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Preparation and Characterization of eco-friendly Carboxymethyl Cellulose Antimicrobial Nanocomposite Hydrogels

Journal of Renewable Materials 2018年第5期6卷 536-547页

作者： Sawsan Dacrory Hussein abou-Yousef ragab e.abou-zeid Samir Kamel Mohamed S.Abdel-Aziz Mohamed elbadry Cellulose and Paper Department National Research Centre33 El Buhouth St.DokkiGiza 12622Egypt Microbial Chemistry Department National Research Centre33 El Buhouth St.DokkiGiza 12622Egypt Department of Chemistry Faculty of ScienceAin Shams UniversityAbbassiaCairo 11566Egypt

Carboxymethyl cellulose hydrogels were developed through crosslinking process using eco-friendly crosslinkers such as maleic,succinic,and citric *** cellulose was prepared from the cellulosic fraction of olive industry residues.A series of hydrogels with varying crosslinker acid concentrations,reaction times,and reaction temperatures was produced to study the swelling capacities and gel fraction of the obtained *** study pertains to the preparation of antimicrobial nanocomposite hydrogels through in-situ incorporation of the silver nanoparticles during the crosslinking *** nanoparticles were prepared by reduction of AgNO3 with leaves of Ricinus *** particle size of prepared silver nanoparticles was detected by transmission electron microscopy(TeM).Chemical structure and morphological characterizations of the prepared hydrogels were performed using Fourier transform infrared spectroscopy(FTIR),scanning electron microscopy(SeM),and energy-dispersive X-ray spectroscopy(eDX).Finally,the antimicrobial activity of the loaded silver hydrogels against Gram negative(G-ve),Gram positive(G+ve),and Candida albicans yeast was demonstrated.

关键词： Hydrogel crosslinked carboxymethyl cellulose silver nanoparticles antibacterial activity

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Surfactant-Assisted Poly(lactic acid)/Cellulose Nanocrystal Bionanocomposite for Potential Application in Paper Coating

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Journal of Renewable Materials 2018年第4期6卷 394-401页

作者： ragab e.abou-zeid Mohamed A.Diab Salah A.A.Mohamed Ahmed Salama Hind Abdullah Aljohani Kamel Rizq Shoueir Cellulose and Paper Department National Research Centre33 El-Bohouth St.DokkiP.O.12622GizaEgypt Packing and Packaging Materials Department National Research Centre33 El-Bohouth St.DokkiP.O.12622GizaEgypt Tabuk University Chemistry DepartmentCollege of Al WajhAl WajhSaudi Arabia Institute of Nanoscience&Nanotechnology Chemistry departmentKafr Elsheikh University33516 Kafr ElsheikhEgypt

The current article addresses a new strategy for the preparation of polylactic acid/cellulose nanocrystal(PLA/CNCs)nanobiocomposite films with improved structural morphology,mechanical and barrier properties for food packaging *** addition of hexadecyltrimethylammonium bromide(CTAB)and sodium lauryl sulfate(SLS)as cationic and anionic surfactants respectively,was found to play a crucial role in preventing re-aggregation of the CNCs during drying and improving the dispersion of CNCs in the *** coated paper was characterized using mechanical tests,water vapor permeability(WVP),X-ray diffraction(XRD),scanning electron microscopy(SeM)and air *** results showed that the paper coated with PLA containing 7.5%CNCs and 0.15%CTAB based on weight of PLA,gives the highest measured paper properties,where an increase in tensile strength(+133%),Young’s modulus(+309%),tear index(+183%),burst(+60.8)and a decrease in air permeability(−92%)was obtained.

关键词： Cellulose nanocrystal surfactant paper coating mechanical properties air permeability water vapor permeability

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Removal of Cu(II),Pb(II),Mg(II),and Fe(II) by Adsorption onto Alginate/Nanocellulose Beads as Bio-Sorbent

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Journal of Renewable Materials 2021年第4期9卷 601-613页

作者： ragab e.abou-zeid Korany A.Ali Ramadan M.A.Gawad Kholod H.Kamal Samir Kamel Ramzi Khiari Cellulose and Paper Department National Research CentreGiza12622Egypt Applied Organic Chemistry Department Center of Excellence for Advanced ScienceNational Research CentreGiza12622Egypt Water Pollution Research Department National Research Centre Giza12622Egypt Faculty of Sciences of Monastir Research Unit of Applied Chemistry and EnvironmentUniversity of MonastirMonastir5019Tunisia Higher Institute of Technological Studies(ISeT)of Ksar-Hellal Ksar-Hellal5070Tunisia University of Grenoble Alpes CNRSGrenoble INPLGP2GrenobleF-38000France

Alginate blended with cellulose nanocrystals(CNC),cellulose nanofibers(CNF),and tri-carboxylate cellulose nanofibers(TPC-CNF)prepared and encapsulated in the form of microcapsules(bio-polymeric beads).The cellulosic nanomaterials that used in this study were investigated as nanomaterials for wastewater treatment *** experiments were performed to study the removal of copper,lead,magnesium,and iron from aqueous solutions by the prepared *** effects of the sorbent dosage and the modified polymers on the removing efficiency of the metal cations were *** absorption was used to measure the metal ions *** modified bio-polymeric beads(Alg-CNF,Alg-CNC,and Alg-TPC-CNF)exhibited high-efficiency towards removing of the metal cations;Cu^(2+),Pb^(2+),Mg^(2+),and Fe^(2+).The Alg-TPC-CNF composite was exhibited excellent removing efficiency which around 95%for Pb,92%for Cu,43%for Fe and 54%for *** outcomes affirm that the utilization of nanomaterials giving higher adsorption capacities contrasted with similar material in its micro or macrostructure form.

关键词： Biopolymers nanocellulose alginate heavy metal removal wastewater treatment

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