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Simplified quantitative analysis method and its application in the insitu synthesized copper-based azide chips

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Defence Technology（防务技术） 2024年第2期32卷 309-316页

作者： Jie Ren Yunfeng Li Mingyu Li Xingyu Wu Jiabao wang qingxuan Zeng State Key Laboratory of Explosion and Technology Beijing Institute of TechnologyBeijing 100081China

Copper-based azide(Cu(N_(3))2 or CuN_(3),CA)chips synthesized by in-situ azide reaction and utilized in miniaturized explosive systems has become a hot research topic in recent years.However,the advantages of in-situ synthesis method,including small size and low dosage,bring about difficulties in quantitative analysis and differences in ignition capabilities of CA chips.The aim of present work is to develop a simplified quantitative analysis method for accurate and safe analysis of components in CA chips to evaluate and investigate the corresponding ignition ability.In this work,Cu(N_(3))2 and CuN_(3)components in CA chips were separated through dissolution and distillation by utilizing the difference in solubility and corresponding content was obtained by measuring N_(3)-concentration through spectrophotometry.The spectrophotometry method was optimized by studying influencing factors and the recovery rate of different separation methods was studied,ensuring the accuracy and reproducibility of test results.The optimized method is linear in range from 1.0-25.0 mg/L,with a correlation coefficient R^(2)=0.9998,which meets the requirements of CA chips with a milligram-level content test.Compared with the existing ICP method,component analysis results of CA chips obtained by spectrophotometry are closer to real component content in samples and have satisfactory accuracy.Moreover,as its application in miniaturized explosive systems,the ignition ability of CA chips with different component contents for direct ink writing CL-20 and the corresponding mechanism was studied.This study provided a basis and idea for the design and performance evaluation of CA chips in miniaturized explosive systems.

关键词： Copper-based azide chips Spectrophotometry Separation method Quantitative analysis Ignition ability

Impact localization of composite laminates based on weight function compensation localization algorithm of thin film sensors

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International Journal of Smart and Nano Materials 2023年第2期14卷 139-154页

作者： Ying wang Hongmei Li Shaowei Lu Xingmin Liu Wei Li Xiaoqiang wang Lu Zhang qingxuan wang College of Aerospace Engineering Shenyang Aerospace University(SAU)ShenyangChina College of Material Science and Engineering Shenyang Aerospace University(SAU)ShenyangChina

Composite structures are sensitive to impact damage in practical engineering.Electric resistance change method(ERCM)is an ideal technique for damage monitoring of composite structures.Due to the anisotropy of fiber-resin matrix composites,impact location monitoring is difficult,and research on impact location of fiber composite laminates(FRPs)is limited.A preparation method of MXene/CNT/CuNps thin film sensor is proposed.According to the modeling simulation and theoretical calculation,the resistance change characteristics of the thin film sensor are obtained,the relationship between the impact distance and the resistance change is established,and the sensor array is designed.A three-point localization algorithm and a weight function compensation localization algorithm are proposed,which can improve the imaging accuracy of the impact position.The impact point location was observed and analyzed using ultrasonic C-scan technology.The results show that the weight function compensation positioning algorithm can accurately locate the impact of the composite structure,and the error in the X direction is 7.1%,the error in the Y direction is 0.03%,which verifies the effectiveness of the method.

关键词： Electric resistance change method Mxene/CNT/CuNps film sensor damage localization Weighting function

The cytokine network involved in the host immune response to periodontitis

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International Journal of Oral Science 2019年第4期11卷 276-288页

作者： Weiyi Pan qingxuan wang Qianming Chen State Key Laboratory of Oral Diseases & National Clinical Research Center for Oral Diseases & Chinese Academy of Medical Sciences Research Unit of Oral Carcinogenesis and Management West China Hospital of Stomatology Sichuan University

Periodontitis is an inflammatory disease involving the destruction of both soft and hard tissue in the periodontal region.Although dysbiosis of the local microbial community initiates local inflammation,over-activation of the host immune response directly activates osteoclastic activity and alveolar bone loss.Many studies have reported on the cytokine network involved in periodontitis and its crucial and pleiotropic effect on the recruitment of specific immunocytes,control of pathobionts and induction or suppression of osteoclastic activity.Nonetheless,particularities in the stimulation of pathogens in the oral cavity that lead to the specific and complex periodontal cytokine network are far from clarified.Thus,in this review,we begin with an up-to-date aetiological hypothesis of periodontal disease and summarize the roles of cytokines in the host immune response.In addition,we also summarize the latest cytokine-related therapeutic measures for periodontal disease.

关键词： cytokine stimulation inflammation

混杂钢纤维超高性能混凝土轴拉力学性能及本构模型

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复合材料学报 2024年第1期41卷 383-394页

作者：王秋维梁林史庆轩西安建筑科技大学土木工程学院西安710055

通过单轴受拉试验,研究了平直型(短直、长直)和端钩钢纤维混掺的超高性能混凝土(Ultra-high performance concrete,UHPC)轴心受拉力学性能,基于试验结果分析了钢纤维掺量和混杂配比对UHPC抗拉强度、应变能力、韧性等的影响。结果表明:U... 详细信息

通过单轴受拉试验,研究了平直型(短直、长直)和端钩钢纤维混掺的超高性能混凝土(Ultra-high performance concrete,UHPC)轴心受拉力学性能,基于试验结果分析了钢纤维掺量和混杂配比对UHPC抗拉强度、应变能力、韧性等的影响。结果表明:UHPC轴拉试件发生多缝延性破坏,且宏观主裂缝的倾斜、弯曲程度随端钩纤维的混掺越发明显;混杂短直和端勾钢纤维UHPC的轴拉性能随着端勾纤维掺量的增大而显著提升,而混掺长直和端勾钢纤维UHPC的轴拉性能呈相反变化趋势;混杂钢纤维在UHPC受拉过程中呈现出逐级、分层次、相互作用的阻裂增韧特点,短直和端钩钢纤维掺量均为1.0vol%的UHPC轴拉力学性能最佳,其抗拉强度、应变能力和韧性同比单掺短直纤维试件分别提高28.2%、147%和31.1%。基于实测轴拉应力-应变曲线分析,提出了考虑纤维相互作用和纤维增强因子的混杂钢纤维UHPC轴拉本构模型,与相关试验曲线吻合良好,可用于预测UHPC受拉应力-应变关系。

关键词： UHPC 混杂钢纤维应力-应变曲线轴拉力学性能本构模型

自复位装配式RC框架结构基于能量平衡的抗震塑性设计方法

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建筑结构学报 2024年第6期45卷 192-202页

作者：马立成史庆轩王秋维王朋王斌西安建筑科技大学土木工程学院陕西西安710055 西安建筑科技大学结构工程与抗震教育部重点实验室陕西西安710055

为了解决装配式混凝土框架结构节点连接薄弱、损伤机制不可控、耗能能力不足、震后难以修复等问题,针对带有可控塑性铰(CPH)的自复位装配式混凝土框架结构(SC-PRCF),基于能量平衡的抗震设计理念,考虑自复位结构体系滞回行为与理想弹塑... 详细信息

为了解决装配式混凝土框架结构节点连接薄弱、损伤机制不可控、耗能能力不足、震后难以修复等问题,针对带有可控塑性铰(CPH)的自复位装配式混凝土框架结构(SC-PRCF),基于能量平衡的抗震设计理念,考虑自复位结构体系滞回行为与理想弹塑性结构体系的差异,以及结构上部楼层塑性发展不充分等因素,参照可恢复功能防震结构的四水准抗震设防目标,提出了SC-PRCF结构抗震塑性设计方法。并设计了一榀7层SC-PRCF结构,同时按照GB 50011—2010《建筑抗震设计规范》设计了一榀7层现浇混凝土框架(RCF)结构作为对比。通过动力弹塑性分析,验证了抗震塑性设计方法的有效性和SC-PRCF结构性能的优越性。研究结果表明:按照抗震塑性设计方法可使SC-PRCF结构满足“小震及中震不坏、大震可修复、可更换、巨震不倒塌”的抗震设防目标,同时可获得“强柱弱梁”的破坏模式,实现了渐进屈服耗能,使全楼层均能参与能量耗散,且能延长失效路径,避免出现薄弱层。

关键词：装配式混凝土框架结构自复位可控塑性铰塑性设计抗震性能残余变形

期刊论文支撑数据FAIR原则的应用评估与案例分析

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现代情报 2024年第2期44卷 17-29页

作者：刘桂锋王清炫韩牧哲江苏大学科技信息研究所江苏镇江212013 江苏大学图书馆江苏镇江212013

[目的/意义]FAIR原则在科技期刊的应用有助于增强期刊论文支撑数据的可发现、交互、共享与重用。评估FAIR实施情况有利于其推广实施,以期为我国期刊论文的支撑数据共享与重用提供有益参考。[方法/过程]本文在国外FAIR原则评估模型的基础... 详细信息

[目的/意义]FAIR原则在科技期刊的应用有助于增强期刊论文支撑数据的可发现、交互、共享与重用。评估FAIR实施情况有利于其推广实施,以期为我国期刊论文的支撑数据共享与重用提供有益参考。[方法/过程]本文在国外FAIR原则评估模型的基础上,综合考虑各模型的优势和指标设计特点,结合《数据分析与知识发现》期刊论文相关的科学数据特征,构建FAIR原则指标评价体系,基于该体系从4个维度分析调研结果,最后对中文期刊论文的支撑数据FAIR应用提出合理化建议与优化策略。[结果/结论]FAIR原则在期刊论文支撑数据的应用仍需进一步完善,科研人员的数据共享意识及对于FAIR原则的认知度远远不够,建议从宏观和微观两个层面推广FAIR原则及其实施,推动数据更加开放和可重用。

关键词： FAIR原则期刊论文支撑数据数据管理数据科学应用评估案例分析

Compliant substratum modulates vinculin expression in focal adhesion plaques in skeletal cells

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International Journal of Oral Science 2019年第2期11卷 151-159页

作者： Chenchen Zhou qingxuan wang Demao Zhang Linyi Cai Wei Du Jing Xie State Key Laboratory of Oral Diseases & National Clinical Research Center for Oral Diseases & West China Hospital of Stomatology Sichuan University

The biophysical properties of the extracellular matrix (ECM) dictate tissue-specific cell behaviour.In the skeleton system,bone shows the potential to adapt its architecture and contexture to environmental rigidity via the bone remodelling process,which involves chondrocytes,osteoblasts,osteoclasts,osteocytes and even peripheral bone marrow-derived stem/stromal cells (BMSCs).In the current study,we generated stiff (~1 014 ± 56) kPa,Young’s modulus) and soft (~46 ± 11) kPa silicon-based elastomer polydimethylsiloxane (PDMS) substrates by mixing curing agent into oligomeric base at 1:5 and 1:45 ratios,respectively,and investigated the influence of substrate stiffness on the cell behaviours by characterizing cell spreading area,cell cytoskeleton and cell adhesion capacity.The results showed that the cell spreading areas of chondrocytes,osteoblasts,osteoclasts,osteocytes and BMSCs were all reduced in the soft substrate relative to those in the stiff substrate.F-actin staining confirmed that the cytoskeleton was also changed in the soft group compared to that in the stiff group.Vinculin in focal adhesion plaques was significantly decreased in response to soft substrate compared to stiff substrate.This study establishes the potential correlation between microenvironmental mechanics and the skeletal system,and the results regarding changes in cell spreading area,cytoskeleton and cell adhesion further indicate the important role of biomechanics in the cell-matrix interaction.

关键词： extracellular matrix(ECM) BMSCs polydimethylsiloxane(PDMS)

拼接成型UHPC免拆模板钢筋混凝土柱的抗震性能

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哈尔滨工业大学学报 2024年第1期56卷 103-116页

作者：王朋尤学辉黄杰史庆轩陶毅王秋维西部绿色建筑国家重点实验室(西安建筑科技大学) 西安710055 西安建筑科技大学土木工程学院西安710055 结构工程与抗震教育部重点实验室(西安建筑科技大学) 西安710055

为研究超高性能混凝土(UHPC)免拆模板钢筋混凝土(URC)柱的抗震性能,选取UHPC免拆模板拼接方式和表面处理方式为试验设计参数,制作并完成了9个URC柱和1个钢筋混凝土(RC)柱的拟静力加载试验。模板拼接方式为螺栓加角钢连接、螺栓连接和环... 详细信息

为研究超高性能混凝土(UHPC)免拆模板钢筋混凝土(URC)柱的抗震性能,选取UHPC免拆模板拼接方式和表面处理方式为试验设计参数,制作并完成了9个URC柱和1个钢筋混凝土(RC)柱的拟静力加载试验。模板拼接方式为螺栓加角钢连接、螺栓连接和环氧树脂砂浆连接;表面处理方式为光面处理、气泡膜印花处理和设肋处理,通过拟静力试验研究了模板拼接方式及表面处理方式对该类柱抗震性能的影响。此外,基于平截面假定,提出了URC柱的正截面偏压承载力计算式。结果表明:峰值荷载前,UHPC模板与核心混凝土黏结面无明显破坏,URC柱表现出良好的整体性,尤其是采用螺栓加角钢连接的URC柱,即使加载至极限位移时,也没有发生界面黏结失效破坏;与普通RC柱相比,URC柱的承载力提高了6.4%~43.3%,延性提高了11.4%~48.7%,耗能能力提高了27.7%~85.3%;三种连接方式中,采用螺栓加角钢连接的URC柱承载力最高,连接最可靠。最后,基于平截面假定提出的公式计算值与试验值吻合较好,可为工程应用提供参考。

关键词：超高性能混凝土免拆模板钢筋混凝土柱抗震性能承载力计算

铅黏弹性阻尼器增强钢管约束钢筋混凝土柱节点抗震性能研究

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振动与冲击 2024年第6期43卷 238-247页

作者：王秋维景烜光史庆轩李雪梅西安建筑科技大学土木工程学院西安710055 西安建筑科技大学结构工程与抗震教育部重点实验室西安710055

针对钢管约束钢筋混凝土(steel tubed reinforced concrete,STRC)柱节点抗震性能薄弱的现状,提出采用改良的铅黏弹性阻尼器进行增强。基于ABAQUS工作平台对铅黏弹性阻尼器试件建立有限元模型,将数值计算所得滞回和骨架曲线、耗能性能及... 详细信息

针对钢管约束钢筋混凝土(steel tubed reinforced concrete,STRC)柱节点抗震性能薄弱的现状,提出采用改良的铅黏弹性阻尼器进行增强。基于ABAQUS工作平台对铅黏弹性阻尼器试件建立有限元模型,将数值计算所得滞回和骨架曲线、耗能性能及疲劳性能与试验结果进行对比,两者吻合较好。在此基础上探讨了铅芯直径、铅芯布置形式及复合黏弹性体厚度比值对铅黏弹性阻尼器力学性能的影响。结果表明:相较于扇形铅黏弹性阻尼器,改良后的四边形铅黏弹性阻尼器表现出更好的力学性能;随着铅芯直径的增大,阻尼器的耗能能力指标均得到大幅提高;建议铅芯个数取2个,铅芯面积与复合黏弹性层面积比值取6%~8%,复合黏弹性体厚度比值约为0.67。建立不同布置方案的铅黏弹性阻尼器增强STRC柱节点试件模型,对其破坏形态、滞回特性和箍筋应力进行对比分析,给出合理的布置方案,为实际工程提供参考。

关键词：钢管约束钢筋混凝土(STRC)柱铅黏弹性阻尼器数值分析抗震性能