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Effect of Filler Content on Flexural and Viscoelastic Properties of Coir Fibers and Argania Nut-shells Reinforced Phenolic Resin Composites

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Journal of Bionic Engineering 2022年第6期19卷 1886-1898页

作者： Hala Bensalah Marya Raji Kamal Gueraoui Abdelazziz Khtira Hamid Essabir rachid bouhfid Abou el kacem Qaiss Group of Mechanics and Materials Energy Research CenterFaculty of ScienceMohammed V University in Rabat10100RabatMorocco Composites and Nanocomposites Center Moroccan Foundation for Advanced ScienceInnovation and Research(MAScIR)10100RabatMorocco Mohammed Ⅵ Polytechnic University Lot 660 Hay Moulay Rachid43150Ben GuerirMorocco Group of Simulation in Mechanics and Energy Energy Research CenterFaculty of ScienceMohammed Ⅴ University10100RabatMorocco Group of Semiconductors and Environmental Sensor Technologies Energy Research CenterFaculty of ScienceMohammed V University10100RabatMorocco Mechanic Materials and Composites(MMC) Laboratory of Energy EngineeringMaterials and SystemsNational School of Applied Sciences of AgadirIbn Zohr University80000AgadirMorocco

The characteristics of two different kinds of lignocellulosic materials(vegetable fillers)with two morphologies as Argania nut-shells(ANS)particles and Coir Fibers(CF)were used as reinforcement for phenolic resin(Bakelite)in this work,and the composite are studied as a function of filler types,shape,content(10,20,and 30%wt.percent)and manufacturing loading force(1500 and 3000 LBs).Compression molding was used to create the composites,which were then evaluated using Scanning electronic microscopy(SEM),Fourier-transform infrared spectroscopy(FTIR),bending,dynamic-mechanical-thermal and rheological studies.The morphology of broken samples demonstrates that both fillers are well dispersed and distributed.When fillers are added to the matrix,the flexural characteristics improve,and the optimal values are attained in the case of Argania nut-shells.The results showed that the kind and shape of the fillers had a direct influence on the dynamic mechanical characteristics of the composites due to the reinforcement's modulus augmentation.It was noticed that,the increment of manufacturing loading force decreased the mechanical and dynamical properties of composites.The optimum properties obtained indicate that the composites can only be manufactured at low manufacturing loading force(1500 LBs).

关键词： Phenolic resin composites Bionic materials Coir Fibers Argania nut-shells Dynamical mechanical properties Rheological properties

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pH-indicative Films Based on Chitosan–PVA/Sepiolite and Anthocyanin from Red Cabbage: Application in Milk Packaging

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Journal of Bionic Engineering 2022年第3期19卷 837-851页

作者： Marya Raji Laila El Foujji Mohamed El Mehdi Mekhzoum Mounir El Achaby Hamid Essabir rachid bouhfid Abou el kacem Qaiss Moroccan Foundation for Advanced Science Innovation and ResearchComposites and Nanocomposites CenterRabat Design CenterRue Mohamed El JazouliMadinat El IrfaneRabat10100Morocco Faculty of Science Laboratoire de Chimie Organique Et HétérocycliqueUniversity Mohammed V in RabatRabat10100Morocco Materials Science and Nano-Engineering Department Mohammed VI Polytechnic UniversityLot 660–Hay Moulay RachidBen Guerir43150Morocco Mechanic Materialsand Composites(MMC)Laboratory of Energy EngineeringMaterials and SystemsNational School of Applied Sciences of AgadirIbn Zohr UniversityAgadir80000Morocco

Biobased smart packaging is been the most interesting research field.In this study,pH-sensitive films based on anthocyanin molecules from red cabbage and sepiolite mineral nano-clay as functional additives were studied.The films were fabricated by casting method of blend polymer Chitosan/Poly(Vinyl Alcohol)at two fillers loading(5wt.%and 10wt.%).The structural,morphological,thermal,optical,hygroscopic,and mechanical properties as well as the pH sensitivity of films were investigated.The thermal properties confirm that the amount of the anthocyanin in sepiolite was around 6.4%.The tensile strength and the young’s modulus of produced composites at 10wt.%sepiolite–anthocyanin content was increased to 8.90 MPa and 163 MPa,respectively.The maximum water absorption that the films may absorb was 12.3%.pH sensitivity analysis showed that the Smart films change the color by changing the pH level,from pink at pH lower than 6 to yellow at pH higher than 6.Thus,the developed pH-sensitive films show band gaps in visible light that make them useful for monitoring milk spoilage.

关键词： Smart packaging Anthocyanin Red cabbage pH-sensitive and milk spoilage

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Morphological, Structural, Thermal and Tensile Properties of High Density Polyethylene Composites Reinforced with Treated Argan Nut Shell Particles

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Journal of Bionic Engineering 2015年第1期12卷 129-141页

作者： Hamid Essabir Mounir EI Achaby EI Moukhtar Hilali rachid bouhfid AbouEIkacem Qaiss Moroccan Foundation for Advanced Science Innovation and Research (MAScIR) Institute of Nanomaterials and Nanotechnology (NANOTECH) Laboratory of Polymer Processing Rabat Morocco National School of Applied Sciences Ibn Zohr University Laboratory Mechanics Processes Energy and Environment Agadir Morocco

High Density Polyethylene （HDPE） composites reinforced with treated bio-filler from Argan-Nut Shell （ANS） at various filler contents are prepared by extrusion and injection molding processes. The microstructures of the composites are charac- terized by Fourier Transform Infrared Spectroscopy （FTIS） and Scanning Electron Microscopy （SEM）; the thermal stability is analyzed by Thermogravimetric Analysis （TGA）, and their mechanical properties are investigated by dynamical mechanical analysis and rheological testing. The morphological and structural results indicate an improvement in adhesion between the ANS fillers and HDPE matrix upon alkali treatment. The mechanical properties of the composites show a significant increase in young＇s modulus with the addition of filler, a gain of 58% is marked compared to neat polymer, Thermal analysis reveals that the incorporation of bio-filler in polymer results in a decrease in decomposition temperatures. This research offers an ecological alternative to upgrade the valorization of abundant and unexploited Moroccan resources. In addition, the possibility of finding uses for ANS in composite manufacturing will help open new markets for what is normally considered waste or for use in low value products.

关键词： argan tree argan nut shell particles polymer composite melt extrusion mechanical properties

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Production and Characterization of High Density Polyethylene Reinforced by Eucalyptus Capsule Fibers

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Journal of Bionic Engineering 2018年第3期15卷 558-566页

作者： Wafa Ouarhim Mohammed-Ouadi Bensalah Denis Rodrigue Hamid Essabir rachid bouhfid Abou el kacem Qaiss Moroccan Foundation for Advanced Science Innovation and Research (MAScIR) Institute of Nanomaterials and Nanotechnology (NANOTECH) Laboratory of Polymer Processing Rabat Morocco Faculty of Science Laboratory of Mechanic and Materials (LMM) Mohammed V-Rabat University Rabat Morocco Department of Chemical Engineering and CERMA Universite Laval Quebec G1V0A6 Canada

In this work, Eucalyptus Capsule Fibers （ECF） are proposed as a new natural fiber reinforcement to produce bio-composites due to their biological origin, specific smell and color. High Density Polyethylene （HDPE） is used as the matrix to compare three reinforcement types, raw ECF, alkali treated ECF, and ECF treated with PE-graft-maleic anhydride （PE-g-MA） as a coupling agent at three concentrations （5 wt.%, 10 wt%, and 15 wt%）. A complete set of characterization is performed including tension, torsion, hardness, Melt Flow Index （MFI）, Attenuated Total Reflection Fourier Transform Infrared Spectroscopy （ATR-FTIR）, Contact Angle （CA）, Scanning Electron Microscopy （SEM）, Thermogravimetric Analysis （TGA） and Dynamic Mechanical Analysis （DMA）. The results show that the best mechanical and rheological improvements are obtained by using the coupling agent with alkali treated fibers.

关键词： eucalyptus capsule fibers polyethylene alkaline treatment coupling agent mechanical properties

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Laminated Epoxy Biocomposites Based on Clay and Jute Fibers

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Journal of Bionic Engineering 2017年第2期14卷 379-389页

作者： Hind Abdellaoui Hala Bensalah Marya Raji Denis Rodrigue rachid bouhfid Abou el kacem Qaiss Moroccan Foundation for Advanced Science Innovation and Research (MASclR) Institute of Nanomaterials and Nanotechnology (NANOTECIt) Laboratory of Polymer Processing Rabat Morocco Faculty of Science Laboratory of Simulation in Mechanics and Energy Mohammed V University Rabat Morocco Faculty of Science Laboratory Laboratoire de Chimieorganique et Heterocyclique Mohammed V University Rabat Morocco Department of chemical engineering and CERMA Universite Laval Quebec G1V0A6 Canada

Jute/epoxy hybrid laminated biocomposites were manufactured by using Illite clay particles at various content （5 wt.% - 20 wt.%）. The effects of hybridization on the morphology, structure, and mechanical properties were investigated. The properties of the biocomposites reinforced with jute fibers were mainly influenced by the interfacial adhesion between the jute fibers and the epoxy matrix. An alkali treatment was applied to improve the interfacial fiber-matrix adhesion and thus obtaining better mechanical properties. Besides the chemical treatment, epoxy hybridization using clay particles also had a strong effect on the overall properties of laminated biocomposites. The mechanical properties of the jute/epoxy biocomposites reinforced with Illite clay increased with clay content, up to an optimum value at 15 wt.%. The average technique and the laminates theory were performed to validate the coherence of the elastic moduli between the calculated and experimental values. A difference between the experimental and predicted data was observed, which was attributed to the simplifying assumptions made in both models. The laminates theory gave better overall predictions.

关键词： laminated biocomposites hybridization mechanical properties interracial adhesion surface treatment

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A Comparison between Sabra and Alfa Fibers in Rubber Biocomposites

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Journal of Bionic Engineering 2019年第4期16卷 754-767页

作者： Wafa Ouarhim Hamid Essabif Mohammed-Ouadi Bensalah Denis Rodrigue rachid bouhfid Abou el kacem Qaiss Moroccan Foundation for Advanced Science Innovation and Research(MAScIR)Composites and Nanocomposites Center(CNC)Rabat 10100Morocco Faculty of Science Laboratory of Mechanic and Materials(LMM)Mohammed V-RabatUniversityRabat 10100Morocco National School of Applied Science(ENSA) Ibn Zohr University-AgadirAgrandir 80000Morocco Department of Chemical Engineering and CERMA Universite LavalQuebec G1V0A6Canada

The main objective of this investigation is to valorize a Moroccan crop residue(Sabra fibers,Agave Americana L.)and to compare with Alfa fibers(,Stipa tenacissima L.)as reinforcement in an elastomeric matrix in term of the relaxation properties,mechanical and rheological properties.The preparation and properties of these two natural fibers embedded in Styrene-Butadiene Rubber(SBR)are presented with and without the addition of Styrene-Ethylene-Butadiene-Styrene grafted with Maleic Anhydride(SEBS-g-MA)as a coupling agent.Five different series(SBR,SBR/Alfa,SBR/Alfa/SEBS,SBR/Sabra and SBR/Sabra/SEBS)were compounded by extrusion and compression molding.As a result,the addition of the coupling agent in the elastomeric matrix improves the relaxation properties,mechanical and rheological properties.Moreover,Sabra fibers show the good results compared to Alfa fibers.Finally,the Zener model was used to determine the rheological time response of the composites.A good agreement between the experimental data and the model was observed(R^2=0.99).

关键词： Sabra fibers Alfa fibers SBR biocomposite relaxation mechanical and rheological properties Zener model

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Mechanical and Thermal Properties of Polypropylene Reinforced with Almond Shells Particles： Impact of Chemical Treatments

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Journal of Bionic Engineering 2015年第3期12卷 483-494页

作者： Fatima Zahra El Mechtali Hamid Essabir Souad Nekhlaoui Mohammed Ouadi Bensalah Mohammad Jawaid rachid bouhfid AbouEIkacem Qaiss Laboratory of Mechanic and Materials (LMM) Mohammed V-Rabat University Faculty of Science Rabat Morocco Moroccan Foundation for Advanced Science Innovation and Research (MAScIR) Institute of Nanomaterials and Nanotechnology (NANOTECH) Laboratory of Polymer Processing Rabat Morocco Laboratory of Mechanics in Processes Energy and Environment National School of Applied Sciences Ibn Zohr University Agadir Morocco Department of Biocomposite Technology Institute of Tropical Forestry and Forest Products (INTROP) Universiti Putra Malaysia 43400 UPM Serdang Selangor Malaysia

Polypropylene （PP） matrix composites reinforced with chemically treated Almond Shell （AS） particles with and without compatibilizer （PP-g-MA） was prepared by a twin-screw extrusion at loading of 20 wt.% AS particles. Two types of chemical treatments （alkali treatment with sodium hydroxide and etherification with dodecane bromide） of the particles were carried out to improve the interface adhesion between particles and PP matrix. Results show that chemical modifications of AS particles affect the mechanical and viscoelastic properties of AS/PP composites. The composites reinforced with alkali treated particles and the compatibilized matrix lead to a notable increase in the Young＇s modulus （14%） compared to the composites with untreated AS particles. The ductility of composite was also evaluated by the yield strain, and results show a notable increase （31%） compared to that of composites with untreated particles. The thermal stability increased with the use of etherification （385 ℃）, with gains in the temperature up to 23 ℃ compared to neat PP （362 ℃）. The achieved results show that the AS/PP composites can be used in several applications. A thermoplastic matrix compsite mixed with treated AS particles appears to be a good alternative to obtain environmentally friendly products.

关键词： PP AS chemical treatment composite extrusion injection

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