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On the microstructure and texture evolution in 17-4 PH stainless steel during laser powder bed fusion: Towards textural design

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Journal of Materials Science & Technology 2022年第22期117卷 183-195页

作者： M.S.Moyle n.Haghdadi X.Z.Liao S.P.ringer S.Primig School of Materials Science&Engineering UNSW SydneyNSW 2052Australia Australian Centre for Microscopy&Microanalysis The University of SydneyNSW 2006Australia School of Aerospace Mechanical and Mechatronic EngineeringThe University of SydneyNSW 2006Australia

Additive Manufacturing (AM) of metals allows the production of parts with complex designs, offeringadvanced properties if the evolution of the texture can be controlled. 17-4 precipitation hardening (PH)stainless steel is a high strength, high corrosion resistance alloy used in a range of industries suitable forAM, such as aerospace and marine. Despite 17-4 PH being one of the most common steels for AM, thereare still gaps in the understanding of its AM processing–structure relationships. These include the natureof the matrix phase, as well as the development of texture through AM builds under different processingconditions. We have investigated how changing the laser power and scanning strategy affects the microstructure of 17-4 PH during laser powder bed fusion. It is revealed that the matrix phase is δ-ferritewith a limited austenite presence, mainly in regions of the microstructure immediately below melt *** fraction is independent of the printing pattern and laser power. However, reducing the timebetween adjacent laser passes during printing results in an increase in the austenite volume *** effect of the higher laser power, as well as additional remelting within the printing strategy, isan increase in the average grain size by epitaxial ferrite grain growth across multiple build layers andthe development of a mosaic type microstructure. Changes to the scanning strategy have significant impacts on the textures observed along the build direction, while (100) texture along the scanning directionis observed consistently. Mechanisms for texture formation and the mosaic structure are proposed thatpresents a pathway to the design of texture via AM process control.

关键词： Additive manufacturing 17-4 PH stainless steel Microstructure Texture

Electrode-induced impurities in tin halide perovskite solar cell material CsSnBr_(3) from first principles

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npj Computational Materials 2021年第1期7卷 555-563页

作者： Yuhang Liang Xiangyuan Cui Feng Li Catherine Stampfl Simon P.ringer Rongkun Zheng School of Physics The University of SydneyNew South Wales 2006Australia School of Aerospace Mechanical and Mechatronic EngineeringThe University of SydneyNew South Wales 2006Australia

All-inorganic lead-free CsSnBr_(3)is attractive for applications in solar cells due to its nontoxicity and stability,but the device performance to date has been *** the intrinsic properties,impurities induced from electrodes may significantly influence the device ***,we systematically studied the stability,transition energy levels,and diffusion of impurities from the most commonly used electrodes(Au,Ag,Cu,graphite,and graphene)in CsSnBr_(3)based on density functional theory *** results reveal that,whereas graphite and graphene electrodes exhibit negligible influence on CsSnBr_(3)due to the relatively high formation energies for carbon impurities in CsSnBr_(3),atoms from the metal electrodes can effectively diffuse into CsSnBr_(3)along interstice and form electrically active impurities in CsSnBr_(3).In this case,a significant amount of donor interstitial impurities,such as Agti,Cuti,and Auti,will be formed under p-type conditions,whereas the Sn-site substitutional acceptor impurities,namely Au_(Sn)^(2-),Ag_(Sn)^(2-),and Cu_(Sn)^(2-),are the dominant impurities,especially under n-type *** particular,except for Auti,all these major impurities from the metal electrodes act as nonradiative recombination centers in CsSnBr_(3)and significantly degrade the device *** work highlights the distinct behaviors of the electrode impurities in CsSnBr_(3)and their influence on the related devices and provides valuable information for identifying suitable electrodes for optoelectronic applications.

关键词： stability perovskite halide

Microstructural properties of over-doped Gan-based diluted magnetic semiconductors grown by MOCVD

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Journal of Semiconductors 2012年第7期33卷 16-19页

作者：陶志阔张荣修向前崔旭高李丽李鑫谢自力郑有炓郑荣坤 Simon P ringer Key Laboratory of Advanced Photonic and Electronic Materials School of Electronic Science and EngineeringNanjing University College of Electronic Science and Engineering Nanjing University of Posts and Telecommunications Australia Key Center for Microscopy and Microanalysis University of Sydney

We have grown transition metal （Fe, Mn） doped Gan thin films on c-oriented sapphire by metal-organic chemical vapor deposition. By varying the flow of the metal precursor, a series of samples with different ion con- centrations are synthesized. Microstructural properties are characterized by using a high-resolution transmission electron microscope. For Fe over-doped Gan samples, hexagonal Fe3n clusters are observed with Fe3n （0002） parallel to Gan （0002） while for Mn over-doped Gan, hexagonal Mn6n2.58 phases are observed with Mn6n2.58（0002） parallel to Gan （0002）. In addition, with higher concentration ions doping into the lattice matrix, the partial lattice orientation is distorted, leading to the tilt orGan （0002） planes. The magnetization of the Fe over-doped Gan sam- ple is increased, which is ascribed to the participation of ferromagnetic iron and Fe3n. The Mn over-doped sample displays very weak ferromagnetic behavior, which probably originates from the Mn6n2.58.

关键词： MOCVD DMS high-resolution TEM

Serotonin type 3 receptor subunit gene polymorphisms associated with psychosomatic symptoms in irritable bowel syndrome:A multicenter retrospective study

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World Journal of Gastroenterology 2022年第21期28卷 2334-2349页

作者： Sabrina Berens Yuanjun Dong nikola Fritz Jutta Walstab Mauro D'Amato Tenghao Zheng Verena Wahl Felix Boekstegers Justo Lorenzo Bermejo Cristina Martinez Stefanie Schmitteckert Egbert Clevers Felicitas Engel Annika Gauss Wolfgang Herzog Robin Spiller Miriam Goebel-Stengel Hubert Mönnikes Viola Andresen Frieling Thomas Jutta Keller Christian Pehl Christoph Stein-Thöringer Gerard Clarke Timothy G Dinan Eamonn M Quigley Gregory Sayuk Magnus Simrén Jonas Tesarz Gudrun Rappold Lukas van Oudenhove Rainer Schaefert Beate niesler Department of General Internal Medicine and Psychosomatics University Hospital HeidelbergHeidelberg 69120Germany Department of Human Molecular Genetics Institute of Human GeneticsUniversity of HeidelbergHeidelberg 69120Germany Department of General Internal Medicine and Psychosomatics Internal Medicine IIUniversity Hospital HeidelbergHeidelberg 69120Germany Department of Human Molecular Genetics University of HeidelbergHeidelberg 69120Germany Gastrointestinal Genetics Lab CIC bioGUNE-BRTADerio 48160Spain IKERBASQUE Basque Foundation for ScienceBilbao 48001Spain Unit of Clinical Epidemiology Department of Medicine SolnaKarolinska InstitutetStockholm 17177Sweden Institute of Medical Biometry and Informatics Heidelberg UniversityHeidelberg 69120Germany Lleida Institute for Biomedical Research Dr.PifarréFoundation(IRBLleida) Av.Alcalde Rovira RoureLleida 25198Spain Department of Clinical and Experimental Medicine Translational Research Center for Gastrointestinal DisordersKU LeuvenLeuven 3000Belgium Department of Gastroenterology Infectious Diseases and IntoxicationsUniversity of HeidelbergHeidelberg 69120Germany Department of General Internal Medicine and Psychosomatics Heidelberg UniversityHeidelberg 69120Germany nottingham Digestive Diseases Centre University of NottinghamNottingham NG72QLUnited Kingdom Helios Klinikum Rottweil Rottweil 78628Germany Department of Medicine Institute of Neurogastroenterology(H.M.)Martin-Luther-HospitalBelin 14193Germany Israelitisches Krankenhaus in Hamburg Hamburg 22297Germany Internal Medicine II Helios Klinikum KrefeldKrefeld 47805Germany Israelitisches Krankenhaus Hamburg Hamburg 22297Ghana Krankenhaus Vilsbiburg Vilsbiburg 84137Germany Division of Microbiome and Cancer German Cancer Research Center(DKFZ)Heidelberg 69120Germany Department of Psychiatry and neurobehavioral Science University College CorkCork T23Ireland Medicine in Digestive Disorders Department of MedicineLynda K.and David M.Underwood Center for Digestive DisordersHou

BACKGROUnD Single-nucleotide polymorphisms(SnPs)of the serotonin type 3 receptor subunit(HTR3)genes have been associated with psychosomatic symptoms,but it is not clear whether these associations exist in irritable bowel syndrome(IBS).AIM To assess the association of HTR3 polymorphisms with depressive,anxiety,and somatization symptoms in individuals with *** In this retrospective study,623 participants with IBS were recruited from five specialty centers in Germany,Sweden,the United States,the United Kingdom,and ***,anxiety,and somatization symptoms and sociodemographic characteristics were *** functional SnPs—HTR3A c.-42C>T,HTR3B c.386A>C,HTR3C c.489C>A,and HTR3E c.*76G>A—were genotyped and analyzed using the dominant and recessive *** also performed separate analyses for sex and IBS *** scores were calculated as the number of minor alleles of the SnPs *** impact of HTR3C c.489C>A was tested by radioligand-binding and calcium influx *** Depressive and anxiety symptoms significantly worsened with increasing numbers of minor HTR3C c.489C>A alleles in the dominant model(F_(depressive)=7.475,P_(depressive)=0.006;F_(anxiety)=6.535,P_(anxiety)=0.011).A higher SnP score(range 0-6)was linked to a worsened depressive symptoms score(F=7.710,P-linear trend=0.006)in *** potential relevance of the HTR3C SnP was corroborated,showing changes in the expression level of 5-HT3AC variant *** We have provided the first evidence that HTR3C c.489C>A is involved in depressive and anxiety symptoms in individuals with *** SnP score indicated that an increasing number of minor alleles is linked to the worsening of depressive symptoms in IBS.

关键词： Irritable bowel syndrome 5-HT3 receptor subunit gene polymorphisms Single-nucleotide polymorphism score Depression Anxiety Somatization

Development of Low Carbon Microalloyed High Strength Ultra-Thin Cast Strip Products Produced by the Castrip~ Process With Excellent Strength-Ductility Properties

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Journal of Iron and Steel Research(International) 2011年第S1期18卷 846-850页

作者： C.R. Killmore K.R. Carpenter H.R. Kaul D.G. Edelman J.M. Cairney S.P. ringer J.G. Williams P.C. Campbell W.n. Blejde BlueScope Steel Five Islands Road Pt Kembla 2500 Australia nucor Steel Indiana 4537 S. nucor Rd. Crawfordsville In 47933 USA Australian Centre for Microscopy and Microanalysis University of Sydney NSW 2006 Australia Castrip LLC1915 Rexford Rd. Charlotte nC 28211 USA

The CASTRIP* process produces a range of high strength Ultra-thin Cast Strip (UCS) products (380-550 MPa) in thicknesses between 0.9 mm and 1.5 mm, which is very challenging to produce via conventional hot and cold rolled processing routes. The twin roll CASTRIP process fully exploits the hardenability and strengthening potential of nb in a low C-Mn-nb-V microalloyed steel type. Significant microstructural strengthening from solute nb was obtained, even at low microalloying levels, as well as modest Mn additions, through enhancing the hardenability and further strengthening was obtained in coated products by exploiting age hardening during processing on a continuous hot dip galvanising line. Atom probe tomography and TEM determined that nb was retained in solid solution and subsequent age hardening resulted from the formation of nb and V rich nanosized particles. Age hardening was achieved without loss of ductility producing galvanised strip with an excellent strength-ductility combination (Y.S. >600 MPa, T.E. >10%).

关键词： strip casting microalloying niobium ntom probe tomography age hardening high strength CASTRIP Process

Assessment of Mg(OH)_(2)/TiO_(2) coating in the Mg-Ca-Zn alloy for improved corrosion resistance and antibacterial performance

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Journal of Magnesium and Alloys 2023年第1期11卷 361-378页

作者： Leonardo Hernández Jesús Ramón-Sierra Montserrat Soria-Castro Ángel Bacelis Geonel Rodríguez-Gattorno Elizabeth Ortiz-Vázquez Gloria Acosta Applied Physics Department Center for Research and Advanced Studies of the National Polytechnic Institute(CINVESTAV-IPN)Carr.Ant.a Progreso km.6C.P.97310MeridaYucatanMexico Tecnológico nacional de México/Instituto Tecnológico de Mérida.Av.Tecnológico s/n Km.4.5 ant.Carr.Mérida-Progreso C.P.97118MéridaYucatánMéxico Facultad de Química Universidad Nacional Autónoma de México(UNAM)Av.Universidad 3000C.P.04510CoyoacánCDMXMéxico

The high activity of metallic magnesium and alloys limits its potential in biomedical applications;in recent years,extensive efforts have been devoted to modulating this *** this work,we present Mg(OH)_(2) and TiO_(2)barrier coatings to reduce the degradation of magnesium alloy(Mg-Ca-Zn)*** coatings were deposited by the anodization method and the spin-coating technique,*** anodized layer was coated with TiO_(2)generated from the hydrolysis of 3%weight of TTIP(Ti[OCH(CH_(3))_(2)]_(4),Titanium(IV)isopropoxide)in 2-Propanol deposited by the spin-coating *** the degradation in.ringer’s solution by electrochemical impedance spectroscopy and OCP revealed a 98%reduction in pittings in uncoated samples after 14 days of *** p H measurements revealed that the TiO_(2)coating reduced the alkalization of the physiological environment,keeping the pH at 6.0 *** vitro studies of two types of bacteria(*** and ***)exhibited zones of inhibition in the agar and activity bactericidal(kill time test).The mechanisms behind the improved degradation resistance and enhanced antibacterial activity are presented and discussed *** modification with Mg(OH)_(2)/TiO_(2)coatings is a promising strategy to control the biodegradation of magnesium implants for bone regeneration.

关键词： Magnesium alloy EIS Mg(OH)_(2) TiO_(2) Antibacterial coatings

Evaluation of various solutions for small bowel graft preservation

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World Journal of Gastroenterology 1998年第2期4卷 48-51页

作者： Li YS Li JS Li n Jiang ZW Zhao YZ Li nY Liu Fn Institute of General Surgery Jinling Hospital Nanjing 210002 Jiangsu Province China Department of Pathology Jinling Hospital Nanjing 210002 Jiangsu Province China

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关键词： intestine, small/transplantation organ preservation adenosine triphosphate intestine, small/transplatation na(+) K(+) exchanging ATPase adenine nucleotides

Effect of ringer's Solution on Wear and Friction of Stainless Steel 316L after Plasma Electrolytic nitrocarburising at Low Voltages

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Journal of Materials Science & Technology 2011年第10期27卷 906-912页

作者： n.Afsar Kazerooni M.E.Bahrololoom M.H.Shariat F.Mahzoon T.Jozaghi Department of Materials Science and Engineering Shiraz University

A plasma electrolytic nitrocarburising （PEn/C） process was performed on stainless steel 316L to improve the surface properties for using as medical implants. A bath was optimised to reduce the required voltage to 150 volts. Aqueous urea-based solutions with 10% nH4Cl were prepared with slightly different amounts of na2CO3 to optimise the electrolyte composition. The surface and the cross-section morphologies were studied by scanning electron microscopy. The microstructure and the chemical composition of samples were investigated by X-ray diffraction （XRD） and energy dispersive X-ray （EDX） techniques. The microstructure of the outer layer of the coatings was found to be a complex oxide containing Cr and Fe. The wear properties of the samples were examined by using a pin on disk wear test with ringer＇s solution and were compared with their wear properties in the ambient atmosphere. The Ringe（s solution acted as a lubricant, reducing friction coefficient. Hardness and roughness were also studied. The bath with the composition of 10% nH4CI and 3% na2CO3 exhibited the best tribological properties. The results showed that the tribological properties of treated samples were improved and the wear mechanism was abrasion of the pin.

关键词： Plasma electrolytic nitrocarburising ringer's solution Tribological properties

Effect of herpesvirus infection on pancreatic duct cell secretion

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World Journal of Gastroenterology 2005年第38期11卷 5997-6002页

作者： Péter Hegyi Balázs rdg Zoltán Rakonczai Jr Tamás Takács János Lonovics Annamária Szabolcs Réka Sári András Tóth Julius G Papp András Varró Mária K Kovács Mike A Gray Barry E Argent Zsolt Boldogki First Department of Medicine Department of Biology Division of Cardiovascular Pharmacology School of Cell and Molecular Biosciences

AIM: To examine the effect of acute infection caused by herpesvirus (pseudorabies virus, PRV) on pancreatic ductal ***: The virulent Ba-DupGreen (BDG) and nonvirulent Ka-RREpOlacgfp (KEG) genetically modified strains of PRV were used in this study and both of them contain the gene for green fluorescent protein (GFP). Small intra/interlobular ducts were infected with BDG virus (107 PFU/mL for 6 h) or with KEG virus (1010 PFU/mL for 6 h), while non-infected ducts were incubated only with the culture media. The ducts were then cultured for a further 18 *** rate of HCO3- secretion [base efflux -J(B-)] was determined from the buffering capacity of the cells and the initial rate of intracellular acidification (1) after sudden blockage of basolateral base loaders with dihydro-4,4,-diisothiocyanatostilbene-2,2,-disulfonic acid (500 μmol/L)and amiloride (200 μmol/L), and (2) after alkali loading the ducts by exposure to nH4Cl. All the experiments were performed in HCO3--buffered ringer solution at 37 ℃ (n = 5ducts for each experimental condition). Viral structural proteins were visualized by immunohistochemistry. Virallyencoded GFP and immunofluorescence signals were recorded by a confocal laser scanning ***: The BDG virus infected the majority of accessible cells of the duct as judged by the appearance of GFP and viral antigens in the ductal cells. KEG virus caused a similarly high efficiency of infection. After blockage of basolateral base loaders, BDG infection significantly elevated -J(B-) 24 h after the infection, compared to the non-infected group. However, KEG infection did not modify -J(B-). After alkali loading the ducts, -J(B-) was significantly elevated in the BDG group compared to the control group 24 h after the infection. As we found with the inhibitor stop method, no change was observed in the group KEG compared to the non-infected ***: Incubation with the BDG or KEG strains of PRV results in an effective infection o

关键词：疱疹病毒胰腺细胞胰管分泌病毒感染