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Recovery of silica from sodium silicate solution of calcined boron mud

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Rare Metals 2016年第2期35卷 204-210页

作者： Zhi-Qiang Ning Yu-Chun Zhai Hong-Wei Xie qiu-shi song Ka Yu School of Materials and Metallurgy Northeastern University

The effect of several parameters on the recovery of silicon dioxide from calcined boron mud（CBM）such as stirring speed, temperature, sodium silicate concentration, and carbonation time was studied. The recovery of silicon dioxide is 88 % when the stirring speed is450 r min-1, temperature is 60 °C, sodium silicate concentration is 1 mol L-1, and the carbonation time is 6 *** effect of carbonation time on the recovery of silicon dioxide is divided into three kinetic regimes, and the carbonation process of sodium silicate solution follows a second-order reaction based on the double-film theory model. The apparent rate constant of the three kinetic regimes is 0.064, 3.178, and 1.130 L h mol-1, *** amorphous SiO_2 products obtained by carbonating the purified solution have 99.6 % purity and are spherical with diameters of about 100 nm.

关键词： Boron mud Carbonation Recovery Silicon dioxide

Nickel leaching from low-grade nickel matte using aqueous ferric chloride solution

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Rare Metals 2019年第12期38卷 1199-1206页

作者： Zhi-Qiang Ning Hong-Wei Xie qiu-shi song Hua-Yi Yin Yu-Chun Zhai School of Metallurgy Northeastern University

Nickel leaching from low-grade nickel matte(LGNM) using aqueous ferric chloride solution was *** influence of factors such as leaching temperature and concentration of ferric chloride on the nickel leaching ratio was *** results show that increasing leaching temperature and concentration of ferric chloride increases the nickel leaching *** overall nickel leaching process follows the unreacted shrinking core model,and the surface chemical reaction is the rate-controlling *** activation energy and the reaction order of the nickel leaching process,controlled by the surface chemical reaction,were calculated to be 52.96 kJ mol^(-1)and 0.5,***,the kinetics equation for the nickel leaching was found to be 1-(1-α)^(1/3)=7.18×10~4C^(0.5)exp[-52,960/(RT)]t.

关键词： Nickel matte Ferric chloride Sulfur Kinetics

Electrochemical derusting in molten Na_(2)CO_(3)–K_(2)CO_(3)

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International Journal of Minerals,Metallurgy and Materials 2021年第4期28卷 637-643页

作者： Dong-yang Zhang Xue Ma Hong-wei Xie Xiang Chen Jia-kang Qu qiu-shi song Hua-yi Yin Key Laboratory for Ecological Metallurgy of Multimetallic Mineral of Ministry of Education School of MetallurgyNortheastern UniversityShenyang 110819China Key Laboratory of Data Analytics and Optimization for Smart Industry of Ministry of Education Northeastern UniversityShenyang 110819China

The formation of a rust layer on iron and steels surfaces accelerates their degradation and eventually causes material *** addition to fabricating a protective layer or using a sacrificial anode, repairing or removing the rust layer is another way to reduce the corrosion rate and extend the lifespans of iron and ***, an electrochemical healing approach was employed to repair the rust layer in molten Na_(2)CO_(3)-K_(2)CO_(3).The rusty layers on iron rods and screws were electrochemically converted to iron in only several minutes and a metallic luster *** electron microscopy(SEM) and energy dispersive X-ray spectroscopy(EDS) analyses showed that the structures of the rust layer after healing were slightly porous and the oxygen content reached a very low ***, high-temperature molten-salt electrolysis may be an effective way to metalize iron rust of various shapes and structures in a short time, and could be used in the repair of cultural relics and even preparing a three-dimensional porous structures for other applications.

关键词： molten salt electro-deoxidation rust stainless steel derusting

Enhanced service stability and thermoelectric performance in Cu_(2)−δSebased composites

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Science China Materials 2024年第7期67卷 2369-2370页

作者： Pengfei qiu Xun shi State Key Laboratory of High Performance Ceramics and Superfine Microstructure Shanghai Institute of CeramicsChinese Academy of SciencesShanghai 200050China

Thermoelectric(TE)materials can directly convert the industrial waste heat into useful electricity based on the Seebeck effect,providing a promising way to tackle the environmental pollution and global energy crisis[1].In the past several decades,many new high-performance TE materials have been discovered to enrich the TE *** them,Cu_(2)−δSe-based TE materials,which are in line with the“phonon-liquid electron-crystal”concept,have sparked widespread interest due to the high TE figure-of-merit(ZT)and the combination of elements that are nontoxic and earth-abundant[2].In 2012,Liu et al.[3]reported a ZT of 1.5 at 1000 K in the stoichiometric Cu_(2)*** alloying S at the Se-site,the ZT was enhanced to around 2.0 at 1000 K[4].Via incorporating carbon nanotubes,the ZT was further enhanced to 2.4 at 1000 K[5].Moreover,Yang et al.[6]and Zhou et al.[7]reported that the ZT of Cu_(2)Se/BiCuSeO composites can reach 2.7–2.8 around 1000 K.

关键词： composites BiCuSeO performance

Effect of Modulus Heterogeneity on the Equilibrium Shape and Stress Field ofαPrecipitate in Ti-6Al-4V

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Computer Modeling in Engineering & Sciences 2024年第7期140卷 1017-1028页

作者： Di qiu Rongpei shi Materials Genome Institute Shanghai UniversityShanghai200444China School of Materials Science and Engineering Harbin Institute of TechnologyShenzhen518055China Shanghai Frontier Science Center of Mechanoinformatics Shanghai UniversityShanghai200444China Zhejiang Laboratory Hangzhou311100China

For media with inclusions(e.g.,precipitates,voids,reinforcements,and others),the difference in lattice parameter and the elastic modulus between the matrix and inclusions cause stress concentration at the *** stress fields depend on the inclusions’size,shape,and distribution and will respond instantly to the evolving *** study develops a phase-field model concerningmodulus *** effect of modulus heterogeneity on the growth process and equilibrium state of theαplate in Ti-6Al-4V during precipitation is ***αprecipitate exhibits strong anisotropy in shape upon cooling due to the interplay of the elastic strain and interfacial *** calculated orientation of the habit plane using the homogeneous modulus ofαphase shows the smallest deviation fromthat of the habit plane observed in the experiment,compared to the case where the homogeneous modulus ofβphase is *** addition,the equilibrium volume ofαphase within the systemusing homogeneousβmodulus exhibits the largest dependency on the applied *** stress fields across theα/βinterface are further calculated under the assumption of modulus heterogeneity and compared to those using homogeneous modulus of eitherαorβ*** study provides an essential theoretical basis for developing mechanics models concerning systems with heterogeneous structures.

关键词： Elastic heterogeneity habit plane stress field titanium phase-field simulation

A low-power Bluetooth-based wireless sensor network and its global confliction-solving impact localization method

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Chinese Journal of Aeronautics 2024年第1期37卷 153-161页

作者： Yuanjia WANG Lei qiu Qiyun XU Liming shi College of Aerospace Engineering Nanjing University of Aeronautics and AstronauticsNanjing 210016China Department of Electrical and Electronic Engineering University of EdinburghEdinburgh EH89YLUK

During the whole service lifetime of aircraft structures with composite materials,impacts are inevitable and can usually cause severe but barely visible *** the occurrences of impact are random and unpredictable,it is a hotspot direction to develop an online impact monitoring system that can meet strict limitations of aerospace applications including small size,light weight,and low power ***(PZT)sensor,being able to generate impact response signals with no external power and cover a large-scale structure with only a small amount of them,is a promising ***,for real systems,networks with multiple nodes are normally required to monitor large-scale structures in a global way to identify any impact localization confliction,yet the existing studies are mostly evaluated with single nodes instead of ***,in this paper,based on a new low-power node designed,a Bluetooth-based digital impact monitoring PZT sensor network is proposed for the first time with its global confliction-solving impact localization *** of the system as a network are researched and analyzed on a complex real aircraft wing box for a global confliction-solving impact localization,showing a satisfying high accuracy.

关键词： Bluetooth-based low-power design Confliction-solving evaluation Complex composites Piezoelectric sensors Wireless impact monitoring network

Boron nitride silicone rubber composite foam with low dielectric and high thermal conductivity

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Chinese Journal of Chemical Engineering 2024年第4期68卷 224-230页

作者： Shuilai qiu Hang Wu Fukai Chu Lei song College of Safety and Ocean Engineering China University of Petroleum-BeijingBeijing 102249China State Key Laboratory of Fire Science University of Science and Technology of ChinaHefei 230026China

Silicone rubber(SR)is widely used in the field of electronic packaging because of its low dielectric *** this work,the porosity of the SR was improved,and the dielectric constant of the SR foam was reduced by adding expanded microspheres(EM).Then,the thermal conductivity of the system was improved by combining the modified boron nitride(f-BN).The results showed that after the f-BN was added,the dielectric constant and dielectric loss were much lower than those of pure ***-sized modified boron nitride(f-mBN)improved the dielectric and thermal conductivity of the SR foam better than that of nano-sized modified boron nitride(f-nBN),but f-nBN improved the volume resistivity,tensile strength,and thermal stability of the SR better than *** the mass ratio of f-mBN and fnBN is 2:1,the thermal conductivity of the SR foam reaches the maximum value of 0.808 W·m^(-1)·K^(-1),which is 6.5 times that before the *** heat release rate and fire growth index are the lowest,and the improvement in flame retardancy is mainly attributed to the high thermal stability and physical barrier of f-BN.

关键词： Foam Composites Dielectric properties Thermal conductivity Mechanical properties Flame retardant

Satellite anomaly detection based on reconstruction discrepancy theory utilizing a new dual-branch reconstruction model

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Science China Technological Sciences 2024年第10期67卷 3294-3307页

作者： ZHAO HaoTian qiu shi LIU Ming CAO XiBin Research Center of Satellite Technology School of AstronauticsHarbin Institute of Technology

To enhance the accuracy of deep learning methods based on reconstruction discrepancy in satellite anomaly detection tasks, this study proposes a dual-branch reconstruction model(DBRM) and designs a comprehensive satellite anomaly detection framework around this model. Firstly, we introduce the temporal-channel mixer(TC-Mixer) module, which mainly comprises a self-attention layer for capturing long-range temporal dependencies in telemetry data, and two types of feed-forward networks(FFN) for extracting complex patterns in the temporal and channel dimension of telemetry data. This design endows the TC-Mixer module with robust capabilities for extracting complicated dependencies in telemetry data. Secondly, with the TC-Mixer module as the main component, we designed the DBRM. This model utilizes a shared latent representation layer, allowing the regeneration branch and forecasting branch of the DBRM to share most of the feature extraction network architecture. This approach significantly enhances the model's regression accuracy while reducing computational complexity. Thirdly, using the DBRM as the core network model, we devised a comprehensive satellite anomaly detection framework. This includes an anomaly criterion that considers the reconstruction discrepancy of both the regeneration and forecasting branches, the peak-over-threshold(POT) method for anomaly thresholding, and the MIC-based feature engineering method, etc. Finally, we conducted comparative experiments with several SOTA anomaly detection algorithms on two public and one private satellite anomaly detection datasets. The experimental results validate the effectiveness and superiority of our proposed method.

关键词： anomaly detection reconstruction discrepancy dual-branch reconstruction model (DBRM) satellite telemetry data time series

Hyperspectral Image Based Interpretable Feature Clustering Algorithm

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Computers, Materials & Continua 2024年第5期79卷 2151-2168页

作者： Yaming Kang PeishunYe Yuxiu Bai shi qiu School of Information Engineering Yulin UniversityYulin719000China Key Laboratory of Spectral Imaging Technology CAS Xi’an Institute of Optics and Precision MechanicsChinese Academy of SciencesXi’an710119China

Hyperspectral imagery encompasses spectral and spatial dimensions,reflecting the material properties of *** application proves crucial in search and rescue,concealed target identification,and crop growth *** is an important method of hyperspectral *** vast data volume of hyperspectral imagery,coupled with redundant information,poses significant challenges in swiftly and accurately extracting features for subsequent *** current hyperspectral feature clustering methods,which are mostly studied from space or spectrum,do not have strong interpretability,resulting in poor comprehensibility of the ***,this research introduces a feature clustering algorithm for hyperspectral imagery from an interpretability *** commences with a simulated perception process,proposing an interpretable band selection algorithm to reduce data *** this,amulti-dimensional clustering algorithm,rooted in fuzzy and kernel clustering,is developed to highlight intra-class similarities and inter-class *** optimized P systemis then introduced to enhance computational *** system coordinates all cells within a mapping space to compute optimal cluster centers,facilitating parallel *** approach diminishes sensitivity to initial cluster centers and augments global search capabilities,thus preventing entrapment in local minima and enhancing clustering *** conducted on 300 datasets,comprising both real and simulated *** results show that the average accuracy(ACC)of the proposed algorithm is 0.86 and the combination measure(CM)is 0.81.

关键词： Hyperspectral fuzzy clustering tissue P system band selection interpretable