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Tailoring the texture and mechanical properties of 3%Y_(2)O_(3)p/ZGK200 composites fabricated by unidirectional and cross rolling followed by annealing

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Journal of Magnesium and Alloys 2024年第4期12卷 1479-1495页

作者： Xihai Li Hong Yan Zhiwei Shan rongshi Chen Shi-changxu Innovation Center for Advanced Materials Institute of Metal ResearchChinese Academy of Sciences72 Wenhua RoadShenyang 110016China School of Materials Science and Engineering University of Science and Technology of China72 Wenhua RoadShenyang 110016China School of Materials Science and Engineering Shandong University of Science and TechnologyQingdaoShandong 266590China Center for Advancing Materials Performance from the Nanoscale(CAMP-Nano)and Hysitron Applied Research Center in China(HARCC) State Key Laboratory for Mechanical Behavior of MaterialsXi’an Jiaotong UniversityXi’an 710049China

3%Y_(2)O_(3)p/ZGK200 composites were subjected to unidirectional rolling(UR)and cross rolling(CR)at 400℃and 350℃followed by annealing at 300℃for 1.*** microstructure,texture and mechanical properties of rolled and annealed composites were systematically *** rolled composites exhibited a heterogeneous microstructure,consisting of deformed grains elongated along rolling direction(RD)and Y_(2)O_(3)particles bands distributed along *** annealing,static recrystallization(SRX)occurred and most deformed grains transformed into equiaxed grains.A non-basal texture with two strong T-texture components was obtained after UR while a non-basal elliptical/circle texture with circle multi-peaks was obtained after CR,indicating that rolling path had great influences on texture of the *** annealing process,R-texture component disappeared or weakened,as results,a non-basal texture with double peaks tilting from normal direction(ND)to transverse direction(TD)and a more random non-basal texture with circle multi-peaks were obtained for UR and CR composites,*** yield strength of rolled composites after UR showed obvious anisotropy along RD and TD while a low anisotropic yield strength was obtained after *** Y_(2)O_(3)particles broke during *** fracture of the composites was attributed to the existence of Y_(2)O_(3)clusters and interfacial debonding between particles and matrix during tension,as a result,the ductility was not as superior as matrix alloy.

关键词： Magnesium matrix composites Unidirectional rolling Cross rolling Texture Mechanical properties

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Low-cycle fatigue behavior of solutionized and aged WE43 magnesium alloys at room temperature

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Journal of Magnesium and Alloys 2024年第6期12卷 2284-2297页

作者： Yong Cai Jianxiong Wei Hong Yan Yipeng Chen rongshi Chen School of Materials Science and Engineering University of Science and Technology of China72 Wenhua RoadShenyang 110016China Shi-changxu Innovation Center for Advanced Materials Institute of Metal ResearchChinese Academy of Sciences72 Wenhua RoadShenyang 110016China School of Materials Science and Engineering Shandong University of Science and TechnologyQingdaoShandong 266590China

The low-cycle fatigue behavior of solutionized(T4)and aged(T6)WE43 magnesium alloys was studied at room *** total strain amplitudes(△ε_(t)/2)were 0.4%,0.5%,0.6%,0.7%and 1.0%.Detailed microstructure evolution was characterized by scanning electron microscope(SEM),electron backscattered diffraction(EBSD)and transmission electron microscopy(TEM).The results showed that plastic strain amplitude decreased with the increasing cycle number in T4 alloy,which is due to the dense persistent slip bands(PSBs)and dynamic precipitates hinderingdislocation *** contrast,the plastic strain amplitude increases gradually in T6 alloy,which is attributed to the enhanced activation of pyramidal *** low-cycle fatigue life of T6 alloy with larger fatigue ductility coefficient is longer than that of T4 *** Coffin-Manson model can accurately predict the fatigue life of T4 and T6 alloys compared to Jahed-Varvani(JV)energy *** T4 alloy,the fatigue damage mechanism was dominated by basal *** T6 alloy,the enhanced pyramidal slip plays an important role to accommodate plastic deformation.

关键词： Low-cycle fatigue WE43 alloy Cyclic hardening/softening JV model Dislocation

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Effect of annealing treatment on the microstructure and mechanical properties of warm-rolled Mg-Zn-Gd-Ca-Mn alloys

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International Journal of Minerals,Metallurgy and Materials 2024年第10期31卷 2208-2220页

作者： Yifan Song Xihai Li Jinliang Xu Kai Zhang Yaozong Mao Hong Yan Huiping Li rongshi Chen School of Materials Science and Engineering Shandong University of Science and TechnologyQingdao 266590China Shi-changxu Innovation Center for Advanced Materials Institute of Metal ResearchChinese Academy of SciencesShenyang 110016China Shandong Key Laboratory of Advanced Aluminium Materials and Technology Binzhou Institute of TechnologyBinzhou 256606China

The basal texture of traditional magnesium alloy AZ31.is easy to form and exhibits poor plasticity at room *** address these problems,a multi-micro-alloyed high-plasticity Mg-1.8Zn-0.8Gd-0.1.a-0.2Mn(wt%)alloy was developed using the unique role of rare earth and Ca solute *** addition,the influence of the annealing process on the grain size,second phase,texture,and mechanical properties of the warm-rolled sheet at room temperature was analyzed with the goal of developing high-plasticity mag-nesium alloy sheets and obtaining optimal thermal-mechanical treatment *** results show that the annealing temperature has a significant effect on the microstructure and properties due to the low alloying content:there are small amounts of larger-sized block and long string phases along the rolling direction(RD),as well as several spherical and rodlike particle phases inside the *** increas-ing annealing temperature,the grain size decreases and then increases,and the morphology,number,and size of the second phase also change *** particle phase within the grains vanishes at 450℃,and the grain size increases *** the full recrystal-lization stage at 300-350℃,the optimum strength-plasticity comprehensive mechanical properties are presented,with yield strengths of 1.2.1.and 1.6.9 MPa,tensile strengths of 271.1.and 275.8 MPa in the RD and transverse direction(TD),and elongation values of 27.4%and 32.3%,***,there are still some larger-sized phases in the alloy that influence its mechanical properties,which offers room for improvement.

关键词： Mg-Zn-Gd-Ca-Mn alloy annealing treatment microstructure texture dynamic recrystallization mechanical properties

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脉冲激光辅助激光增材制造研究进展

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表面技术 2024年第13期53卷 1-12,32页

作者：郑敏黄婷肖荣诗北京工业大学智能光子制造研究中心北京100124

针对辅助脉冲激光作用在固相区的情况,分别论述了非同步式表面、非同步式层间以及同步式脉冲激光辅助激光增材制造的工艺特点,分析了增材制造构件组织、成形缺陷以及应力分布的调控机理,并系统对比了非同步式和同步式脉冲激光辅助激光... 详细信息

针对辅助脉冲激光作用在固相区的情况,分别论述了非同步式表面、非同步式层间以及同步式脉冲激光辅助激光增材制造的工艺特点,分析了增材制造构件组织、成形缺陷以及应力分布的调控机理,并系统对比了非同步式和同步式脉冲激光辅助激光增材制造的调控效果,总结了同步式脉冲激光辅助激光增材制造的工艺优势。针对辅助脉冲激光作用在熔池区的情况,研究了脉冲激光功率密度、频率对熔池热动力学行为的作用机理(Marangoni对流、超声波搅拌空化、冲击波效应等),进而明晰了辅助脉冲激光冲击熔池对增材制造构件组织、成形缺陷的影响机理。最后,对脉冲激光辅助激光增材制造技术的研究进展进行了总结,并对下一阶段的发展方向进行了展望。

关键词：激光增材制造脉冲激光冲击组织成形缺陷残余应力

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金属材料激光微焊接研究进展(特邀)

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中国激光 2024年第4期51卷 60-76页

作者：杜伟哲黄旭霆郑敏肖荣诗黄婷北京工业大学材料与制造学部智能光子制造研究中心北京100124

设备器件精密化、微型化是工业发展的重要趋势。在航空航天、动力电池、消费电子、生物医疗等应用领域中,零部件的日益微型化对微加工工艺提出了更高的要求。金属材料微焊接是微加工领域的重要需求之一,而激光具有能量密度高、热输入精... 详细信息

设备器件精密化、微型化是工业发展的重要趋势。在航空航天、动力电池、消费电子、生物医疗等应用领域中,零部件的日益微型化对微加工工艺提出了更高的要求。金属材料微焊接是微加工领域的重要需求之一,而激光具有能量密度高、热输入精确可控、焊接变形小等特点,是金属材料微焊接的重要技术手段。对金属材料激光微焊接技术展开了探讨,明确了其内涵,阐明了微尺度效应的影响,并总结了激光微焊接常见的缺陷及其质量控制方法,介绍了同种金属材料和异种金属材料激光微焊接的重要应用前景。最后,指出了金属材料激光微焊接技术存在的问题,并展望了未来的发展方向。

关键词：激光技术金属箔材激光微焊接尺度效应工艺参数应用

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等通道转角挤压对Mg-1.d、Mg-2Zn二元合金组织及力学性能的影响

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稀有金属材料与工程 2024年第6期53卷 1735-1740页

作者：许金良宋宜帆丁睿智闫宏陈荣石山东科技大学材料科学与工程学院山东青岛266400 中国科学院金属研究所师昌绪先进材料创新中心辽宁沈阳110016

使用OM、EBSD等手段研究了等通道转角挤压(ECAE)对Mg-1.d、Mg-2Zn2种二元合金组织和力学性能的影响。结果表明,在相同挤压条件下,Mg-2Zn合金发生完全再结晶,晶粒长大粗化,且强度塑性不随着挤压道次变化;Mg-1.d合金则只发生了部分动态再... 详细信息

使用OM、EBSD等手段研究了等通道转角挤压(ECAE)对Mg-1.d、Mg-2Zn2种二元合金组织和力学性能的影响。结果表明,在相同挤压条件下,Mg-2Zn合金发生完全再结晶,晶粒长大粗化,且强度塑性不随着挤压道次变化;Mg-1.d合金则只发生了部分动态再结晶,组织为细小的动态再结晶晶粒和变形晶粒,伴随挤压道次的增加,再结晶程度提升,合金的抗拉强度与塑性增加了1.。这与溶质原子Gd比Zn更能抑制再结晶和晶粒长大有关。Mg-1.d合金的再结晶晶粒的取向分散,而未再结晶的晶粒c轴取向由ED向TD偏转45°,这与宏观织构的检测相互印证,晶粒内部产生大量的小角度晶界,小角度晶界两侧发生围绕c轴的转动。

关键词：等通道转角挤压(ECAE) Mg-1.d合金 Mg-2Zn合金再结晶织构力学性能

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GH31.8薄板搭接环芯组合光纤激光焊接焊缝形貌调控

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电加工与模具 2024年第3期 37-42页

作者：周嘉树肖荣诗北京工业大学物理与光电工程学院智能光子制造研究中心北京100124

航空发动机因内流道结构的入口端和出口端不同,其焊接问题是一大难题,如何在实际焊接中做到焊缝熔宽连续可控已成为研究热点。针对GH31.8高温合金开展环芯组合光纤进行激光搭接焊研究,通过纯中心激光焊接得到了焊缝深度为1.5 mm的工艺参... 详细信息

航空发动机因内流道结构的入口端和出口端不同,其焊接问题是一大难题,如何在实际焊接中做到焊缝熔宽连续可控已成为研究热点。针对GH31.8高温合金开展环芯组合光纤进行激光搭接焊研究,通过纯中心激光焊接得到了焊缝深度为1.5 mm的工艺参数,在此基础上通过环芯组合焊接得到了实际熔深为1.51.1.81.mm、熔宽为0.25~0.75 mm的焊缝,对环芯组合光纤激光器的中心光束和环形光束传播规律及焊缝形貌调控原因进行分析。分析发现,环形光束的加入有利于降低激光束照射到材料表面的温度梯度,从而影响焊缝成形,通过环芯组合的激光焊接可得熔深合理、熔宽连续调控的GH31.8薄板搭接焊缝。

关键词： GH31.8薄板环芯组合光纤焊缝熔宽

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Cu箔集流体飞秒激光深刻蚀织构化及其对锂离子电池性能的影响

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表面技术 2024年第1期53卷 115-122页

作者：王京博曹利李松原肖荣诗黄婷北京工业大学材料与制造学部北京100124

目的使用飞秒激光在Cu箔表面深刻蚀织构化,制备微纳沟槽结构,提高锂离子电池Si电极循环稳定性。方法系统研究激光能量密度、单位点有效脉冲数对厚度为9μm的Cu箔的表面形貌和微纳结构的影响规律,根据结果设计不同沟槽密度和沟槽深度... 详细信息

目的使用飞秒激光在Cu箔表面深刻蚀织构化,制备微纳沟槽结构,提高锂离子电池Si电极循环稳定性。方法系统研究激光能量密度、单位点有效脉冲数对厚度为9μm的Cu箔的表面形貌和微纳结构的影响规律,根据结果设计不同沟槽密度和沟槽深度的Cu箔,并组装成Si电极锂离子半电池,通过循环测试及循环后电极形貌揭示其稳定性提升的内在机理。结果最佳的激光能量密度为3.1. J/cm^(2),此时改变单位点有效脉冲数和扫描间距可有效控制刻蚀沟槽的密度和深度。Si电极的循环稳定性随着Cu箔表面沟槽密度和沟槽深度的增加而逐渐提升,当沟槽密度为75%、沟槽深度为6μm时,循环300圈后剩余的容量高达91. mA·h/g,保持率为89%,电极形貌相对最完整、稳定。结论刻蚀表面纳米结构增加了电极层与集流体之间的黏结强度;微米沟槽结构进一步保护了电极层,缓解了体积膨胀效应。采用Cu箔集流体深刻蚀显著改善了Si电极的剥离和开裂现象,实现了其电化学性能的提升。

关键词：绿光飞秒激光激光刻蚀 Cu箔集流体 Si电极循环稳定性

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Tailoring the Texture and Mechanical Anisotropy of Multi-cross Rolled Mg-Zn-Gd Alloy by Annealing

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Acta Metallurgica Sinica(English Letters) 2023年第2期36卷 251-265页

作者： Xihai Li Hong Yan rongshi Chen School of Materials Science and Engineering University of Science and Technology of ChinaShenyang110016China Shi-Changxu Innovation Center for Advanced Materials Institute of Metal ResearchChinese Academy of SciencesShenyang110016China School of Materials Science and Engineering Shandong University of Science and TechnologyQingdao266590China

The unidirectional rolled Mg-Zn-Gd sheet usually exhibited non-basal texture with two peaks whose tilting angle were about 42°from normal direction to transverse direction(TD),which would cause the mechanical *** this study,multi-cross rolling followed by annealing was used to tailor the texture and mechanical anisotropy for Mg-Zn-Gd *** increasing annealing temperature,the rolled basal texture with two peaks gradually transformed into the circle texture with *** order to figure out different texture components evolution during annealing,the basal texture,R-texture and T-texture component were defined and *** results showed that the change of R-texture and T-texture component was asynchronous with increasing annealing temperature from 250 to 400℃.The tilting angle of R-texture component increased slightly,while the tilting angle of T-texture component increased obviously,and this phenomenon was attributed to the preferential nucleation at grain nucleation stage rather than preferential grain *** yield strength along TD was more sensitive to annealing temperature compared with that along rolling direction(RD),resulting in different descending slopes and yield strength anisotropy with increasing annealing *** at 300℃was the best annealing temperature due to low yield strength anisotropy,moderate strength and good elongation among these annealing *** Schmid factor for basal slip indicated that the activity of basal slip along RD increased slightly,while that along TD increased obviously with increasing annealing temperature from 250 to 400℃,which should be caused by the asynchronous change of R-texture component and T-texture component,consequently resulting in the transformation from isotropic yield strength to anisotropic yield strength.

关键词： Mg-Zn-Gd alloy Annealing Texture Yield strength Electron back-scattering diffraction(EBSD)

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Superplasticity of Mg-5.8Zn-1.-Zr alloy sheet fabricated by combination of extrusion and hot-rolling processes

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Science China(Technological Sciences) 2009年第1期52卷 166-171页

作者： YAN Hong CHEN rongshi HAN EnHou State Key Laboratory for Corrosion and Protections Institute of Metal ResearchChinese Academy of SciencesShenyang 110016China Graduate University of Chinese Academy of Sciences Beijing 100049China

Superplastic behaviors of quasicrystal phase containing Mg-5.8Zn-1.-0.48Zr alloy sheets fabricated by combination of extrusion and hot-rolling processes have been investigated at temperature ranging from 623 to 753 K and at the strain rates ranging from 1.-4 to 1.-2 s-1.by uniaxial tensile tests. An excellent superplasticity with the maximum elongation to failure of 1.20% was obtained at 753 K and the strain rate of 1.04×1.-3 s-1.and its strain rate sensitivity, m, is as high as up to 0.75. The microstructure was stable during superplastic deformation due to the uniformly distributed fine quasicrystal particles. In addition, micro-cavities and their coalescences were observed in the superplastic deformation of the ZW61.magnesium alloy. Grain boundary sliding (GBS) was considered to be the main deformation mechanism during the superplastic deformation. Dislocation creep controlled by atom diffusion through grain boundaries or interior grains is suggested mainly to accommodate the GBS in super-plastic deformation.

关键词： magnesium alloy quasicrystal microvoid superplasticity

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