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Evaluation of Mineral Elements Content of Senegal Fruits

Journal of Minerals and Materials Characterization and Engineering 2022年第2期10卷 163-173页

作者： rokhaya Sylla gueye Jérôme Ledauphin Fabienne Baraud Lydia Leleyter Mélanie Lemoine rokhaya gueye Adama Diedhiou Mamadou Balde Nango Gaye Matar Seck Djibril Fall Alassane Wele Laboratoire de Chimie Physique Minérale Organique et Thérapeutique Université Cheikh Anta Diop (UCAD) Dakar Sénégal Unité de Recherche “Aliments Bioprocédés Toxicologie Environnement” Université de Caen Normandie Caen France Laboratoire de Chimie Analytique et Bromatologie (UCAD) Dakar Sénégal

This study determined mineral value and antioxidant activity of Senegal fruits for contributing to improving healthy diet and preventing some chronic diseases. Mineral element contents of Dialium guineense, Landolphia heudelotti, Mangifera indica, Cyperus esculentus and Saba senegalensis, which are widely available and consumed, were studied. The results by ICP-OES spectrophotometry after acid mineralization showed highest levels of (per 100 g fruits), calcium (158 mg), potassium (1018 mg), magnesium (532 mg), zinc (26 mg) with juice of Landolphia heudelotti fruit pulp. Mangifera indica pulp is richer in sodium (89 mg), phosphorus (556 mg), sulphur (384 mg) and silicon (110 mg). Dialium senegalensis pulp is richer in iron (23 mg) and manganese (19 mg). Lyophilized Cyperus esculentus rhizomes analyzed by atomic absorption spectrophotometry gave highest concentrations of (per 100 g fruits), calcium (2550 mg), potassium (11,843 mg) and magnesium (7669 mg) but sodium content (22 mg) is lower. In vitro antioxidant activity evaluation with the DPPH radical showed for 10 mg/ml concentration, highest inhibition percentage for Saba senegalensis 4.03%, followed by Landolphia heudelotti and Dialium guineense, which were significantly similar 2.29% and 2.20% respectively, Mangifera indica 1.7% and finally Cyperus esculentus 0.5%, but much lower compared to the ascorbic acid equal to 96.32% used as a reference.

关键词： Fruits Senegal Mineral Elements Antioxidant Activity

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Physico-Chemical and Mineralogical Characterizations of Tchiky Clays (Thies, Senegal) for Pharmaceutical Uses

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Journal of Minerals and Materials Characterization and Engineering 2023年第2期11卷 36-48页

作者： rokhaya Sylla gueye Nango Gaye Ousmane Ka Mamadou Baldé Adama Diedhiou Ngoné Diouf Samba F. Ndoye Idrissa Ndoye Yoro Tine rokhaya gueye Mouhamadou B. Diop Matar Seck Djibril Fall Alassane Welé Laboratory of Physical Mineral Organic and Therapeutic Chemistry Cheikh Anta Diop University (UCAD) Dakar Senegal Laboratory of Analytical Chemistry and Bromatology UCAD Dakar Senegal Laboratory of Geomaterials Institute of Earth Sciences UCAD Dakar Senegal

Our study focused on the valuation of Tchiky clays. This work aims to evaluate its properties to explore possible uses in pharmacy. Physico-chemical and mineralogical characterizations were carried out, as well as pharmacopoeial tests and an evaluation of the antioxidant activity. Thus, chemical analysis by X-ray fluorescence spectrometry gave silicon (55.65%), iron (15.73%), aluminum (13.53%), potassium (6.05%), titanium (3.98%), magnesium (2.10%), and calcium (0.82%). X-ray diffraction showed the presence of kaolinite, quartz and illite. This study also revealed that the sample studied was essentially a plastic clay of hard consistency, with average flowability. The evaluation of the antioxidant activity gave a percentage inhibition of 62.97% for a concentration of 7.5 g/l with an IC50 of 5.5 g/l. These results should allow use as an excipient in pharmacy, particularly in liquid, semi-liquid and pasty formulations.

关键词： Clays Tchiky Minerals Pharmacopoeia Antioxidant Activity

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Assessment of Poultry Feed Contamination Level by Aflatoxin B1: Quantification by Two Chromatographic Analysis Methods

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Food and Nutrition Sciences 2022年第11期13卷 950-961页

作者： rokhaya gueye Viviane Chatchueng Sandefo Babacar Beye Elhadji Ousmane Faye Amadou Diop Serigne Omar Sarr Bara Ndiaye Yérim Mbagnick Diop Laboratoire de Chimie Analytique et Bromatologie Faculté de Médecine de Pharmacie et d’Odontologie-Stomatologie Université Cheikh Anta DIOP Dakar Sénégal Laboratoire de Mycotoxines Institut de Technologie Alimentaire Route des Pères Maristes Dakar Sénégal

Aflatoxin B1 is a mycotoxin that can contaminate a wide feedstuffs variety. Ingestion of contaminated feed by poultry can lead to impaired health and zootechnical performances but also a human diet safety problem related to residues presence in animal origin products. Aflatoxin B1 contamination of poultry feed samples marketed in Dakar city and in peri-urban areas (Gorom, Sangalkam) was studied. A total of 15 samples were collected from Dakar city markets as well as from poultry farms in Gorom and Sangalkam areas. Aflatoxin B1 quantification was performed by high performance liquid chromatography and thin-layer chromatography. HPLC results showed that all samples were contaminated with levels ranging from 0.15 to 22 ppb, 0.099 to 2.05 ppb and 0.099 to 4.95 ppb respectively for Gorom, Sangalkam and Dakar. Only the finishing feed from Gorom had an aflatoxin B1 level above the maximum limit set by regulations. TLC is a suitable method for aflatoxins detection. However, it was associated with overestimation for aflatoxin B1 quantification. Results suggest that poultry feed represents a real source of human diet contamination. In addition, HPLC remains the most reliable quantification technique for quality control.

关键词： Poultry Feed Aflatoxin High Performance Liquid Chromatography Thin-Layer Chromatography Dakar

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Review of Research on Li-Ion Batteries Waste Management

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Open Journal of Inorganic Chemistry 2022年第2期12卷 19-38页

作者： rokhaya Sylla gueye Nango Gaye Mamadou Baldé Adama Diedhiou Ngoné Diouf Seck Gorgui Awa Idrissa Ndoye Yoro Tine Matar Seck Djibril Fall Alassane Wele Mahy Diaw Laboratory of Physical Inorganic Organic and Therapeutic Chemistry Faculty of Medicine Pharmacy and Odontology Cheikh Anta Diop Dakar University (UCAD) Dakar Senegal Gaston Berger Saint-Louis University (UGB) Saint-Louis Senegal Alioune Diop Bambey University (UADB) Bambey Senegal

Li-ion batteries (Libs) are a mature technology widely used for energy storage in various electronic devices. Nowadays, this technology has become a leading candidate for the portable electronics market and for electric vehicles due to its good performance. As a result, the demand for Libs containing critical metals, rare earth elements and precious metals is increasing day by day with the accelerated upgrades of consumer electronics, which promotes the supply risk of many mining resources. In addition, the problems associated with the production of end-of-life Lib are increasing on a global scale. Used Libs are e-waste containing significant levels of critical raw materials (such as Co, Li, Mn and Ni) along with harmful substances. Without proper management of Lib waste, these precious metals and toxic substances may end up in nature and cause environmental and public health problems. In order to preserve nature, ensure sustainable resource management and stimulate the circular economy, it has become crucial to properly manage and recycle end-of-life Li-ion batteries. By the way, conventional methods focusing on pyrometallurgical treatments combined with hydrometallurgical treatment are widely studied to recover design metals from Libs waste. It is in this context that we have conducted this bibliographic synthesis, focusing on the efficiency of the solvents employed and their competitiveness for a more environmentally friendly economic management. In this manuscript, recent leaching, solvent extraction, electrodeposition and precipitation strategies to recover precious metals from end-of-life Li-ion battery designs are reviewed and the evolution of these processes is discussed.

关键词： Libs Waste Leaching Extraction Rate Affinity Partition Coefficient

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Antioxidant and antiglycation properties of two mango(Mangifera indica L.) cultivars from Senegal

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Asian Pacific Journal of Tropical Biomedicine 2018年第3期8卷 137-141页

作者： Samba Fama Ndoye Didier Fraisse Blandine Akendengue Mbaye Diaw Dioum rokhaya Sylla gueye Cheikh Sall Insa Seck Catherine Felgines Matar Seck Francois Senejoux Laboratory of Organic and Therapeutic Chemistry Faculty of Medicine Pharmacy and Odontology Cheikh Anta Diop University Universite Clermont Auvergne INRAUNH Department of Pharmacology and Toxicology Faculty of Medicine and Health Sciences (USS) Laboratory of Chemistry Training and Research Unit of Health Thies University

Objective: To evaluate the total phenolic contents, antioxidant and antiglycation activities of leaves, barks, roots and kernels from two cultivars of Mangifera indica(Anacardiaceae). Methods: Total phenolic contents were determined by using Folin-Ciocalteu's method. The antioxidant activities were assessed by three different protocols including DPPH, oxygen radical absorbance capacity and iron(Ⅱ) chelation assays. In addition, in vitro bovine serum albumin/D-ribose assay was chosen to evaluate the antiglycation properties of the extracts. Results: All the investigated extracts were found to contain high level of total phenols as well as potent antioxidant activities. Kernel extracts showed the highest total phenol contents and DPPH radical scavenging activities whereas higher oxygen radical absorbance capacity values were observed for leave, root and bark extracts. Besides, extracts from leaves, roots and barks from both cultivars exhibited potent inhibitory effects against the formation of advanced glycation end products, with IC_(50) values lower than the standard positive control aminoguanidine. Conclusions: The potent antiglycation and antioxidative activities of these two Mangifera indica cultivars suggest a possible role in targeting aging, diabetic complications and oxidative stress related diseases.

关键词： Mangifera indica Cultivars Polyphenols Antioxidant Antiglycation

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Effect of Water Content and Grains Size Distribution on the Characteristic Resilient Young’s Modulus (<i>E<sub>c</sub></i>) Obtained Using Anisotropic Boyce Model on Gravelly Lateritic Soils from Tropical Africa (Burkina Faso and Senegal)

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Open Journal of Civil Engineering 2021年第1期11卷 134-152页

作者： Bibalo Ida Josiane Ki Makhaly Ba rokhaya gueye Pierre Hornych Ali Sana Laboratoire de Mécanique et Modélisation (L2M) UFR Sciences de l’Ingénieur Université de Thiès Thiès Sénégal

This research was carried out to determine the rheological parameters of lateritic soils in order to contribute to the improvement of the technical documents used for pavement design in tropical Africa. The study is based on the loading repeated of cyclic triaxial tests (LRT) performed at University Gustave Eiffel (formerly Institut Français des Sciences et Technologies des Transports de l’Aménagement et des Réseaux (IFSTTAR)) in Nantes with the application of the European standard EN 13286-7: 2004 [1]. The tests were performed at constant confinement stress and using the stepwise method to determine the resilient axial () and radial () deformation as a function of the axial and radial stresses. Four gravel lateritic soils from different sites selected in Burkina Faso and Senegal were the subject of this research for the triaxial tests. These materials have a maximum diameter of 20 mm a

关键词： Lateritic Soil Cyclic Triaxial with Repeated Loading (LRT) Characteristic Resilient Young’s Modulus Anisotropic Boyce Model Water Content Grains Size Distribution

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Covariates of Disability-Profile Transitions in Older People Living at Home

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Journal of Biosciences and Medicines 2014年第3期2卷 25-36页

作者： Michel Raiche Rejean Hebert Marie-France Dubois N’Deye rokhaya gueye Nicole Dubuc Research Centre on Aging Sherbrooke University Geriatrics InstituteSherbrookeCanada Faculty of Medicine and Health Sciences Universitede SherbrookeSherbrookeCanada Faculty of Arts&Faculty of sciences Universitede Saint-BonifaceWinnipegCanada

The objective of this study was to explore the relationship of sociodemographic, clinical, and health-services use-related variables with transitions between disability-based profiles. In a longitudinal study of 1386 people aged 75 and over living in the community at baseline, disabilities were assessed annually for up to four years with the Functional Autonomy Measurement System (SMAF), which generates 14 Iso-SMAF profiles. These profiles are grouped into 4 disability states, which are predominant alterations in instrumental activities of daily living (IADLs), mobility, mental functions as well as severe and mixed disabilities. Continuous-time, multi-state Markov modeling was used to identify the factors associated with transitions made by older people between these states and to institutionalization and death. Greater age and receiving help for ADL were associated with four transitions, while altered cognitive functions and hospitalization were associated with three, all involving more decline or less recovery. From mild IADL profiles, men have a higher risk of transitioning to intermediate predominantly mental profiles, while women are at higher risk of transitioning to intermediate predominantly mobility profiles. Unmet needs are associated with deterioration, from mild IADL to intermediate predominantly mobility profiles. These results help understanding the complex progression of disabilities in older people.

关键词： Aged Disability Profiles Transitions Covariates Multistate Model Case-Mix Classification Longitudinal

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Validation of a Capillary Electrophoresis Method for Analyzing Chlorphenamine Maleate-Based Drugs Using the Accuracy Profile Approach

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American Journal of Analytical Chemistry 2016年第5期7卷 452-459页

作者： Serigne Omar Sarr Eddy Kevin Senan Ouendo Thierno Mouhamed Wane El Hadji Assane Diop Diop Amadou Serigne Momar Ndiaye rokhaya gueye Khadidiatou Thiam Aminata Sarr Ousmane Niass Djibril Fall Bara Ndiaye Serge Rudaz Yérim Mbagnick Diop Laboratory of Analytical Chemistry and Food Sciences Cheikh Anta Diop University Dakar Senegal National Medicines Control Laboratory Ministry of Health Dakar Senegal Laboratory of Pharmaceutical Analytical Chemistry School of Pharmacy Geneva Switzerland Laboratory of Organic and Therapeutic Chemistry Cheikh Anta Diop University Dakar Senegal

This study aimed at validating an analytical method, using the accuracy profile approach, for the assay of chlorphenamine maleate by capillary electrophoresis. The validation was done using concentrations ranging between 75% and 125% of the target concentration of 600 mg/ml. Validation standards were prepared separately in triplicate for each series. Studied validation criteria were selectivity, linearity, trueness, precision (repeatability and intermediate precision), accuracy and limits of detection and quantification. The method was selective, with recoveries ranging between 99.55% and 99.84%. The relative standard deviations of repeatability and intermediate precision were <5%. The accuracy profile confirmed the performance of the assay method between 75% and 100% of the target concentration of 600 mg/ml. The detection and quantification limits were 5 mg/l and 15 mg/l respectively. This ecological and economical method was applied to identify and quantify chlorphenamine maleate in 3 samples of chlorphenamine maleate-based drugs provided by the Senegalese National Medicines Control Laboratory. All analyzed samples were in accordance with official standards.

关键词： Analytical Validation Chlorphenamine Maleate Quality Capillary Electrophoresis CEB Senegal

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Velocity Form Calculations of Generalized Oscillator Strengths for 3s→ (3p, 4p, 5p, 6p) Dipole Transitions of Atomic Sodium in Debye Plasma

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Open Journal of Applied Sciences 2024年第6期14卷 1512-1529页

作者： Louis Gomis Clement Diatta Moustapha Sadibou Tall Ibrahima gueye Faye Rama Gomis Yande Diouf Mamadou Coulibaly Laboratoire de Physique des Plasmas et de Recherches Interdisciplinaires Departement de Physique Universite Cheikh Anta Diop Dakar Senegal

In this paper, the generalized oscillator strengths (GOSs) of excitations of atomic sodium from ground state to 2p63s0 (3p, 4p, 5p, 6p) states, immersed in Debye plasma, were calculated by using wavefunctions which were obtained numerically from the restricted Hartree-Fock (RHF) equation. This RHF equation employs the local density approach for exchange interactions including plasma Debye screening. Theoretical RHF and random phase approximation with exchange (RPAE) velocity calculations have shown that the GOSs for excitations to 3 s0(3 p,4 p,5 p,6 p)depend on the plasma Debye screening effects, as shown by the reduction in the GOS amplitude with decreasing Debye length λD. The agreement between the present RPAE V results for the transitions 3 s→3 s0(3 p,4 p,5 p)and the length calculations of Martínez-Flores was satisfactory. Correlation effects were found quite to be significant in the vicinity of the maxima of the GOS of the 3 s→3 s0(4 p,5 p,6 p)excitations by using the RPAE V approach. We note the poor influence of many electron correlations on the GOS of (3 s→3 p)transition with the same principal quantum number. Finally, we comment that the RPAE V calculations are useful in investigating electron correlation effects on the transition GOS of atomic sodium planted in Debye plasma. The present velocity results also reveal that the 3 s→3 s0(5p, 6p)transition GOSs tend to be delocalized due to more significant screening effects at Debye lengths λD=20and 30 a.u. for excited subshells 5p and 6p, respectively. We report here novel results of GOS for 3 s→3 s06ptransition obtained from different Debye lengths.

关键词： Plasma Screening Effect Correlation Effect Sodium Atomic Velocity Form GOS Restricted Hatree-Fock Random Phase Approximation with Exchange

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Treatment of Kidney Stones by Percutaneous Nephrolithotomy: Evaluation of the Results of the First Series of Our Experience in the Urology Department of the Idrissa Pouye General Hospital in Dakar

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Open Journal of Urology 2024年第2期14卷 104-114页

作者： Mouhamadou Moustapha Mbodji Mohamed Jalloh Medina Ndoye Abdourahmane Diallo Issa Labou Lamine Niang Serigne Magueye gueye Department of Urology and Andrology Hospital General Idrissa Pouye Dakar Senegal

The principle of PCNL is the extraction through a nephrostomy channel of kidney stones which are defined as the presence of crystalline concretions in the kidneys. Objectives: The objective of this work was to study the epidemiological, clinical and paraclinical aspects of patients with renal lithiasis treated by PCNL and on the other hand the different technical aspects of PCNL. Materials and Methods: This was a retrospective descriptive study, conducted in the urology department of HOGIP, covering the period from January 2015 to January 2019. We studied the demographic and clinical aspects of patients presenting renal lithiasis;we also studied the technical aspects and treatment outcomes. Statistical significance was set for α = 0.05. Results: Our series covered 82 PCNLs performed during the study period. The average age was 45.95 years, the age group [40 - 49 years] was more affected. Our study involved 44 men and 38 women, a sex ratio of 1.15. At the clinic, atypical lumbar pain was more frequent in 45.83% of cases. On URO-CT, the calculations were located more at the pyelic level (31.2%) and lower caliceal (27.2%). The size of stones measured between 15 and 20 mm in 30.52%. The stone density was between 500 and 1000 HU in 47.54% of cases. Intraoperatively, the patients were placed in lateral decubitus in 41.46% of cases. Only one access to the kidney was necessary in 87.8% of cases. The lithoclast was used in 65.85% of cases. The overall success rate (stone free) in our series was 96%. The majority of cases, 41.44%, drainage were done by natural means (totally tubeless). The average duration was 92 minutes. The complications encountered in our experience concerned 10 cases, a rate of 12.19%. Conclusion: Urinary lithiasis is more and more frequent in our regions. The development of Endo-urology offers several therapeutic options. Thus, PCNL occupies an important place in the management of kidney stones.

关键词： HOGIP Kidney Stones PCNL Stone Free Uro CT Scan

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