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CO oxidation and 4-nitrophenol reduction over ceria-promoted platinum nanoparticles impregnated with ZSm-5 zeolite

Journal of Rare Earths 2022年第8期40卷 1247-1254页

作者： Zeinhom m.el-bahy mohammed T.Alotaibi salah m.el-bahy Department of Chemistry Faculty of ScienceAl-Azhar UniversityNasr City11884CairoEgypt Department of Chemistry Turabah University CollegeTaif UniversityP.O.Box 11099Taif 21944Saudi Arabia

Active new ceria-promoted platinum supported on ZSm-5 catalysts were prepared and characterized by X-ray diffraction(XRD),Fourier transform infrared spectra(FTIR),transform.electron microscopy(TEm),temperature programmed desorption(TPD),and FTIR of CO *** samples were prepared by the incipient wetness impregnation method and calcined at 500℃.The XRD patterns and FTIR spectra prove that the zeolite framework is kept unaltered after metal *** images prove the presence of Pt nanoparticles with particle size starting from 14 to 27 *** FTIR data suggest the formation of Pt-O-Ce ***-situ FTIR of CO adsorption over reduced samples proves the presence of Pt~0 only,and no Pt^(n+)-CO species are *** prepared catalysts were tested in both oxidation reaction(CO oxidation) in the gas phase and in reduction reaction(4-nitrophenol reduction) in the aqueous ***,CO oxidation by O_(2) results in the formation of a CO_(2) peak at 2347 cm^(-1) as the only CO oxidation product in the studied frequency *** intensity of the CO_(2) peak increases after the addition of Ce,and it is 4 times higher in Pt_(1) Ce_(0.5)ZSm-5 than that in the Ce-free *** to the FTIR data and previous reports,the increase in the catalytic activity may be due to the formation of Pt-O-Ce ***,Ce-promoted Pt_(1) ZSm5 also exhibits enhanced catalytic activity towards the reduction of 4-nitrophenol to 4-aminophenol by NaBH_(4) in the aqueous *** first-order rate constant of the reduction increases ≈13 times after incorporating equal ratios of Pt and Ce(Pt_(1) Ce_(1)ZSm-5),and the activation energy(E_(a)) decreases to 40% of that in the reaction over Pt_(1) ZSm-5.

关键词： 4-Nitrophenol CO oxidation TPD-CO Platinum-cerium ZSm-5 Rare earths

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Facial synthesis of carbon nanotube interweaved FeOOH as chloride-insertion electrode for highly efficient faradic capacitive deionization

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Progress in Natural Science:materials International 2024年第4期34卷 731-738页

作者： Lu Zhang Harry Lye Hin Chong Dan Luo salah m.el-bahy Pak Yan moh Xingtao Xu Zeinhom m.el-bahy Environmental Science Programme Faculty of Science and Natural Resources Universiti Malaysia Sabah Water Research Unit Faculty of Science and Natural Resources Universiti Malaysia Sabah marine Science and Technology College Zhejiang Ocean University Department of Chemistry Turabah University College Taif University Department of Chemistry Faculty of Science Al-Azhar University

Faradic-based capacitive deionization（FDI） has been widely acknowledged as one of the most promising desalination techniques to solve the freshwater crisis, yet was largely limited by heavily trailed development of its anode materials, which subsequently hindered its desalination performance in terms of both desalination capacity and stability. Herein, we developed a new type of anode material for FDI by coupling chloride-insertion FeOOH with carbon nanotubes（CNTs@FeOOH）. The essence of this study lay in the composition of FeOOH with CNTs that could not only facilitate charge/electron transfer but also prevent structural aggregation. Consequently, the CNTs@FeOOH-based FDI system displays excellent desalination performance(desalination capacity: 50.36 mg g-1; desalination rate: 0.41 mg g-1s-1) with robust long-term stability（13.86 % reduction over 80 cycles）, which could motivate the future development of other highly-efficient desalination systems.

关键词： Faradic capacitive deionization Capacitive deionization FeOOH Carbon nanotube

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Vertically Aligned Silicon Carbide Nanowires/Boron Nitride Cellulose Aerogel Networks Enhanced Thermal Conductivity and electromagnetic Absorbing of Epoxy Composites

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Nano-micro Letters 2022年第7期14卷 209-227页

作者： Duo Pan Gui Yang Hala mAbo-Dief Jingwen Dong Fengmei Su Chuntai Liu Yifan Li Ben Bin Xu Vignesh murugadoss Nithesh Naik salah mel-bahy Zeinhom mel-bahy minan Huang Zhanhu Guo Key Laboratory of materials Processing and mold(Zhengzhou University) Ministry of EducationNational Engineering Research Center for Advanced Polymer Processing TechnologyZhengzhou UniversityZhengzhou 450002People’s Republic of China Department of Chemistry College of ScienceTaif UniversityP.O.Box 11099Taif 21944Saudi Arabia mechanical and Construction Engineering Faculty of Engineering and EnvironmentNorthumbria UniversityNewcastle upon Tyne NE18STUK Integrated Composites Laboratory(ICL) Department of Chemical and Biomolecular EngineeringUniversity of TennesseeKnoxvilleTN 37996USA Advanced materials Division Engineered Multifunctional Composites(EMC)Nanotech LLCKnoxvilleTN 37934USA College of materials Science and Engineering Taiyuan University of Science and TechnologyTaiyuan 030024People’s Republic of China Department of mechanical and manufacturing Engineering Manipal Institute of TechnologyManipal Academy of Higher EducationManipalKarnataka 576104India Department of Chemistry Turabah University CollegeTaif UniversityP.O.Box 11099Taif 21944Saudi Arabia Department of Chemistry Al-Azhar UniversityNasr CityCairo 11884Egypt

With the innovation of microelectronics technology, the heat dissipation problem inside the device will face a severe test. In this work, cellulose aerogel(CA) with highly enhanced thermal conductivity(TC) in vertical planes was successfully obtained by constructing a vertically aligned silicon carbide nanowires(SiC NWs)/boron nitride(BN) network via the ice template-assisted strategy. The unique network structure of SiC NWs connected to BN ensures that the TC of the composite in the vertical direction reaches 2.21 W m^(-1) K^(-1) at a low hybrid filler loading of 16.69 wt%, which was increased by 890% compared to pure epoxy(EP). In addition, relying on unique porous network structure of CA, EP-based composite also showed higher TC than other comparative samples in the horizontal direction. meanwhile, the composite exhibits good electrically insulating with a volume electrical resistivity about 2.35 × 10^(11) Ω cm and displays excellent electromagnetic wave absorption performance with a minimum reflection loss of-21.5 dB and a wide effective absorption bandwidth(m 8.8 to 11.6 GHz. Therefore, this work provides a new strategy for manufacturing polymer-based composites with excellent multifunctional performances in microelectronic packaging applications.

关键词： Epoxy Ice template Vertical alignment Thermal conductivity multifunctionality

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One-pot hydrothermal preparation of hierarchical manganese oxide nanorods for high-performance symmetric supercapacitors

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Journal of Energy Chemistry 2022年第2期31卷 116-126页

作者： Bidhan Pandit Emad S.Goda mahmoud H.Abu elella Aafaq ur Rehman Sang Eun Hong Sachin R.Rondiya Pranay Barkataki Shoyebmohamad F.Shaikh Abdullah m.Al-Enizi salah mel-bahy Kuk Ro Yoon Department of materials Science and Engineering and Chemical Engineering Universidad Carlos III de MadridAvenida de la Universidad 3028911 LeganésMadridSpain Organic Nanomaterials Lab Department of ChemistryHannam UniversityDaejeon 34054Republic of Korea Fire Protection Laboratory National Institute of Standards136Giza 12211Egypt Chemistry Department Faculty of ScienceCairo UniversityGiza 12613Egypt Graduate School of Energy Science and Technology Chungnam National University99 Daehak-roYuseong-guDaejeon 34134Republic of Korea School of Chemistry Cardiff UniversityMain BuildingPark PlaceCardiffCF103AT WalesUnited Kingdom Department of Physics Visvesvaraya National Institute of TechnologySouth Ambazari RoadNagpur-440010MaharashtraIndia Department of Chemistry College of ScienceKing Saud UniversityP.O.Box 2455Riyadh 11451Saudi Arabia Department of Chemistry Turabah University CollegeTaif UniversityP.O.Box 11099Taif 21944Saudi Arabia

An eco-friendly,new,and controllable approach for the preparation of manganese oxide(a-mnO_(2))nanorods has been introduced using hydrothermal reaction for supercapacitor *** in-depth crystal structure analysis ofα-mnO_(2) is analyzed by X-ray Rietveld refinement by using Full Prof program with the help of pseudo-Voigt profile *** developed a-mnO_(2) electrode attains a remarkable capacitance of 577.7 F/g recorded at a current density value of 1 A/g with an excellent cycle life when is used for 10,000 repeated cycles due to the porous nanorod-morphology assisting the ease penetration of electrolyte ions into the electroactive *** diffusive and capacitive contributions of the electrode have been estimated by considering standard numerical packages in *** successfully assembling the aqueous symmetric supercapacitor(SSC)cell by utilizing the as-preparedα-mnO_(2),an excellent capacitance of 163.5 F/g and energy density of 58.1 Wh/kg at the constant current density of 0.5 A/g are obtained with an expanded potential frame of 1.6 ***,the cell has exceptionally withstood up to 10,000 cycles with an ultimate capacitance retention of 94.1%including the ability to light an LED for 18 *** findings recommend the developed a-mnO_(2) electrode to be a highly felicitous electrode for the field of energy storage.

关键词： α-mnO_(2)nanorods Rietveld refinement Symmetrical supercapacitors High energy density

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Effect of Pd or Ir on the catalytic performance of mo/H-ZSm-5 during the non-oxidative conversion of natural gas to petrochemicals

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Journal of Natural Gas Chemistry 2008年第4期17卷 337-343页

作者： Ahmed K.Aboul-Gheit Ahmed E.Awadallah salah m.el-Kossy Abdel-Lateef H.mahmoud Process Development Division Egyptian Petroleum Research Institute Faculty of Science Department of ChemistryMNF University Ageeba Petroleum Co.

Natural gas conversion to petrochemicals, principally, benzene, naphthalene, toluene, as well as ethylene under non-oxidative conditions was examined in a fixed bed flow reactor at 700 ℃ and gaseous hourly space velocity （GHSV） of 1500 ml·g ^-1·h^-1 at time-on-stream ranging from 5 rain to 4 h using catalysts containing 6.0%mo/H-ZSm-5 promoted with Pd or Ir metal. The catalysts were characterized by XRD, TPD, and TGA. The addition of Pd or Ir to 6%mo/H-ZSm-5 catalyst promoted ethylene production but inhibited the cyclization reaction to aromatics owing to the strong interaction between these noble metals and the framework Al species, which were attached to the acid sites during the impregnation process. Coke deposition on the catalysts was found to decrease upon addition of 0.5wt% of Pd or Ir to 6%mo/H-ZSm-5 catalyst owing to the hydrogenating activity of these metals.

关键词： natural gas methane benzene ethylene molybdenum Pd Ir H-ZSm-5

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The Impact of Inoculum Preparation media on Pollutant Removal through Phycoremediation of Agricultural Drainage Water by Desmodesmus sp.

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Phyton-International Journal of Experimental Botany 2023年第10期92卷 2875-2890页

作者： Asmaa salah Hoda Sany Abo el-Khair B.el-Sayed Reham m.el-Bahbohy Heba I.mohamed Ayman Amin Plant Physiology Division Department of Agricultural BotanyFaculty of AgricultureCairo UniversityGizaP.O.Box 12613Egypt Algal Biotechnology Unit National Research CentreDokkiGiza12622Egypt Biological and Geological Science Department Faculty of EducationAin Shams UniversityCairo11341Egypt

Water is the most essential natural resource for the future *** production is extensively water-dependent and a significant polluter of water ***,this work investigated the effect of two different preparation media[Bold’s Basal medium(BBm)and Domiati cheese whey(DCW)]for agricultural drainage water(ADW)*** treatments were incubated for 6 *** to the results of biomass productivity,specific growth rate,photosynthetic pigments,and biochemical composition,Desmodesmus *** grow in drainage water without *** two treatments significantly reduced the concentration of nitrate,phosphate,chemical oxygen demand,and sodium in ***,using cheese whey with BBm as inoculum preparation media enhanced the lipid accumulation in the algal biomass(25.4%w/w)and gave the best biodiesel properties among ***,combining remediation of drainage water with microalgae mass production can achieve the sustainability of agriculture.

关键词： Desmodesmus sp. drainage water nutrients recycle photosynthetic pigments phycoremediation water scarcity

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Assessing the Efficacy of Improved Learning in Hourly Global Irradiance Prediction

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Computers, materials & Continua 2023年第11期77卷 2579-2594页

作者： Abdennasser Dahmani Yamina Ammi Nadjem Bailek Alban Kuriqi Nadhir Al-Ansari salah Hanini Ilhami Colak Laith Abualigah el-Sayed m.el-kenawy Department of mechanical Engineering Faculty of Science and TechnologyGIDD Industrial Engineering and Sustainable Development LaboratoryUniversity of RelizaneBourmadiaRelizane48000Algeria Laboratory of Biomaterials and Transport Phenomena(LBmPT) University of MedeaUrban PoleMedea26000Algeria Energies and materials Research Laboratory Faculty of Sciences and TechnologyUniversity of TamanghassetTamanrasset10034Algeria Sustainable Development and Computer Science Laboratory Faculty of Sciences and TechnologyAhmed Draia University of AdrarAdrarAlgeria CERIS Instituto Superior TécnicoUniversidade de LisboaLisbon1049-001Portugal Civil Engineering Department University for Business and TechnologyPristina10000Kosovo Department of Civil Environmental and Natural Resources EngineeringLulea University of TechnologyLulea97187Sweden Engineering and Architecture Faculty Nisantasi UniversityIstanbulTurkey Computer Science Department Prince Hussein Bin Abdullah Faculty for Information TechnologyAl al-Bayt UniversityMafraq25113Jordan Hourani Center for Applied Scientific Research Al-Ahliyya Amman UniversityAmman19328Jordan mEU Research Unit Middle East UniversityAmman11831Jordan Applied Science Research Center Applied Science Private UniversityAmman11931Jordan School of Computer Sciences Universiti Sains MalaysiaPulau Pinang11800Malaysia Department of Computing and Information Systems School of Engineering and TechnologySunway University MalaysiaPetaling Jaya27500Malaysia Faculty of Artificial Intelligence Delta University for Science and TechnologyMansoura35712Egypt

Increasing global energy consumption has become an urgent problem as natural energy sources such as oil,gas,and uranium are rapidly running *** into renewable energy sources such as solar energy is being pursued to counter *** energy is one of the most promising renewable energy sources,as it has the potential to meet the world’s energy needs *** study aims to develop and evaluate artificial intelligence(AI)models for predicting hourly global *** hyperparameters were optimized using the Broyden-FletcherGoldfarb-Shanno(BFGS)quasi-Newton training algorithm and STATISTICA *** from two stations in Algeria with different climatic zones were used to develop the *** error measurements were used to determine the accuracy of the prediction models,including the correlation coefficient,the mean absolute error,and the root mean square error(RmSE).The optimal support vector machine(SVm)model showed exceptional efficiency during the training phase,with a high correlation coefficient(R=0.99)and a low mean absolute error(mAE=26.5741 Wh/m^(2)),as well as an RmSE of 38.7045 Wh/m^(2) across all ***,this study highlights the importance of accurate prediction models in the renewable energy,which can contribute to better energy management and planning.

关键词： Renewable energy energy prediction global irradiation artificial intelligence BFGS quasi-Newton training algorithm

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Impact of National Egyptian school feeding program on growth,development,and school achievement of school children

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World Journal of Pediatrics 2020年第4期16卷 393-400页

作者： A.m.metwally marwa m.el-Sonbaty L.A.el Etreby E.m.salah el-Din N.Abdel Hamid H.A.Hussien A.m.Hassanin Z.m.monir medical Research Division Community Medicine DepartmentNational Research Centre(Affiliation ID:60014618)DokkiCairoEgypt Department of Pediatrics College of MedicineTaibah UniversityMadinahKingdom of Saudi Arabia medical Research Division Child Health DepartmentNational Research Centre(Affiliation ID:60014618)DokkiCairoEgypt Agricultural Research Centre GizaEgypt

Background School feeding program(SFP)increases access to education and to better *** study aims to evaluate the effects of SFP on physical growth,cognitive development,psychosocial behavior,and learning achievement of school *** A quasi-experimental study was *** intervention group included 903 pupils in the fifth grade receiving the school meal,while the control group included 886 pupils,matched for age and sex,without *** meal consisted of a pie made of flour fortified with vitamins A,B6,B12,C,thiamin,riboflavin,niacin,folate,calcium,iron,zinc,and *** position,nutritional status,and dietary behavior were *** tests were *** behavior was rated and educational achievement was *** hoc and independent sample t tests were used to detect the association of the studied parameters with the intake of school *** Children who took the meal had better scores on visual memory,auditory vigilance tests(9.71±2.80 vs.7.45±3.25;25.02±3.36 vs.10.82±8.92,respectively,Pmemory test(8.20±2.21vs.7.75±3.05)(Pmeal was the main predictor of visual memory and auditory vigilance(Pmic achievements when combined with family size and meals’frequency(Pmeal improves academic achievements of school children.

关键词： Cognition Growth Performance School feeding

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The Effect of Atrial Septal Defect Closure on Cardiac Volumetric Changes in Adults, Transcatheter Versus Surgical Closure, a Pilot Cardiac magnetic Resonance Study

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Congenital Heart Disease 2023年第6期18卷 679-691页

作者： Amr mansour Noha m.Gamal Alaa m.Nady Amr Ibraheem Dalia m.salah Khaled m.el-maghraby Cardiology Department Congenital and Structural Heart Disease UnitAin Shams University HospitalsFaculty of MedicineAin Shams UniversityCairoEgypt Cardiology Department Faculty of MedicineAssuit UniversityAssuitEgypt Cardiothoracic Surgery Department Faculty of MedicineAssuit UniversityAssuitEgypt Anesthesia Department Faculty of MedicineAssuit UniversityAssuitEgypt

Background:Closure of an atrial septal defect(ASD)reduces right-side heart volumes by abolishing shunting with simultaneous improvement of the left ventricle(LV)ﬁlling and functions due to ventricular interdependence,thereby improving ***,studies conducted on atrial volume changes after ASD closure are *** magnetic resonance(CmR)is considered as the gold standard method for measuring cardiac volume and ***:We aimed to study the effect of transcatheter and surgical closure of secundum ASD on cardiac volumes and systolic functions as well as the fate of tricuspid regurgitation(TR),using CmR ***:We prospectively enrolled 30 adult patients with isolated secundum ASD who were referred to ASD *** evaluation of cardiac chambers indexed volumes,systolic function,myocardial mass index,and tricuspid regurgitant fraction were done at before and 6 months after ***:RV volumes decreased in both groups when compared to baseline(p-value 0.001),the device group had more reduction in volumes and more improvement in RV function after closure(p-value 0.001)when compared to the surgical *** changes in the RV mass index were insigniﬁcant between both groups(p-value 0.31).Functional TR improved to the same extent in both *** ventricular end diastolic volume index(LVEDVI)and LV mass index increased sig-niﬁcantly in both groups when compared to baseline in both groups but with no difference between groups p-value 0.01),left ventricular end systolic volume index(LVESVI)changes were insigniﬁ*** systolic function improved in patients who underwent device closure only(63.53±3.85 vs.67.13±4.34,p-value 0.01).There was a signiﬁcant reduction in right atrial(RA)volumes and an insigniﬁcant decrease in left atrial(LA)volumes,with no difference between ***:Transcatheter and surgical secundum ASD closure resulted in volumetric changes in some cardiac chambers with better improvement in bi-ventricular

关键词： Atrial septal defect closure cardiac volumetric changes functional tricuspid regurgitation cardiac CmR

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Rooted Tree Optimization for Wind Turbine Optimum Control Based on Energy Storage System

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Computers, materials & Continua 2023年第2期74卷 3977-3996页

作者： Billel meghni Afaf Benamor Oussama Hachana Ahmad Taher Azar Amira Boulmaiz salah Saad el-Sayed m.el-kenawy Nashwa Ahmad Kamal Suliman mohamed Fati Naglaa K.Bahgaat Department of electrical Engineering Badji Mokhtar UniversityLSEM LaboratoryAnnaba23000Algeria Department of electrical Engineering Biskra UniversityLGEB LaboratoryBiskra07000Algeria Department of Drilling and Rig mechanics Ksadi Merbah UniversityOuargla30000Algeria College of Computer and Information Sciences Prince Sultan UniversityRiyadh11586Saudi Arabia Faculty of Computers and Artificial Intelligence Benha UniversityBenha13518Egypt Department of electronics University of Badji MokhtarLERICA LaboratoryAnnaba23000Algeria Delta Higher Institute for Engineering&Technology(DHIET) Mansoura35511Egypt Faculty of Artificial Intelligence Delta University for Science and TechnologyMansoura35712Egypt Faculty of Engineering Cairo UniversityGiza12613Egypt Department of Communications and electronics Engineering Faculty of EngineeringCanadian International College(CIC)ElShiekh ZayedEgypt

The integration of wind turbines(WTs)in variable speed drive systems belongs to the main factors causing lowstability in electrical ***,in order to avoid this issue,WTs hybridization with a storage system is a *** paper investigates WT system operating at variable *** system contains of a permanent magnet synchronous generator(PmSG)supported by a battery storage system(BSS).To enhance the quality of active and reactive power injected into the network,direct power control(DPC)scheme utilizing space-vector modulation(SVm)technique based on proportional-integral(PI)control is ***,to improve the rendition of this method(DPC-SVm-PI),the rooted tree optimization technique(RTO)algorithm-based controller parameter identification is used to achieve PI optimal *** compare the performance ofRTO-based controllers,they were implemented and tested along with some other popular controllers under different working *** obtained results have shown the supremacy of the suggested PIRTO algorithm compared to competing controllers regarding total harmonic distortion(THD),overshoot percentage,settling time,rise time,average active power value,overall efficiency,and active power steadystate error.

关键词： Rooted tree optimization(RTO)method direct power control(DPC) wind turbine(WT) proportional integral(PI) PmSG

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