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Molecular Structure of (1-Benzyl-4-phenyl-1H-1,2,3-triazol-5-yl)(4-bromophenyl) methanone: A Combined Experimental and Theoretical Study

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Chinese Journal of Structural Chemistry 2014年第12期33卷 1749-1756页

作者： muhammad naeem Ahmed IFZAN Arshad WANG Bo SHAHID Hameed BILAL Ahmad Khan KHAWAJA Ansar Yasin muhammad Moazzam Naseer Department of Chemistry The University of Azad Jammu and Kashmir Muzaffarabad 13100 Pakistan Department of Chemistry Quaid-i-Azam University Islamabad 45320 Pakistan Department of Chemistry Tsinghua University

One-pot three component reaction was used to synthesize 1,4,5-trisubstituted 1,2,3-triazole(A) from the corresponding acid chloride, benzyl azide and 1-copper(I) phenylethyne. The molecular structure was determined by single-crystal X-ray analysis. The compound crystallizes in the orthorhombic space group Pbca, a = 14.9815(14), b = 9.6496(10), c = 25.528(2) A, Z = 8. Furthermore, crystal packing demonstrated a molecular wall-like structure based on supramolecular chains of A, stabilized by CH···O, CH···Br, N···C and CH···π interactions. Molecular geometry in the ground state has been determined by density functional theory(DFT) by B3LYP/6-311G* basis set and compared with the experimental data. The computed vibrational frequencies are compared with the experimental FT-IR data and frontier molecular orbital analyses were performed at the same level of theory. Theoretical parameters are in good agreement with the corresponding X-ray diffraction values.

关键词： synthesis 1,2,3-triazole crystal structure molecular packing optimization

Gene expression pattern of K transporter GhHAK5 gene of potassium efficient and in-efficient cotton cultivars based on morphological physiognomies as affected by potassium nutrition and reduced irrigation

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Journal of Cotton Research 2023年第3期6卷 166-185页

作者： AKHTAR muhammad naeem HAQ Tanveer ul AKHTAR muhammad Waseem ABBASS Ghulam Pesticide Quality Control Laboratory Multan Under Agriculture Research Punjab/Government of Punjab Department of AgricultureMultanPakistan Department of Soil and Environmental Sciences MNS-University of AgricultureMultanPakistan Department of Seed Science and Technology University of Agriculture FaisalabadFaisalabadPakistan

Background Under K deficiency the uptake and distribution pattern in plant cells is mediated through different transport proteins and channels which were controlled by specific gene ***,a hydroponic experiment was conducted under control condition for testing the gene expression pattern of the K transporter under adequate and low K supply *** that,a 2-year field experiment was conducted to evaluate five selected cotton cultivars(four K-efficient cultivars,viz.,CIM-554,CYTO-124,FH-142,IUB-2013,and one K non-efficient,BH-212) screened from the initial hydroponics culture experiment and two levels of potassium(0 K_(2)O kg·ha^(-1) and 50 K_(2)O kg·ha^(-1)) were tested under reduced irrigation(50% available water content;50 AWC) and normal irrigation conditions(100% available water content;100 AWC).Result Results revealed that the transcript levels of GhHAK5aD in roots were significantly higher in K^(+) efficient cultivars than that in K^(+) non-efficient *** GhHAK5aD expression upon K^(+) deficiency was higher in roots but lower in shoots,indicating that GhHAK5aD could have a role in K^(+) uptake in roots,instead of transport of K^(+) from root to ***,under field conditions the cultivar FH-142 showed an increase of 22.3%,4.9%,2.4%,and 1.4% as compared with BH-212,IUB-2013,CYTO-124,and CIM-554,respectively,in seed cotton yield(SCY) with K application under reduced irrigation *** applied K,the FH-142 showed an increase in net photosynthetic rate by 57.3% as compared with the rest of the cultivars under reduced irrigation over K ***,the overall performance indicators of K-efficient cultivars like FH-142,CYTO-124,CIM-554,and IUB-2013 were better than BH-212(K in-efficient) under reduced irrigation conditions with applied K at 50 kg·ha^(-1).Fiber quality trait improved significantly with K application under water *** increase in micronaire was 3.6%,4.7%,7.8%,3.4%,and 6.7% in BH-212,IUB-2013,CIM-554,C

关键词： Cotton K-efficient cultivars Drought Potassium use efficiency WUE

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Structural and dielectric properties of doped ferrite nanomaterials suitable for microwave and biomedical applications

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Progress in Natural Science:Materials International 2015年第5期25卷 419-424页

作者： Imran Sadiq Shahzad Naseem muhammad naeem Ashiq M.A.Khan Shanawer Niaz M.U.Rana Centre of Excellence in Solid State Physics University of the Punjab Institute of Chemical Sciences Bahauddin Zakariya University Department of Physics BUITEMS 4. Department of Physics University of Sargodha

The sol-gel auto-combustion method was adopted to synthesize nanomaterials of single-phase X-type hexagonal ferrites with the composition of Sr;Gd;Ni;Fe;Cd;O;（x=0.00,0.02,0.04,0.06,0.08,0.10 and y = 0,0.1,0.2,0.3,0.4,0.5）.The structural properties were carried out by XRD analysis and the lattice parameters show variation with the doping of *** average particle size measured by TEM was in the range of 8-10 nm which is beneficial in obtaining suitable signal-to-noise ratio in recording media and biomedical *** room temperature resistivity enhanced with the increase of the dopant *** increase in resistivity indicates that the synthesized materials can be considered good for the formation of the multilayer chip inductors（MLCIs） as well as for the reduction of eddy current *** dielectric constant decreased with the increase in the frequency which is the general reported trend of the hexagonal ferrites and can be explained on the basis of Koop’s theory and Maxwell-Wagner *** abnormal dielectric behavior indicates the formation of small polarons in the *** maximum value of tangent loss at low frequencies reflects the application of these materials in medium frequency devices（MF）.

关键词： Sol–gel Nanocrystalline materials Thermal properties Electrical properties Dielectric properties

Reforming of Methane by CO2 over Bimetallic Ni-Mn/γ-Al2O3 Catalyst

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Chinese Journal of Chemical Physics 2014年第2期27卷 214-220,I0004页

作者： Anis Hamza Fakeeha muhammad Awais naeem Wasim Ullah Khan Ahmed Elhag Abasaeed Ahmed Sadeq Al-Fatesh 沙特国王大学工程学院化学工程系利雅得11421

γ-Al2O3 supported Ni-Mn bimetallic catalysts for CO2 reforming of methane were prepared by impregnation method. The reforming reactions were conducted at 500-700℃ and atmospheric pressure using CO2/CH4/N2 with feed ratio of 17/17/2, at total flow rate of 36 mL/min. The catalytic performance was assessed through CH4 and CO2 conversions, synthesis gas ratio （H2/CO） and long term stability. Catalytic activity and stability tests revealed that addition of Mn improved catalytic performance and led to higher stability of bimetallic catalysts which presented better coke suppression than monometallic catalyst. In this work, the optimum loading of Mn which exhibited the most stable performance and least coke deposition was 0.5wt%. The fresh and spent catalysts were characterized by various techniques such as Brunauer-Emmett-Teller, the temperature programmed desorption CO2- TPD, thermogravimetric analysis, X-ray diffraction, scanning electron microscope, EDX, and infrared spectroscopy.

关键词： CH4 CO2 Bimetallic Dry reforming Ni/γ-Al2O3 Mn and H2/CO

Three Tier Fog Networks: Enabling IoT/5G for Latency Sensitive Applications

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China Communications 2019年第3期16卷 1-11页

作者： Romana Shahzadi Ambreen Niaz Mudassar Ali muhammad naeem Joel J.P.C.Rodrigues Farhan Qamar Syed muhammad Anwar University Engineering and Technology COMSATS University Islamabad Wah campus National Institute of Telecommunications (Inatel) Instituto de Telecomunicac??es University ITMO University of Fortaleza (Unifor)

Following the progression in Internet of Things(IoT) and 5G communication networks, the traditional cloud computing model have shifted to fog computing. Fog computing provides mobile computing, network control and storage to the network edges to assist latency critical and computation-intensive applications. Moreover, security features are improved in fog paradigm by processing critical data on edge devices instead of data centres outside the control plane of users. However, fog network deployment imposes many challenges including resource allocation, privacy of users, non-availability of programming model and testing software and support for the heterogenous networks. This article highlights these challenges and their potential solutions in detail. This article also discusses threetier fog network architecture, its standardization and benefits in detail. The proposed resource allocation mechanism for three tier fog networks based on swap matching is described. Results show that by practicing the proposed resource allocation mechanism, maximum throughput with reduced latency is achieved.

关键词： cloud computing fog networks matching games internet of things

Framework for Effective Utilization of Distributed Scrum in Software Projects

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Computer Systems Science & Engineering 2023年第1期44卷 407-422页

作者： Basit Shahzad Wardah naeem Awan Fazal-e-Amin Ahsanullah Abro muhammad Shoaib Sultan Alyahya Department of Software Engineering National University of Modern LanguagesIslamabad44000Pakistan Department of Software Engineering College of Computer and Information SciencesKing Saud UniversityRiyadh11543Saudi Arabia Department of Computer Science Sukkur IBA UniversitySindh65200Pakistan Department of Information Systems College of Computer and Information SciencesKing Saud UniversityRiyadh11543Saudi Arabia

There is an emerging interest in using agile methodologies in Global Software Development(GSD)to get the mutual benefits of both *** is currently admired by many development teams as an agile most known meth-odology and considered adequate for collocated *** the same time,stake-holders in GSD are dispersed by geographical,temporal,and socio-cultural *** to the controversial nature of Scrum and GSD,many significant challenges arise that might restrict the use of Scrum in *** conducted a Sys-tematic Literature Review(SLR)by following Kitchenham guidelines to identify the challenges that limit the use of Scrum in GSD and to explore the mitigation strategies adopted by practitioners to resolve the *** validate our reviewfindings,we conducted an industrial survey of 305 *** results of our study are consolidated into a research *** framework represents current best practices and recommendations to mitigate the identified distributed scrum challenges and is validated byfive experts of distributed *** of the expert review were found supportive,reflecting that the framework will help the stakeholders deliver sustainable products by effectively mitigating the identified challenges.

关键词： Global software development distributed Scrum sustainable development challenges mitigation strategies

Crystal Structure Analysis of 1-Hydroxy-3,5-dimethoxy-9H-xanthen-9-one Isolated from Ajuga bracteosa Root Extract and Its Biological Studies

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Chinese Journal of Structural Chemistry 2019年第9期38卷 1519-1529页

作者： AKHTER Kulsoom AHMED Muhammed naeem GHOUS Tahseen RASHEED Basharat TAHIR muhammad Nawaz ARSHAD Ifzan Department of Chemistry The University of Azad Jammu and KashmirMuzaffarabad13100Pakistan Department of Chemistry Mirpur University of Science and Technology(MUST)Mirpur-10250Azad Jammu and KashmirPakistan Department of Physics University of SargodhaSargodhaPakistan Department of Chemistry Quaid-i-Azam UniversityIslamabadPakistan

The structure of 1-hydroxy-3,5-dimethoxy-9 H-xanthen-9-one isolated from chloroform extract of Ajuga bracteosa root was analyzed by single-crystal X-ray diffraction. DPPH(1,1-diphenyl-2-picryl hydrazyl), ABTS(2,2?-azino-bis-3-ethylbenzothiazoline-6-sulfonic acid) radical scavenging activities(RSA) and Fe2+ chelating activities were carried out to determine the antioxidant potential of the compound. RSA values for the compound were 96%, 96% and 96% for all the three activities respectively at maximum concentration of the compound(100 μ gmL-1) with the IC50 values of 3.40, 4.86 and 0.10(μ gmL-1). Antidiabetic activities including antiglycation and α-glucosidase inhibition were also performed where the antiglycation activity was performed using two techniques including spectrofluorometric as well as spectrophotometric technique. Spectrofluorometric technique provided 97% antiglycation potential while 92% antiglycation potential was observed by spectrophotometric technique for the isolated compound. The compound at a concentration of 10 μ gmL-1 exhibited 31% α-glucosidase inhibitory potential with IC50 of 15.56 μ gmL-1. Antimicrobial activity data showed that the compound was active against all the studied pathogenic bacteria.

关键词： crystal structure radical scavenging activity antidiabetic activity C–H···π interactions

Evaluation of state and community/private forests in Punjab, Pakistan using geospatial data and related techniques

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Forest Ecosystems 2015年第2期2卷 155-167页

作者： naeem Shahzad Urooj Saeed Hammad Gilani Sajid Rashid Ahmad Irfan Ashraf Syed muhammad Irteza World Wide Fund for Nature (WWF) Institute of Geology University of the Punjab International Centre for Integrated Mountain Development (ICIMOD) Department of Land Surveying and Geo-Informatics Hong Kong Polytechnic University

Background： Forests are fundamental in maintaining water supplies, providing economic goods, mitigating climate change, and maintaining biodiversity, thus providing many of the world＇s poorest with income, food and medicine. Too often, forested lands are treated as ＂wastelands＂ or ＂free＂ and are easily cleared for agricultural and infrastructure expansion. Methods： In this paper, the sustainability of two forest ecosystems （state and community/private owned） was evaluated using SPOT-5 satellite images of 2005 and 2011. This study was conducted in a sub-watershed area covering 468 km2, of which 201 km2 is managed by the state and 267 km2 by community/private ownership in the Murree Galliat region of Punjab Province of Pakistan. A participatory approach was adopted for the delineation and demarcation of forest boundaries. The Geographic Object-Based Image Analysis （GEOBIA） technique was used for identification and mapping of ten Land Cover （LC） features. Results： The results show that between the years 2005 to 2011, a total of 55 km2 （24 km2 in state-owned forest and 31 km2 in community/private forest） was converted from forest to non-forest. The conclusion is that conservation is more effective in state-owned forests than in the community/private forests. Conclusions： These findings may help to mobilize community awareness and identify effective initiatives for improved management of community/private forest land for other regions of Pakistan.

关键词： Forest management SPOT-5 satellite images State and community/private owned forests Murree Galliat Pakistan

Weak stem under shade reveals the lignin reduction behavior

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Journal of Integrative Agriculture 2019年第3期18卷 496-505页

作者： Sajad Hussain Nasir Iqbal PANG Ting muhammad naeem Khan LIU Wei-guo YANG Wen-yu College of Agriculture Sichuan Agricultural University/Key Laboratory of Ecophysiology and Farming System in Southwest ChinaMinistry of AgricultureChengdu 611130P.R.China College of Agriculture Bahauddin Zakariya UniversityBahadur Sub-CampusLayyah 31200Pakistan

Shades caused by neighboring tall plants in intercropping systems and weak sunlight are constraints in yield optimization. Shade influences many aspects of plant growth and development, leading to weak stems and susceptibility to lodging. The plant cell wall is composed of certain proteins that allow the walls to stretch out, a process called cell wall loosening. Shade affects anatomical, morphological, and physiological traits of plants, thus reducing the physical strength of the stem in crops by changing the loosening of cell walls. Flexibility of cells facilitates further modifications such as wall loosening. In addition, shade stress causes increased internode length, and reduced xylem synthesis and photosynthesis. In shaded plants, lignin deposition in vascular bundles and sclerenchyma cells of stems is decreased. Lignin is a light sensitive phenolic compound and shading decreases the transcript abundance of several phenolic compound(flavone and lignin) related genes. Shading significantly influences the metabolic activities of phenylalanine ammonia-lyase(PAL), peroxidase(POD), 4-coumarate: CoA ligase(4 CL), and cinnamyl alcohol dehydrogenase(CAD) involved in lignin biosynthesis. Furthermore, suppression of lignin biosynthesis activities by abiotic stresses causes abnormal phenotypes such as collapsed xylem, bent stems, and growth retardation. In this review, the underlying mechanisms illustrate that under shading conditions reduced lignin content results in slender, weak, and unstable stems. The objective of this review is to elaborate lignin biosynthesis and its variability under stressful environmental conditions, especially in shade stress environments. The effects of shade on stem lignin metabolism are discussed on the morphogenetic, physiological, and proteomic levels.

关键词： lignin biosynthesis shade stress lodging stem strength