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New Polymer Syntheses Part 60: A Facile Synthetic Route to Polyamides Based on Thieno[2,3-b]thiophene and Their Corrosion Inhibition Behavior

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Chinese Journal of Polymer Science 2018年第7期36卷 835-847页

作者： kamal I.Aly Amr H.Moustafa Essam k.Ahmed Hany M.Abd El-lateef mohamed Gamal mohamed sahar M.mohamed Polymer Research Lab Chemistry Department Faculty of Science Assiut University Chemistry Department Faculty of Science Sohag University Chemistry Department Faculty of Science Minia University Chemistry Department College of Science King Faisal university

Polyamides containing thieno[2,3-b]thiophene moiety were prepared via a simple polycondensation reaction of the diaminothieno[2,3-b]thiophene monomer la with different kinds of diacid chlorides （including oxalyl, adipoyl, sebacoyl, isophthaloyl, terephthaloyl, 4,4＇-azodibenzoyl, 3,3＇-azodibenzoyl, p-phenylene diacryloyl） in the presence of LiC1 and NMP as a solvent through lowtemperature solution polycondensation. The chemical structures of model compound and synthesized polyamides were confirmed by FTIR, nuclear magnetic resonance spectroscopy （including 1 H-NMR and 13 C-NMR） and elemental analysis. In addition, the thermal stability, crystallinity structure and surface morphology of synthesized polyamides were characterized via thermogravametric analysis （TGA）, wide-angle X-ray diffraction analysis （WAXD） and scanning electron microscopy （SEM）. Also, the corrosion inhibition behavior of selected examples ofpolyamides was investigated; the inhibitive effect of the investigated polymers for carbon steel in 1.0 mol＇L-1 HCI was studied using potentiodynamic polarization （PDP） and electrochemical impedance spectroscopy （EIS） methods. PDP results displayed that the polyamides containing thieno[2,3-b]thiophene moiety can be as mixed-type inhibitors. The inhibition efficiency （P, %） was found to be in the range from 67.13% to 96.01%. There is an increase in P by the synthesized polymers in comparison to the starting monomer. The adsorption of these polymers was found to obey Langmuir adsorption isotherm.

关键词： Thieno[2 3-b]thiophene Polymer synthesis Thermal properties Industrial applications Corrosion inhibition

The impact of cold atmospheric pressure plasma jet on seed germination and seedlings growth of fenugreek(Trigonella foenum-graecum)

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Plasma Science and Technology 2019年第10期21卷 61-72页

作者： sahar A FADHLALMAWLA Abdel-Aleam H mohamed Jamal Q M ALMARASHI Tahar BOUTRAA Physics Department College of ScienceTaibah UniversityAl-Madinah Al-Munawarah 42353Saudi Arabia Physics Department Faculty of ScienceBeni-Suef UniversityBeni-Suef 52511Egypt Department of Biology College of SciencesUniversity of TaibahAl-Madinah Al-Munawarah 42353 Saudi Arabia

The effects of cold atmospheric-pressure plasma jet (CAPPJ) were investigated on germination and early seedling growth of fenugreek (Trigonella foenum-graecum L) seeds. A two-electrode argon CAPPJ system with and without an additional grounded electrode [accelerating grounded (AG) electrode] was used at different exposure times. After 16 h of observation, the germination rates increased by 4 and 7 times, without and with using an AG electrode, respectively, for 1 min of plasma exposure. An increase in shoot fresh weight was observed, especially at 10 min exposure time. A high dry weight of root and shoot at 1 min-AG exposure time was observed. The root:shoot ratio was lower in plasma-treated seedlings, compared with the control plants. The study found that the O-radical emission line (777.4 nm) enhanced 5 times, due to the presence of an AG electrode, which increased the axial electric field and led to the formation of more streamers. The three stated effects (O-radicals, enhancement of the electric field and streamers) could be the cause for the stimulation of seed germination and seedling growth parameters when using the CAPPJ. The scanning electron microscope images showed the etching of the seed surface layers, which was more pronounced when an AG electrode was applied. The results of the current study indicate that the germination rates increased due to the increase of O-radical concentration and the etching of the seed surfaces.

关键词： cold plasma fenugreek (Trigonella foenum-graecum) germination growth

Effect of probiotics on pro-inflammatory cytokines and NF-κB activation in ulcerative colitis

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World Journal of Gastroenterology 2010年第33期16卷 4145-4151页

作者： sahar k Hegazy mohamed M El-Bedewy Department of Clinical Pharmacy Faculty of PharmacyTanta University Internal Medicine Faculty of MedicineTanta University

AIM:To demonstrate the therapeutic effect of probiotics in patients with ulcerative colitis(UC),and their effect on inflammatory mediators and nuclear factor(NF)κB activation in these ***:Thirty patients with mild to moderate UC were randomly classified into two groups:sulfasalazine group,who received sulfasalazine 2400 mg/d;and probiotic group,who received sulfasalazine 2400 mg/d with *** patients were investigated before and after 8 wk of treatment with probiotic(Lactobacillus delbruekii and Lactobacillus fermentum).Colonic activity of myeloperoxidase(MPO)was assayed with UV spectrophotometry,the colonic content of interleukin(IL)-6 was determined by enzyme-linked immunosorbent assay(ELISA),fecal calprotectin was determined by ELISA,and expression of NF-κB p65 and tumor necrosis factor (TNF)-αproteins in colonic tissue was identified by immunohistochemistry and reverse transcription polymerase chain reaction,***:At the start of the study,colonic mucosal injury and inflammation were demonstrated in UC patients by hematoxylin and eosin staining,and an increase in colonic MPO activity,fecal calprotectin,and expression of colonic TNF-αand NF-κB p65 *** use of probiotic for 8 wk significantly ameliorated the inflammation by decreasing the colonic concentration of IL-6,expression of TNF-αand NF-κB p65,leukocyte recruitment,as demonstrated by a decrease in colonic MPO activity,and the level of fecal calprotectin compared to sulfasalazine group and the control group(P<0.05).CONCLUSION:Oral supplementation with probiotics could be helpful in maintaining remission and preventing relapse of UC.

关键词： Ulcerative colitis Probiotics Interleukin-6 Nuclear factor-κB

Antifibrotic effect of aloe vera in viral infection-induced hepatic periportal fibrosis

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World Journal of Gastroenterology 2012年第17期18卷 2026-2034页

作者： sahar k Hegazy mohamed El-Bedewy Akira Yagi Department of Clinical Pharmacy Faculty of PharmacyTanta UniversityTanta 8130Egypt Department of Internal Medicine Faculty of MedicineTanta UniversityTanta 8130Egypt Placenta/Aloe Research Institute Japan Bio-Products Co.Ltd.1488-4Aikawa-machiKurume-shiFukuoka Bio Factory 204Fukuoka 839-0861Japan

AIM:To investigate the anti-oxidative and anti-fibrotic effects of aloe vera in patients with liver ***:Aloe vera high molecular weight fractions(AHM) were processed by patented hyper-dry system in combination of freeze-dry technique with microwave and far infrared-ray *** healthy volunteers as the control group and 40 patients were *** patients were randomly subdivided into two equal groups:the conventional group was treated with placebo(starch),and AHM group was treated with 0.15 gm/d AHM,both for 12 consecutive *** patients were investigated before and after *** activity of aspartate aminotransferase(AST),alanine aminotransferase(ALT),alkaline phosphatase(ALP),hyaluronic acid(HA),transforming growth factor-β(TGF-β) and matrixmetalloproteinase-2(MMP-2) were *** reduced glutathione(GSH) and malondialdehyde(MDA) levels in liver were assayed and the expression of hepatic α-smooth muscle actin(α-SMA) was identified by ***:At the start of the study,the hematoxylin and eosin staining revealed fibro-proliferated bile ductules,thick fibrous septa and dense inflammatory cellular infiltration in the patients before *** use of AHM for 12 wk significantly ameliorated the fibrosis,inhibited the inflammation,and resulted in minimal infiltration and minimal fibrosis compared to the conventional *** enzyme activities of the liver(ALT,AST and ALP) were attenuated after treatment in both groups,and the decrease in the AHM group was more significant as compared with the conventional *** to the AST,the MDA levels were significantly higher before treatment,and were attenuated after treatment in both *** contrast,the hepatic glutathione content in the patients were decreased significantly in the AHM group compared to the *** serum levels of the fibrosis markers(HA,TGF-β and MMP-2) were also reduced significantly after *** expression of α-SMA was m

关键词： Hepatic fine periportal fibrosis Aloe vera α-smooth muscle actin Transforming growth factor-β Hyaluronic acid

Impact of educational interventions on mothers’ awareness and communication with their attention-deficit hyperactivity disorder children

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Journal of Integrative Nursing 2024年第4期6卷 187-195页

作者： Wafaa Hassan Hassnan ALSERATY sahar mohamed ABDULLHAMEED Atallah ALENEZI Dawadmi Nursing College Shaqra UniversityDawadmiSaudi Arabia Faculty of Nursing Tanta UniversityTantaEgypt Faculty of Nursing Minia UniversityMiniaEgypt College of Nursing Imam Mohamed Ibn Saud Islamic UniversityRiyadhSaudi Arabia

Objective:The objectives of this study are to evaluate the effects of the educational intervention on mothers’knowledge,awareness,and communication difficulties experienced with their children and mothers’capacity to successfully interact with their affected child before and after the *** and Methods:A quasi-experimental research design was used.A total of 30 mothers and their children complaining of attention-deficit hyperactivity disorder from four Dawadmi primary schools were *** were collected through a self-developed questionnaire from September 2023 to January 2024 after study acceptance by Shaqra University’s scientific *** prepared according to subjects’needs and current scientific base and demonstrated in 10 sessions in ***:Regarding mothers’age,more than one-fourth of them(26.7%)ranged from 31 to 35 year old,and about a third(36.7%)had secondary *** mother’s job,about 76.7%do not work,and the majority of affected children(66.6%)were male,there were significant improvements in mothers’knowledge pre-and postintervention also a significant improvement in mothers’awareness about symptoms of poor attention,hyperactivity,and impulsivity pre-and postintervention was *** differences were found before and after the intervention regarding the impact of the intervention in decreasing mothers’***:The study hypothesis was accepted,and the intervention improved mothers;knowledge,awareness,and communication *** intervention should be conducted and followed up for a long period of time to manage all mother’s and children’s daily challenges,improve children’s daily activities,and stabilize effective communication patterns between children and their family members.

关键词： Attention-deficit hyperactivity disorder awareness communication educational interventions

Towards hepatitis C virus elimination:Egyptian experience,achievements and limitations

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World Journal of Gastroenterology 2018年第38期24卷 4330-4340页

作者： Dalia Omran mohamed Alboraie Rania A Zayed mohamed-Naguib Wifi Mervat Naguib mohamed Eltabbakh mohamed Abdellah Ahmed Fouad Sherief sahar Maklad Heba Hamdy Eldemellawy Omar khalid Saad Doaa mohamed khamiss mohamed El kassas Department of Endemic Medicine and Hepatology Faculty of MedicineCairo UniversityCairo 11651Egypt Department of Endemic Medicine Faculty of MedicineHelwan UniversityCairo 11599Egypt Department of Internal Medicine Al-Azhar UniversityCairo 11651Egypt Department of Clinical and Chemical Pathology Faculty of MedicineCairo UniversityCairo 11651Egypt Department of Internal Medicine Faculty of MedicineCairo UniversityCairo 11599Egypt Department of Tropical Medicine Faculty of MedicineAin Shams UniversityCairo 11566Egypt National Hepatology and Tropical Medicine Research Institute Cairo 11599Egypt Department of Internal Medicine Faculty of MedicineBeni-Suef UniversityBeni-Suef 62511Egypt Faculty of Medicine Ain Shams UniversityCairo 11566Egypt Department of Clinical and Chemical Pathology El-monera hospitalMinistry of HealthCairo 11562Egypt

Worldwide, more than one million people die each year from hepatitis C virus(HCV) related diseases, and over 300 million people are chronically infected with hepatitis B or C. Egypt used to be on the top of the countries with heavy HCV burden. Some countries are making advances in elimination of HCV, yet multiple factors preventing progress; remain for the majority. These factors include lack of global funding sources for treatment, late diagnosis, poor data, and inadequate screening. Treatment of HCV in Egypt has become one of the top national priorities since 2007. Egypt started a national treatment program intending to provide cure for Egyptian HCV-infected patients. Mass HCV treatment program had started using Pegylated interferon and ribavirin between 2007 and 2014. Yet, with the development of highly-effective direct acting antivirals(DAAs) for HCV, elimination of viral hepatitis has become a real possibility. The Egyptian National Committee for the Control of Viral Hepatitis did its best to provide Egyptian HCV patients with DAAs. Egypt adopted a strategy that represents a model of care that could help other countries with high HCV prevalence rate in their battle against HCV. This review covers the effects of HCV management in Egyptian real life settings and the outcome of different treatment protocols. Also, it deals with the current and future strategies for HCV prevention and screening as well as the challenges facing HCV elimination and the prospect of future eradication of HCV.

关键词： Hepatitis C virus Egypt Direct acting antivirals screening elimination Limitations

Fixed Point Theorem of{a, b, c}Contraction and Nonexpansive Type Mappings in Weakly Cauchy Normed Spaces

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Analysis in Theory and Applications 2013年第3期29卷 280-288页

作者： sahar mohamed Ali Department of Mathematics Faculty of ScienceAin Shams UniversityCairoEgypt

Let C be a closed convex weakly Cauchy subset of a normed space X. Then we define a new {a,b,c} type nonexpansive and {a,b,c} type contraction mapping T from C into C. These types of mappings will be denoted respectively by {a,b,c}-ntype and {a,b,c}-ctype. We proved the following： 1. If T is {a,b,c}-ntype mapping, then inf{ ｜｜ T（x）-x｜｜：x C C} =0, accordingly T has a unique fixed point. Moreover, any sequence {Xn}n∈NN in C with limn→∞｜｜T（xn） - Xn｜｜ = 0 has a subsequence strongly convergent to the unique fixed point of T. 2. If T is {a,b,c}-ctype mapping, then T has a unique fixed point. Moreover, for any x∈C the sequence of iterates {Tn （x）}n∈N has subsequence strongly convergent to the unique fixed point of T. This paper extends and generalizes some of the results given in [2,4, 7] and [13].

关键词： Fixed point generalized type of contaction and nonexpansive mappings normed space.

More on Fixed Point Theorem of{a,b,c}-Generalized Nonexpansive Mappings in Normed Spaces

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Analysis in Theory and Applications 2013年第1期29卷 1-11页

作者： sahar mohamed Ali Department of Mathematics Faculty of ScienceAin Shams University Egypt&General Courses Department Riyadh Philanthropic Society for SciencePrince Sultan UniversityCollege for Women

Let X be a weakly Cauchy normed space in which the parallelogram law holds,C be a bounded closed convex subset of X with one contracting point and T be an{a,b,c}-generalized-nonexpansive mapping from C into *** prove that the infimum of the set{‖x-T(x)‖}on C is zero,study some facts concerning the{a,b,c}-generalized-nonexpansive mapping and prove that the asymptotic center of any bounded sequence with respect to C is *** on the fact that the{a,b,0}-generalized-nonexpansive mapping from C into C has fixed points,accord-ingly,another version of the Browder's strong convergence theorem for mappings is given.

关键词： Fixed point theorem {a b c}-generalized-nonexp ansive mapping asymptotic center,Browder's strong convergence Theorem.

Salivary C-reactive protein and mean platelet volume as possible diagnostic markers for late-onset neonatal pneumonia

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World Journal of Clinical Pediatrics 2024年第1期13卷 41-51页

作者： Wafaa Ahmed Metwali Abdelrahman mohamed Elmashad sahar Mohey Eldin Hazzaa Mohammed Al-Beltagi mohamed Basiony Hamza Department of Pediatric Faculty of MedicineTanta UniversityTanta 31511AlgahrbiaEgypt Department of Clinical Pathology Faculty of MedicineTanta UniversityTanta 31511AlgahrbiaEgypt Department of Pediatric University Medical CenterDr.Suliaman Al Habib Medical GroupManama 26671ManamaBahrain Department of Pediatric University Medical CenterKing Abdulla Medical CityArabian Gulf UniversityManama 26671ManamaBahrain

BACkGROUND Neonatal sepsis,a formidable threat to newborns,is a leading cause of neonatal mortality,with late-onset sepsis manifesting after 72 hours post-birth being particularly ***,a prevalent sepsis presentation,poses a significant risk,especially during the neonatal phase when lung defenses are *** diagnosis of pneumonia is imperative for timely and effective ***,a minimally invasive diagnostic medium,holds great promise for evaluating infections,especially in *** To investigate the potential of serum C-reactive protein(CRP),salivary CRP(sCRP),and mean platelet volume(MPV)as diagnostic markers for late-onset neonatal pneumonia(LONP).METHODS Eighty full-term neonates were systematically examined,considering anthropometric measurements,clinical manifestations,radiology findings,and essential biomarkers,including serum CRP,sCRP,and *** The study reveals noteworthy distinctions in serum CRP levels,MPV,and the serum CRP/MPV ratio between neonates with LONP and healthy *** exhibited a robust discriminatory ability[area under the curve(AUC)=0.87]with high sensitivity and specificity at a cutoff value of>*** between serum CRP,sCRP,and MPV were also ***,sCRP demonstrated excellent predictive value for serum CRP levels(AUC=0.89),underscoring its potential as a diagnostic *** This study underscores the diagnostic promise of salivary and serum biomarkers,specifically MPV and CRP,in identifying and predicting LONP among *** findings advocate for further research to validate their clinical utility in larger neonatal cohorts.

关键词： Neonatal sepsis Late-onset pneumonia Salivary C-reactive protein Mean platelet volume Diagnostic markers Newborn infections