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Tuning heterogeneous microstructures to enhance mechanical properties of nano-TiN particle reinforced Haynes 230 composites by laser powder bed fusion

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Rare Metals 2024年第9期43卷 4548-4565页

作者： Wen-Jie liu Hui li qian-xing Yin He-Jun Du School of Power and Mechanical Engineering Wuhan University The Institute of Technological Sciences Wuhan University School of Mechanical&Aerospace Engineering Nanyang Technological University

Laser powder bed fusion(LPBF) is considered to be one of the most promising additive manufacturing technologies for producing components with geometries and high geometrical precision that are unattainable by traditional technologies. The superalloy exhibits exceptional mechanical and high-temperature performances,rendering it a prime candidate for advanced aero-engine applications. Despite the high demand for LPBF-manufactured superalloys, the superalloy is one of the materials manufactured difficultly by LPBF due to their large laser absorptivity fluctuation, poor molten pool stability and sharp temperature gradient. Hence, superalloys are characterized by severe pores, undesirable coarse columnar grains and poor mechanical properties. In this work, the effect of nano-Ti N particles on defects, molten pool characteristics and microstructure and performance of the composites were investigated. The 4.5 wt% Ti N/Haynes230 samples exhibited exceptional nanohardness and elastic modulus with maximum values reaching 5.53 GPa and 240.03 GPa, respectively. These superior mechanical properties were attributed to the combined effects of spatter and gas pore inhibition, grain refinement and duplex nanophases strengthening. Moreover, the stability of molten pool was enhanced, and spatter was effectively suppressed by adding nano-Ti N particles, while grain refinement and columnar to equiaxed transitions were promoted. Furthermore, the matrix exhibited a high dislocation density due to a significant hindrance of dislocation movement caused by massive nano-phases(e.g., Ti N and M23C6), resulting in the formation of extensive dislocation tangles and *** work offers novel insights into the role of nanoparticles reinforced superalloy composites by LPBF.

关键词： Composites Laser powder bed fusion Mechanical properties Microstructure Molten pool characteristics

Refinement modeling and verification of secure operating systems for communication in digital twins

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Digital Communications and Networks 2024年第2期10卷 304-314页

作者： Zhenjiang qian Gaofei Sun Xiaoshuang xing Gaurav Dhiman School of Computer Science and Engineering Changshu Institute of TechnologySuzhou215500China University Centre for Research and Development Department of Computer Science and EngineeringChandigarh UniversityMohali140413India Department of Computer Science and Engineering Graphic Era Deemed to be UniversityDehradun248002India

In traditional digital twin communication system testing,we can apply test cases as completely as possible in order to ensure the correctness of the system implementation,and even then,there is no guarantee that the digital twin communication system implementation is completely *** verification is currently recognized as a method to ensure the correctness of software system for communication in digital twins because it uses rigorous mathematical methods to verify the correctness of systems for communication in digital twins and can effectively help system designers determine whether the system is designed and implemented *** this paper,we use the interactive theorem proving tool Isabelle/HOL to construct the formal model of the X86 architecture,and to model the related assembly *** verification result shows that the system states obtained after the operations of relevant assembly instructions is consistent with the expected states,indicating that the system meets the design expectations.

关键词： Theorem proving Isabelle/HOL Formal verification System modeling Correctness verification

Structural and chemical transformations of CuZn alloy nanoparticles under reactive redox atmospheres:An in situ TEM study

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Nano Research 2024年第7期17卷 6265-6273页

作者： Shengnan Yue qian li Chaobin Zeng Alexander Klyushin Ramzi Farra Marc-Georg Willinger xing Huang College of Chemistry Fuzhou UniversityFuzhou 350108China Qingyuan Innovation Laboratory Quanzhou 362801China Hitachi High-Tech Scientific Solutions(Beijing)Co. Ltd.Beijing 100015China MAX IV Laboratory Lund UniversityBox 11822100 LundSweden Department of Inorganic Chemistry Fritz-Haber Institute of Max Planck SocietyBerlin 14195Germany Department of Chemistry Technical University of MunichGarching 85748Germany

Alloying metals to form intermetallics has been proven effective in tuning the chemical properties of metal-based ***,intermetallic alloys can undergo structural and chemical transformations under reactive conditions,leading to changes in their catalytic *** and understanding these transformations are crucial for establishing relevant structureperformance relationships and for the rational design of alloy-based *** this work,we used CuZn alloy nanoparticles(NPs)as a model material system and employed in situ transmission electron microscopy(TEM)to investigate the structural and chemical changes of CuZn NPs under H_(2),O_(2)and their *** results show how CuZn NPs undergo sequential transformations in the gas mixture at elevated temperatures,starting with gradual leaching and segregation of Zn,followed by oxidation at the NP *** remaining copper at the core of particles can then engage in dynamic behavior,eventually freeing itself from the zinc oxide *** structural dynamics arises from an oscillatory phase transition between Cu and Cu_(2)O and is correlated with the catalytic water formation,as confirmed by in situ mass spectrometry(MS).Under pure H_(2)or O_(2)atmosphere,we observe different structural evolution pathways and final chemical states of CuZn NPs compared to those in the gas *** results clearly demonstrate that the chemical state of alloy NPs can vary considerably under reactive redox atmospheres,particularly for those containing elements with distinct redox properties,necessitating the use of in situ or detailed ex situ characterizations to gain relevant insights into the states of intermetallic alloy-based catalysts and structure-activity relationships.

关键词： In situ transmission electron microscopy(TEM) CuZn alloy structural and chemical transformations redox atmosphere

Blast damage zone strength reduction method for deep cavern excavation and its application

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Frontiers of Structural and Civil Engineering 2024年第2期18卷 236-251页

作者： Tianzhi YAO Zuguo MO li qian Yunpeng GAO Jianhai ZHANG Xianglin xing Enlong liU Ru ZHANG State Key Laboratory of Hydraulics and Mountain River Engineering College of Water Resources and HydropowerSichuan UniversityChengdu 610065China Power China Chengdu Engineering Corporation limited Chengdu 610072China

The drill and blast(D&B)method is widely used to excavate underground spaces,but explosions generally cause damage to the ***,no blast simulation method can provide computational accuracy and *** this paper,a blast equivalent simulation method called the blast damage zone strength reduction(BDZSR)method is *** method first calculates the range of the blast-induced damage zone(BDZ)by formulae,then reduces the strength and deformation parameters of the rock within the BDZ ahead of excavation,and finally calculates the excavation damage zone(EDZ)for the D&B method by numerical *** method combines stress wave attenuation,rock damage criteria and stress path variation to derive the BDZ depth calculation *** formulae consider the initial geo-stress,and the reliability is verified by numerical *** calculation of BDZ depth with these formulae allows the corresponding numerical simulation to avoid the time-consuming dynamic calculation process,thus greatly enhancing the calculation *** method was applied to the excavation in Jinping Class II hydropower station to verify its *** results show that the BDZSR method can be applied to blast simulation of underground caverns and provide a new way to study blast-induced damage.

关键词： attenuation of stress wave deep-buried underground building drill and blast in situ stress

Thermal Entanglement of a Two-Qubit XXZ Heisenberg Chain with Dzialoshinski-Moriya Interaction

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Communications in Theoretical Physics 2009年第11期52卷 817-819页

作者： qian li FANG Jian-xing School of Physical Science and Technology Suzhou University Suzhou 215006 China

The effect of Dzialoshinski-Moriya(DM)interaction on thermal entanglement of a two-qubit XXZ spin chainin a homogenous magnetic field is *** is found that the DM interaction can enhance thermal *** D is large enough,t... 详细信息

关键词： DM相互作用热纠缠态量子位自旋链海森堡强磁场

Work-function-induced interfacial electron redistribution of MoO_(2)/WO_(2) heterostructures for high-efficiency electrocatalytic hydrogen evolution reaction

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Rare Metals 2024年第2期43卷 489-499页

作者： Tong-Fei li Jing li Lu-Ping Zhang Jia-Wei Ke Meng-xing Fan li-Fang Zhang Cheng-Wei Deng Yi Sun Tao qian Cheng-lin Yan School of Chemistry and Chemical Engineering Nantong UniversityNantong226019China Jiangsu Key Laboratory of New Power Batteries Jiangsu Collaborative Innovation Centre of Biomedical Functional MaterialsSchool of Chemistry and Materials ScienceNanjing Normal UniversityNanjing210023China Aerospace Hydrogen Energy Technology(Shanghai)Co.Ltd. Shanghai201800China Key Laboratory of Core Technology of High Specific Energy Battery and Key Materials for Petroleum and Chemical Industry College of EnergySoochow UniversitySuzhou215006China light Industry Institute of Electrochemical Power Sources Suzhou215006China

The engineering of the electronic configurations of active sites,together with the production of more accessible active sites through heterostructure design,has been established as a forceful methodology for boosting water electrolysis ***,a facile approach is developed to fabricate well-dispersed MoO_(2) and WO_(2) nanoparticles with abundant heterointerfaces entrapped in N,P-doped carbon nanofibers(referred to as MoO_(2)/WO_(2)@N,P-CNFs hereafter)as hydrogen evolution reaction(HER)electrocatalysts in alkaline and acidic *** spectroscopic analyses and theoretical findings manifest that the heterointerface formed by the work function modulation of MoO_(2)/WO_(2) triggers the spontaneous electron redistribution from MoO_(2)to WO_(2) and a built-in electric field,which is essential to promote water adsorption,optimize the H-intermediate adsorption energy,result in the enhanced charge transfer efficiency,and ultimately increase the intrinsic HER ***,the intimate confinement of MoO_(2)/WO_(2) heterostructures in the porous carbon substrate can restrain the active sites from unfavorable coarsening and detachment,thus ensuring facilitated HER kinetics and outstanding structural *** a result,MoO_(2)/WO_(2)@N,P-CNFs exhibit superior catalytic HER performance in acidic and basic solutions,requiring 118 and 95 mV overpotentials to achieve 10 mA·cm^(−2),respectively,surpassing a number of reported non-noble metal-based *** work provides guidelines for the rational design and construction of special metallic heterocomponents with optimized interfacial electronic structure for various electrochemical technologies.

关键词： Electrospinning MoO_(2)/WO_(2) heterostructure Work function Hydrogen evolution reaction

Style-conditioned music generation with Transformer-GANs

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Frontiers of Information Technology & Electronic Engineering 2024年第1期25卷 106-120页

作者： Weining WANG Jiahui li Yifan li Xiaofen xing School of Electronic and Information Engineering South China University of TechnologyGuangzhou 510600China

Recently,various algorithms have been developed for generating appealing ***,the style control in the generation process has been somewhat *** style refers to the representative and unique appearance presented by a musical work,and it is one of the most salient qualities of *** this paper,we propose an innovative music generation algorithm capable of creating a complete musical composition from scratch based on a specified target style.A style-conditioned linear Transformer and a style-conditioned patch discriminator are introduced in the *** style-conditioned linear Transformer models musical instrument digital interface(MIDI)event sequences and emphasizes the role of style ***,the style-conditioned patch discriminator applies an adversarial learning mechanism with two innovative loss functions to enhance the modeling of music ***,we establish a discriminative metric for the first time,enabling the evaluation of the generated music’s consistency concerning music *** objective and subjective evaluations of our experimental results indicate that our method’s performance with regard to music production is better than the performances encountered in the case of music production with the use of state-of-the-art methods in available public datasets.

关键词： Music generation Style-conditioned Transformer Music emotion

Unraveling high efficiency multi-step sodium storage and bidirectional redox kinetics synergy mechanism of cobalt-doping vanadium disulfide anode

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Journal of Energy Chemistry 2024年第7期94卷 148-157页

作者： Enzhi li Mingshan Wang Yuanlong Feng lin Yang qian li Zhenliang Yang Junchen Chen Bo Yu Bingshu Guo Zhiyuan Ma Yun Huang Jiangtao liu xing li School of New Energy and Materials Southwest Petroleum UniversityChengdu 610500SichuanChina Institute of Materials China Academy of Engineering PhysicsMianyang 621908SichuanChina State Key Laboratory of Advanced Chemical Power Sources Guizhou Meiling Power Sources Co.Ltd.Zunyi 563003GuizhouChina school of Chemistry and Chemical Engineering Harbin Institute of TechnologyHarbin 150001HeilongjiangChina

Sodium-based storage devices based on conversion-type metal sulfide anodes have attracted great atten-tion due to their multivalent ion redox reaction ***,they also suffer from sodium polysul-fides(NaPSs)shuttling problems during the sluggish Na^(+) redox process,leading to"voltage failure"and rapid capacity ***,a metal cobalt-doping vanadium disulfide(Co-VS_(2))is proposed to simulta-neously accelerate the electrochemical reaction of VS_(2) and enhance the bidirectional redox of soluble *** is found that the strong adsorption of NaPSs by V-Co alloy nanoparticles formed in situ during the conversion reaction of Co-VS_(2) can effectively inhibit the dissolution and shuttle of NaPSs,and ther-modynamically reduce the formation energy barrier of the reaction path to effectively drive the complete conversion reaction,while the metal transition of Co elements enhances reconversion kinetics to achieve high ***,Co-VS_(2) also produce abundant sulfur vacancies and unsaturated sulfur edge defects,significantly improve ionic/electron diffusion ***,the Co-VS_(2) anode exhibits ultrahigh rate capability(562 mA h g^(-1) at 5 A g^(-1)),high initial coulombic efficiency(~90%)and 12,000 ultralong cycle life with capacity retention of 90%in sodium-ion batteries(SIBs),as well as impressive energy/power density(118 Wh kg^(-1)/31,250 W kg^(-1))and over 10.000 stable cycles in sodium-ion hybrid capacitors(SIHCs).Moreover,the pouch cell-type SIHC displays a high-energy density of 102 Wh kg^(-1) and exceed 600 stable *** work deepens the understanding of the electrochemical reaction mechanism of conversion-type metal sulfide anodes and provides a valuable solution to the shuttlingofNaPSs inSIBsandSIHCs.

关键词： Sodium-ionbatteries Sodium-ion hybrid capacitors Pouch cells Vanadium disulfide Shuttle effect

Cascade equilibrium stage relaxation method by introducing equilibrium efficiency parameter

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Chinese Journal of Chemical Engineering 2024年第2期66卷 145-156页

作者： Xuepu Cao Shengkun Jia xing qian Yiqing Luo Xigang Yuan College of Chemical and Pharmaceutical Hebei University of Science&TechnologyShijiazhuang 050018China School of Chemical Engineering and Technology State Key Laboratory of Chemical EngineeringTianjin UniversityTianjin 300072China College of Information Science and Technology Beijing University of Chemical TechnologyBeijing 100029China

Optimizing multistage processes,such as distillation or absorption,is a complex mixed-integer nonlinear programming(MINLP)*** integer into continuous variables and solving the easier nonlinear programming(NLP)problem is an optimization idea for the multistage *** this article,we propose a relaxation method based on the efficiency *** the efficiency parameter is 1or 0,the proposed model is equivalent to the complete existence or inexistence of the equilibrium *** non-integer efficiency represents partial existence.A multi-component absorption case shows a natural penalty for non-integer efficiency,which can assist the efficiency parameter converging to 0 or ***,its penalty is weaker than the existing relaxation models,such as the bypass efficiency *** a simple distillation case,we show that this property can weaken the nonconvexity of the optimization problem and increase the probability of obtaining better optimization results.

关键词： Mathematical modeling Absorption Distillation Optimization