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On the microstructure and texture evolution in 17-4 PH stainless steel during laser powder bed fusion: Towards textural design

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Journal of Materials Science & Technology 2022年第22期117卷 183-195页

作者： M.S.Moyle n.haghdadi X.Z.Liao S.P.Ringer S.Primig School of Materials Science&Engineering UNSW SydneyNSW 2052Australia Australian Centre for Microscopy&Microanalysis The University of SydneyNSW 2006Australia School of Aerospace Mechanical and Mechatronic EngineeringThe University of SydneyNSW 2006Australia

Additive Manufacturing (AM) of metals allows the production of parts with complex designs, offeringadvanced properties if the evolution of the texture can be controlled. 17-4 precipitation hardening (PH)stainless steel is a high strength, high corrosion resistance alloy used in a range of industries suitable forAM, such as aerospace and marine. Despite 17-4 PH being one of the most common steels for AM, thereare still gaps in the understanding of its AM processing–structure relationships. These include the natureof the matrix phase, as well as the development of texture through AM builds under different processingconditions. We have investigated how changing the laser power and scanning strategy affects the microstructure of 17-4 PH during laser powder bed fusion. It is revealed that the matrix phase is δ-ferritewith a limited austenite presence, mainly in regions of the microstructure immediately below melt *** fraction is independent of the printing pattern and laser power. However, reducing the timebetween adjacent laser passes during printing results in an increase in the austenite volume *** effect of the higher laser power, as well as additional remelting within the printing strategy, isan increase in the average grain size by epitaxial ferrite grain growth across multiple build layers andthe development of a mosaic type microstructure. Changes to the scanning strategy have significant impacts on the textures observed along the build direction, while (100) texture along the scanning directionis observed consistently. Mechanisms for texture formation and the mosaic structure are proposed thatpresents a pathway to the design of texture via AM process control.

关键词： Additive manufacturing 17-4 PH stainless steel Microstructure Texture

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Microstructural and mechanical characteristics of Al-alloyed ductile iron upon casting and annealing

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International Journal of Minerals,Metallurgy and Materials 2012年第9期19卷 812-820页

作者： n. haghdadi B. Bazaz H.R. Erfanian-naziftoosi A.R. Kiani-Rashid Department of Materials Engineering Faculty of Engineering Ferdowsi University of Mashhad 91775-111 Mashhad Iran School of Metallurgy and Materials Engineering College of Engineering University of Tehran 11365-4563 Tehran Iran

Ductile iron containing 6.16wt% A1 was developed to investigate the effects of aluminum on both its microstructure and hardness. It was found that aluminum not only increases the nodule count and pearlite content but also improves the hardness in both sand mold and metal mold castings. Annealing treatments were conducted to attain a homogenous microstructure and improve high-temperature serviceabil- ity. A ferrite/carbide or ferritic matrix was gained depending on the annealing temperature. It is also discovered that annealing has inverse in- fluences on the hardness of the bulk alloy and the ferrite phase. Although it causes a small decrease in the bulk hardness of the specimens, it leads to an increase in the microhardness of the ferrite. Micro-segregation of the alloying elements was also investigated by means of electron probe micro-analysis for the specimens with different annealing durations and the as-cast specimen as well. An optimum annealing time was proposed to result in the least amount of micro-segregation of aluminum and silicon between graphite nodules.

关键词： cast iron casting annealing microstructure hardness

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