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Soft X-ray ptychography method at SSRF

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Nuclear Science and Techniques 2017年第6期28卷 86-94页

作者： Chun-Peng Wang Zi-Jian Xu Hai-Gang Liu Xulei Tao ren-zhong tai Shanghai Institute of Applied Physics Chinese Academy of Sciences University of Chinese Academy of Sciences

Ptychography is a diffraction-based X-ray microscopy technique in which an extended sample is scanned by a coherent beam with overlapped illuminated areas and complex transmission function of the sample is obtained by applying iterative phase retrieval algorithms to the diffraction patterns recorded at each scanned *** permits quantitatively imaging of non-crystalline specimens at a resolution limited only by the X-ray wavelength and the maximal scattering angle *** this paper,the development of soft X-ray ptychography method at the BL08U1 A beamline of Shanghai Synchrotron Radiation Facility is *** experimental setup,experimental parameters selection criteria,and post-experimental data analyzing procedures are presented in detail with a prospect of high-resolution image reconstruction in real *** performance of this newly implemented method is demonstrated through the measurements of a resolution test pattern and two real samples:Pt-Co alloy nanoparticles and a breast cancer *** results indicate that strong scattering specimens can be reconstructed to sub-20 nm resolution,while a sub-25 nm resolution for biological specimens can be achieved.

关键词： Ptychography Coherent diffraction imaging X-ray microscopy Phase retrieval

Design of wide-range energy material beamline at the Shanghai Synchrotron Radiation Facility

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Nuclear Science and Techniques 2018年第2期29卷 91-102页

作者： Zhen-Hua Chen Fan-Fei Sun Ying Zou Fei Song Shuo Zhang Zheng Jiang Yong Wang ren-zhong tai Shanghai Institute of Applied Physics Chinese Academy of Sciences

We report the design of a wide-range energy material beamline(E-line) with multiple experimental techniques at the Shanghai Synchrotron Radiation *** undulators consisted of an elliptically polarizing undulator and in-vacuum undulator that generate the soft and hard X-rays, respectively. The beamline covered a wide energy range from 130 to 18 ke V with both a high photon flux([ 10^(12) phs/s with exit silt 30 lm in soft X-ray and [ 5 9 10^(12) phs/s in hard X-ray within 0.1%BW bandwidth) and promising resolving power(maximum E/DE [ 15,000 in soft X-ray with exit silt 30 lm and [6000 in hard X-ray). Moreover, the beam spots from the soft and hard X-rays were focused to the same sample position with a high overlap ratio, so that the surfaces, interfaces, and bulk properties were characterized in situ by changing the probing depth.

关键词： Synchrotron radiation Beamline Wide energy range E-line Shanghai Synchrotron Radiation Facility

Picosecond time-resolved X-ray ferromagnetic resonance measurements at Shanghai synchrotron radiation facility

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Nuclear Science and Techniques 2022年第5期33卷 126-134页

作者： Xia Yang Jie-Feng Cao Jun-Qin Li Fang-Yuan Zhu Rui Yu Jian He Zi-Long Zhao Yong Wang ren-zhong tai Shanghai Institute of Applied Physics Chinese Academy of SciencesShanghai 201800China University of Chinese Academy of Sciences Beijing 100049China Shanghai Synchrotron Radiation Facility Shanghai Advanced Research InstituteChinese Academy of SciencesShanghai 201204China

An experimental picosecond time-resolved X-ray ferromagnetic resonance(TR-XFMR)apparatus with a time resolution of 13 ps(RMS)or 31 ps(FWHM)was constructed and demonstrated in the 07U and 08U1A soft X-ray beamlines at the Shanghai Synchrotron Radiation Facility(SSRF)using pump-probe detection and X-ray magnetic circular dichroism(XMCD)*** and time-resolved ferromagnetic resonance was excited by continuous microwave phase-locking of the bunch clock within the photon beam during synchrotron radiation and was characterized by detecting the magnetic circular dichroism signals of the elements of interest in the magnetic *** this equipment,we measured the amplitude of the element-specific moment precession during ferromagnetic resonance(FMR)at 2 GHz in a single Ni81Fe19layer.

关键词： Ferromagnetic resonance Time resolution Pump-probe Synchrotron radiation

High-precision X-ray polarimeter based on channel-cut crystals

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Nuclear Science and Techniques 2024年第3期35卷 30-39页

作者： Shang-Yu Si zhong-Liang Li Wen-Hong Jia Lian Xue Hong-Xin Luo Jian-Cai Xu Bai-Fei Shen Lin-Gang Zhang Liang-Liang Ji Yu-Xin Leng ren-zhong tai Shanghai Institute of Applied Physics Chinese Academy of SciencesShanghai 201800China University of Chinese Academy of Sciences Beijing 100049China Shanghai Synchrotron Radiation Facility Shanghai Advanced Research InstituteChinese Academy of SciencesShanghai 201204China Shanghai Institute of Optics and Fine Mechanics Chinese Academy of SciencesShanghai 201800China

We report on using synthetic silicon for a high-precision X-ray polarimeter comprising a polarizer and an analyzer,each based on a monolithic channel-cut crystal used at multiple Brewster reflections with a Bragg angle very close to 45°.Experiments were performed at the BL09B bending magnet beamline of the Shanghai Synchrotron Radiation Facility using a Si(800)crystal at an X-ray energy of 12.914 keV.A polarization purity of 8.4×10^(-9)was *** result is encouraging,as the measured polarization purity is the best-reported value for the bending magnet ***,this is the firstly systematic study on the hard X-ray polarimeter in China,which is crucial for exploring new physics,such as verifying vacuum birefringence.

关键词： X-ray polarimeter Vacuum birefringence Synchrotron radiation Channel-cut crystal

Spatial-and spin-resolution ARPES and magnetism beamline at SSRF

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Nuclear Science and Techniques 2024年第8期35卷 23-37页

作者： Fang‑Yuan Zhu Jie‑Feng Cao Xiang‑Yu Meng Jun‑Qin Li Rui Yu Ya‑Mei Wang Shan Qiao Bo Zhao Ming‑Zhu Zhang zhong‑Kai Liu Mei‑Xiao Wang Yong Wang ren‑zhong tai Shanghai Synchrotron Radiation Facility Shanghai Advanced Research InstituteChinese Academy of SciencesShanghai 201204China ShanghaiTech Laboratory for Topological Physics School of Physical Science and TechnologyShanghai Tech UniversityShanghai 201210China University of Chinese Academy of Sciences Beijing 100049China

The BL07U beamline is a new extreme ultraviolet and soft X-ray beamline housed in the Shanghai Synchrotron Radiation Facility. Beamlines are used in nano-resolved angle-resolved photoemission spectroscopy(nano-ARPES), spin-resolved angle-resolved photoemission spectroscopy(spin-ARPES), X-ray magnetic circular dichroism spectroscopy, and X-ray magnetic linear dichroism spectroscopy for certain scientific research. The BL07U beamline, which is based on a pair of elliptical polarized undulators and a variable-included-angle plane-grating monochromator, delivers circularly or linear polarized X-rays within the energy range of 50–2000 eV. The beamline features two branches: One dedicated to nano-ARPES,which has a minimum spot size of only ~ 200 nm, and another branch comprising spin-ARPES, a vector magnetic field, and superconductive magnetic end-station.

关键词： Soft X-ray beamline Nano-ARPES Spin-ARPES XMCD/XMLD

An APXPS endstation for gas–solid and liquid–solid interface studies at SSRF

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Nuclear Science and Techniques 2019年第5期30卷 103-112页

作者： Jun Cai Qiao Dong Yong Han Bao-Hua Mao Hui Zhang Patrik G.Karlsson John ?hlund ren-zhong tai Yi Yu Zhi Liu State Key Laboratory of Functional Materials for Informatics Shanghai Institute of Microsystem and Information TechnologyChinese Academy of Sciences School of Physical Science and Technology ShanghaiTech University University of Chinese Academy of Sciences Scienta Omicron Shanghai Institute of Applied Physics Chinese Academy of SciencesShanghai Synchrotron Radiation Facility

In the past few decades, various surface analysis techniques find wide applications in studies of interfacial phenomena ranging from fundamental surface science,catalysis, environmental science and energy *** the help of bright synchrotron sources, many of these techniques have been further advanced into novel in-situ/operando tools at synchrotron user facilities, providing molecular level understanding of chemical/electrochemical processes in-situ at gas–solid and liquid–solid *** a proper endstation for a dedicated beamline is one of the challenges in utilizing these techniques efficiently for a variety of user's requests. Many factors,including pressure differential, geometry and energy of the photon source, sample and analyzer, need to be optimized for the system of interest. In this paper, we discuss the design and performance of a new endstation at beamline02 B at the Shanghai Synchrotron Radiation Facility for ambient pressure X-ray photoelectron spectroscopy *** system, equipped with the newly developed hightransmission HiPP-3 analyzer, is demonstrated to be capable of efficiently collecting photoelectrons up to 1500 eV from ultrahigh vacuum to ambient pressure of 20 *** spectromicroscopy mode of HiPP-3 analyzer also enables detection of photoelectron spatial distribution with resolution of 2.8 ± 0.3 lm in one dimension. In addition,the designing strategies of systems that allow investigations in phenomena at gas–solid interface and liquid–solid interface will be highlighted through our discussion.

关键词： Ambient pressure XPS Synchrotron Liquid- solid interface Spectromicroscopy

Latest developments in EUV photoresist evaluation capability at Shanghai Synchrotron Radiation Facility

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Nuclear Science and Techniques 2023年第12期34卷 206-215页

作者： Zhen‑Jiang Li Cheng‑Hang Qi Bei‑Ning Li Shu‑Min Yang Jun Zhao Zhi‑Di Lei Shi‑Jie Zhu Hao Shi Lu Wang Yan‑Qing Wu ren‑zhong tai Shanghai Institute of Applied Physics Chinese Academy of SciencesShanghai 201800China University of Chinese Academy of Sciences Beijing 100049China Shanghai Synchrotron Radiation Facility Shanghai 201204China ShanghaiTech University Shanghai 201210China Key Laboratory of Materials for High Power Lasers Shanghai Institute of Optics and Fine MechanicsChinese Academy of SciencesShanghai 201800China College of Materials Science and Opto‑Electronic Technology University of Chinese Academy of SciencesBeijing 100083China Shanghai University Shanghai 200444China

Evaluating the comprehensive characteristics of extreme ultraviolet(EUV)photoresists is crucial for their application in EUV lithography,a key process in modern *** paper highlights the capabilities of the Shanghai Synchrotron Radiation Facility(SSRF)08U1B beamline in advancing this ***,it demonstrates how this beamline can create fringe patterns with a 15-nm half-pitch on a resist using synchrotron-based EUV *** achievement is vital for evaluating EUV photoresists at the advanced 5-nm *** provide a detailed introduction to the methods and experimental setup used at the SSRF 08U1B beamline to assess an EUV photoresist.A significant part of this research involved the fabrication of high-resolution hydrogen silsesquioxane mask *** gratings,with an aspect ratio of approximately 3,were created using electron beam lithography on an innovative mask *** framework was crucial in eliminating the impact of zeroth-order light on interference *** proposed framework propose offers a new approach to mask fabrication,particularly beneficial for achromatic Talbot lithography and multicoherent-beam interference applications.

关键词： Extreme ultraviolet photoresist Interference lithography High-resolution Electron beam lithography·Hydrogen silsesquioxane Grating

Millisecond dynamics of colloidal suspension studied by X-ray photon correlation spectroscopy at the Shanghai Synchrotron Radiation Facility

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Nuclear Science and Techniques 2024年第1期35卷 1-9页

作者： Chen-Hui Cui Zi-Mu Zhou Lin-Feng Wei Song-Lin Li Feng Tian Xiu-Hong Li Zhi Guo Yi-Hui Xu Huai-Dong Jiang ren-zhong tai Shanghai Synchrotron Radiation Facility Shanghai Advanced Research InstituteChinese Academy of SciencesShanghai 201204China School of Physical Science and Technology ShanghaiTech UniversityShanghai 201210China Shanghai Institute of Applied Physics Chinese Academy of SciencesShanghai 201800China University of Chinese Academy of Sciences Chinese Academy of SciencesBeijing 100049China Center for Transformative Science ShanghaiTech UniversityShanghai 201210China

X-ray photon correlation spectroscopy(XPCS)has emerged as a powerful tool for probing the nanoscale dynamics of soft condensed matter and strongly correlated materials owing to its high spatial resolution and penetration *** technique requires high brilliance and beam coherence,which are not directly available at modern synchrotron beamlines in *** facilitate future XPCS experiments,we modified the optical setup of the newly commissioned BL10U1 USAXS beamline at the Shanghai Synchrotron Radiation Facility(SSRF).Subsequently,we performed XPCS measurements on silica suspensions in glycerol,which were opaque owing to their high *** were collected using a high frame rate area detector.A comprehensive analysis was performed,yielding correlation functions and several key dynamic *** the results were consistent with the theory of Brownian motion and demonstrated the feasibility of XPCS at ***,by carefully optimizing the setup and analyzing the algorithms,we achieved a time resolution of 2 ms,which enabled the characterization of millisecond dynamics in opaque systems.

关键词： XPCS SSRF Silica suspension Glycerol Brownian motion Millisecond dynamics

Coexistence of Polaronic States and Superconductivity in Iron-Pnictide Compound Ba_2Ti_2Fe_2As_4O

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Chinese Physics Letters 2018年第5期35卷 119-122页

作者： Li-Yuan Rong Xun Shi Pierre Richard Yun-Lei Sun Guang-Han Cao Xiang-Zhi Zhang Jun-Zhang Ma Ming Shi Yao-Bo Huang Tian Qian Hong Ding ren-zhong tai Shanghai Synchrotron Radiation Facility Shanghai Institute of Applied Physics Chinese Academy of Sciences Shanghai 201204 School of Physics University of Chinese Academy of Sciences Beijing 100190 Beijing National Laboratory for Condensed Matter Physics and Institute of Physics Chinese Academy of Sciences Beijing 100190 Collaborative Innovation Center of Quantum Matter Beijing 100084 Department of Physics Zhejiang University Hangzhou 310027 Paul Scherrer Institut Swiss Light Source Villigen PSI CH-5232 Switzerland

The electronic structure of iron-pnictide compound superconductor Ba_2Ti_2Fe_2As_4O, which has metallic intermediate Ti_2O layers, is studied using angle-resolved photoemission spectroscopy. The Ti-related bands show a‘peak-dip-hump＇ line shape with two branches of dispersion associated with the polaronic states at temperatures below around 120 K. This change in the spectra occurs along with the resistivity anomaly that was not clearly understood in a previous study. Moreover, an energy gap induced by the superconducting proximity effect opens in the polaronic bands at temperatures below T_c（~21 K）. Our study provides the spectroscopic evidence that superconductivity coexists with polarons in the same bands near the Fermi level, which provides a suitable platform to study interactions between charge, lattice and spin freedoms in a correlated system.

关键词： Ti As Coexistence of Polaronic States and Superconductivity in Iron-Pnictide Compound Ba2Ti2Fe2As4O Fe Ba