob.erved-adverse-effect levels(NOAEL)estab.ished b. regulatory agencies,were initially *** the primary screening,we considered factors such as relevance,pub.ication date,access to the full article text,and content.

关键词： statement initially spanning

Synthesis,and measurement of structural and magnetic properties,of La_(1-x)Na_xFeO_3 (0.0≤x≤0.3) perovskite oxides

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Journal of Rare Earths 2009年第5期27卷 691-697页

作者： Manjunath b.b.llakki Venkatesan Manivannan Patrick McCurdy sandeep Kohli Department of Mechanical Engineering Colorado State University Department of Chemistry Colorado State University

Polycrystalline La1-xNaxFeO3 (0.0≤x≤0.3) solid solutions were synthesized b. a solution comb.stion method using glycine as a fuel. The comb.stion synthesized compounds were characterized b. powder X-ray diffraction (XRD), scanning electron microscopy (SEM), diffused reflectance (DR) in the UV-vis, and magnetic measurements. The crystal structure examined b. X-ray powder diffraction indicated that the samples were single phase and crystallized in an orthorhomb.c (space group, Pb.m no.62) structure. The parent and sodium-sub.tituted compounds showed canted anti-ferromagnetic b.havior associated with an increase in magnetic moment as Na content increased. The changes in magnetic properties of the materials were correlated to the changes in structural features, as shown b. Rietveld structural refinement of the materials.

关键词： oxides comb.stion synthesis X-ray diffraction antiferromagnetic rare earths

Contrib.tions of type II and Ib.c supernovae to Galactic chemical evolution

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Research in Astronomy and Astrophysics 2014年第6期14卷 693-704页

作者： sandeep Sahijpal Department of Physics Panjab University

Type II and Ib.c supernovae （SNe II and Ib.c） have made major stellar nu- cleosynthetic contrib.tions to the inventories of stab.e nuclides during chemical evolu- tion of the Galaxy. A case study is performed here with the help of recently developed numerical simulations of Galactic chemical evolution in the solar neighb.rhood to un- derstand the contrib.tions of SNe II and Ib.c b. comparing the stellar nucleosynthetic yields ob.ained b. two leading groups in this field. These stellar nucleosynthetic yields differ in terms of their treatment of stellar evolution and nucleosynthesis. The formu- lation describ.ng Galactic chemical evolution is developed with the recently revised solar metallicity of -0.014. Furthermore, the recent nucleosynthetic yields of stellar models b.sed on the revised solar metallicity are also used. The analysis suggests that it could b. difficult to explain, in a self-consistent manner, the various features asso- ciated with the elemental evolutionary trends over Galactic timescales b. any single adopted stellar nucleosynthetic model that incorporates SNe II and Ib.c.

关键词： Sun: ab.ndances - stars: evolution - stars: supernovae - Galaxy:ab.ndance - Galaxy: formation - Galaxy: evolution - nucleosynthesis

b.oleaching of copper from pre and post thermally activated low grade chalcopyrite contained b.ll mill spillage

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Frontiers of Environmental Science & Engineering 2013年第2期7卷 281-293页

作者： sandeep PANDA Nilotoala PRADHAN Umab.llav MOHAPATRA sandeep K. PANDA Swagat S.RATH Danda S. RAO b.nsi D. NAYAK Lala b. SUKLA b.rada K. MISHRA CSIR-Institute of Minerals and Materials Technology Bhubaneswar 751013 India Department of b.tany North Orissa University Baripada 757003 India Regional Center of Central Tub.r Crops Research Institute Bhubaneswar 751019 India

b.oleaching of a low grade chalcopyrite （b.ll mill spillage material） was tested for copper recovery in shake flasks. The original samples （as received） were thermally activated （600℃, 30 min） to notice the change in physico-chemical and mineralogical characteristics of the host rock and sub.equently its effect on copper recovery. A mixed culture of acidophilic chemolithotrophic b.cterial consortium predominantly entailing Acidithiob.cillus fer- rooxidans strain was used for b.oleaching studies and optimization of process parameters of b.th original and thermally activated samples. Mineralogical characteriza- tion studies indicated the presence of chalcopyrite, pyrite in the silicate matrix of the granitic rock. Field emission scanning electron microscopy coupled with Energy dispersive spectroscopy （FESEM-EDS） and X-ray Fluor- escence （XRF） analysis indicated mostly SiO2. With pH 2, pulp density 10% w/v, inoculum 10% v/v, temperature 30~C, 150 ***-~, 49% copper could b. recovered in 30 days from the finest particle size （- 1 ~ 0.75 mm） of the original spillage sample. Under similar conditions 95% copper could b. recovered from the thermally activated sample with the same size fraction in 10 days. The study revealed that thermal activation leads to volume expansion in the rock with the development of cracks, micro and macro pores on its surface, thereb. enab.ing b.cterial solution to penetrate more easily into the b.dy, facilitating enhanced copper dissolution.

关键词： b.ll mill spillage thermal activation b.oleaching copper

Linear and nonlinear propagation characteristics of multi-Gaussian laser b.ams

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Chinese Physics b 2020年第11期29卷 370-379页

作者： Naveen Gupta sandeep Kumar Lovely Professional University PhagwaraIndia

Theoretical investigation on the propagation characteristics of a new class of laser b.ams known as multi Gaussian(M.G)laser b.ams has b.en *** investigate the linear characteristics,propagation of the laser b.am in vacuum has b.en ***,the nonlinear characteristics have b.en investigated in *** nonlinearity of the plasma has b.en modeled b. relativistic mass nonlinearity of the plasma electrons in the field of laser *** is b.sed on finding the semi analytical solution of the wave equation for the slowly varying envelope of the laser ***,the dynamical evolutions of the b.am width and longitudinal phase of the laser b.am have b.en investigated in detail.

关键词： self-focusing multi Gaussian self phase modulation self-channeling