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Experimental and modeling investigation of dynamic interfacial tension of asphaltenic–acidic crude oil/aqueous phase containing different ions

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Chinese Journal of Chemical Engineering 2017年第12期25卷 1820-1830页

作者： mostafa lashkarbolooki Shahab Ayatollahi School of Chemical Engineering Babol Noshirvani University of Technology Babol Iran School of Chemical and Petroleum Engineering Sharif University of Technology Tehran Iran

In this way, after experimental measurement of interfacial tension, different models including mono-exponential decay, dynamic adsorption models and empirical equation are used to correlate this time-dependent behavior of interfacial tension(IFT). During the modeling approach, the induction, adsorption, equilibrium, and mesoequilibrium times as well as diffusivity of surface active components known as natural surfactant including asphaltene and resin from crude oil to the interface are obtained. In addition, the surface excess concentration of surface active components at the interface and Gibbs adsorption isotherm are utilized to analyze the measured dynamic IFTs. Finally, the mechanisms of crude oil/aqueous solution IFT including(a) the activity of surfaceactive components and(b) surface excess concentration of them at fluid/fluid interface are proposed and discussed in details.

关键词： Dynamic IFT Adsorption Ion Crude oil EOR

Correlating thermal conductivity of pure hydrocarbons and aromatics via perceptron artificial neural network (PANN) method

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Chinese Journal of Chemical Engineering 2017年第5期25卷 547-554页

作者： mostafa lashkarbolooki Ali Zeinolabedini Hezave Mahdi Bayat School of Chemical Engineering Babol University of Technology Islamic Azad University Dashtestan Branch Department of Chemical Engineering Faculty of EngineeringUniversity of Bojnord

Accurate estimation of liquid thermal conductivity is highly necessary to appropriately design equipments in different industries. Respect to this necessity, in the current investigation a feed-forward artificial neural network(ANN) model is examined to correlate the liquid thermal conductivity of normal and aromatic hydrocarbons at the temperatures range of 257–338 K and atmospheric pressure. For this purpose, 956 experimental thermal conductivities for normal and aromatic hydrocarbons are collected from different previously published *** the modeling stage, to discriminate different substances, critical temperature(Tc), critical pressure(Pc)and acentric factor(ω) are utilized as the network inputs besides the temperature. During the examination, effects of different transfer functions and number of neurons in hidden layer are investigated to find the optimum network architecture. Besides, statistical error analysis considering the results obtained from available correlations and group contribution methods and proposed neural network is performed to reliably check the feasibility and accuracy of the proposed method. Respect to the obtained results, it can be concluded that the proposed neural network consisted of three layers namely, input, hidden and output layers with 22 neurons in hidden layer was the optimum ANN model. Generally, the proposed model enables to correlate the thermal conductivity of normal and aromatic hydrocarbons with absolute average relative deviation percent(AARD), mean square error(MSE), and correlation coefficient(R^2) of lower than 0.2%, 1.05 × 10^(-7) and 0.9994, respectively.

关键词： Thermal conductivity Artificial neural network Critical properties Hydrocarbons Aromatics

Effect of salts and their interaction with ingenious surfactants on the interfacial tension of crude oil/ionic solution

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Chinese Journal of Chemical Engineering 2020年第1期28卷 224-235页

作者： mostafa lashkarbolooki Roohollah Parvizi Shahab Ayatollahi Ebrahim Ghaseminejad Raeeni School of Chemical Engineering Babol Noshirvani University of TechnologyBabolIran Department of Chemical Engineering Islamic Azad UniversityIran School of Chemical and Petroleum Engineering Sharif University of TechnologyTehranIran National Iranian South Oil Company Iran

Understanding the roles of asphaltene and resin as natural surfactants existed in crude oil can enlighten contradicting reported results regarding interfacial tension(IFT) of crude oil/aqueous solution as a function of salinity and ion type. In this way, this study is aimed to investigate the effect of these natural surface active agents on IFT of with special focus on SO4^2-anion and Mg^2+cation. Two different synthetic oil solutions of 8 wt% of the extracted asphaltene and resin dissolved in toluene are prepared, and then IFT values are measured. After that,the obtained results are compared with the IFT of intact crude oil in contact with the same saline solutions examined in the previous stage. The obtained results showed a synergistic effect of Na2SO4+ MgCl2 solution unlike the MgSO4+ MgCl2 and CaSO4+ MgCl2 solutions on IFT reduction of resin at MgCl2 concentration of 15000 mg·kg^-1. In summary, it is found that the affinity of asphaltene molecules towards the interface of oleic phase/ionic solution leads to higher IFT variation.

关键词： IFT Resin Asphaltene Mg^2+ SO4^2-

The role of CO2 and ion type in the dynamic interfacial tension of acidic crude oil/carbonated brine

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Petroleum Science 2019年第4期16卷 850-858页

作者： mostafa lashkarbolooki Ali Zeinolabedini Hezave Shahab Ayatollahi School of Chemical Engineering Babol Noshirvani Incubation Centre of Science and Technology Park Fanavari Atiyeh Pouyandegan Exir CompanyArākIran School of Chemical and Petroleum Engineering Sharif University of TechnologyTehranIran

The e ects of CO2 and salt type on the interfacial tension(IFT) between crude oil and carbonated brine(CB) have not been fully understood. This study focuses on measuring the dynamic IFT between acidic crude oil with a total acid number of 1.5 mg KOH/g and fully CO2-saturated aqueous solutions consisting of 15,000 ppm of KCl, NaCl, CaCl2 and MgCl2 at 30 °C and a wide range of pressures(500–4000 psi). The results of IFT measurements showed that solvation of CO2 into all the studied aqueous solutions led to an increase in IFT of acidic crude oil(i.e., comparison of IFT of crude oil/CB and crude oil/brine), while no significant e ect was observed for pressure. In contrast, the obtained results of studied salts indicated a positive e ect on the IFT reduction of acidic crude oil/carbonated water(CW)(i.e., comparison of IFT of crude oil/CB and crude oil/CW).

关键词： Carbonated brine Interfacial tension Crude oil Enhanced oil recovery(EOR) CO2 sequestration

Catalytic behaviors of Co-Mn/TiO_2 catalysts for Fischer-Tropsch synthesis

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燃料化学学报 2012年第12期40卷 1435-1443页

作者： mostafa Feyzi Faculty of Chemistry Razi UniversityKermanshahIran

The 15%(Co-Mn)/TiO2,(Co/Mn=1/6) catalyst was prepared using fusion procedure and studied for the conversion of synthesis gas to C2 ～ 4 *** effects of calcination conditions and operation conditions such as the H 2 / CO molar feed ratio at different temperatures,gas hourly space velocity(GHSV) and total reaction pressure on the catalytic performance of catalyst were *** stability of the catalyst during 150 h at optimal operation conditions(t = 250℃ H2 /CO= 2/1,GHSV=1 500 h-1 and p =0.3 MPa) has been *** is found that this catalyst is high stable for production C2 ～ 4 *** of both precursors and calcined catalysts by powder X-ray diffraction,scanning electron microscopy(SEM),Brunauer-Emmett-Teller(BET) specific surface area measurement and thermal analysis methods such as thermal gravimetric analysis(TGA) and differential scanning calorimetry(DSC) show that the different preparation method influences the catalyst precursor structure and morphology.

关键词：气化理论燃料化学研究发展

Geochemical and mineralogical characteristics of some gold mine tailings in the Eastern Desert of Egypt

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Frontiers of Earth Science 2022年第4期16卷 906-915页

作者： mostafa REDWAN Geology Department Faculty of ScienceSohag UniversitySohag 82524Egypt

The adverse environmental effects of mine tailings disposal on the surrounding ecosystems are world-wide environmental *** to environmental issues related to tailings discharged on land surface,detailed tailings characterization is a prerequisite for a long-term management *** tailings from four gold mines in Egypt,namely Fatira,El Sid,Barramiya,and Atud were investigated for their geochemical-mineralogical features and the effect of weathering behavior on the release of their heavy *** tailings samples were investigated by mineralogical(XRD and ESEM-EDS),physical(grain-size distribution)and geochemical(XRF)*** of the tailings have uniform silt-size with fine to very finesand and *** tailings have coarse to fine *** carbonate,predominantly calcite was found for the samples from Fatira and Atud,calcite-ankerite from El Sid and dolomite from Barramiya with little ***-mean of Cr(569287 mg/kg),Ni(89191 mg/kg)and Co(4221 mg/kg)values are coinciding with the ultramafic nature in Atud and Barramiya *** Sid tailings have a high-mean concentration of Zn(1357 mg/kg)and Pb(1349 mg/kg).Barramiya tailings have a high-mean As concentration(2635 mg/kg).The Fatira tailings are characterized by high-mean values of Sr(444 mg/kg)and Cu(280 mg/kg)arising from auriferous *** Sr concentrations in Fatira tailings are mainly due to its adsorption to iron *** oxidation is conceded along the cracks and/or the edges of the crystals in the El Sid,Barramiya and Atud *** Threshold Effect Level(TEL)values indicated high contamination from heavy elements to the neighboring *** tailings were deposited downstream into the small *** and water erosion can dissolve efflorescent materials enriched in toxic elements like As,Zn,and Pb at tailings *** release of contaminants could be catastrophic for the environment without mine site rehabilitation strategies.

关键词： gold mine tailings geochemistry mineralogy Egypt

Cooperative distributed state estimation:resilient topologies against smart spoofers

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Control Theory and Technology 2022年第4期20卷 488-503页

作者： mostafa Safi Amirkabir University of Technology HafezTehran 424Iran

A network of observers is considered,where through asynchronous(with bounded delay)communications,they cooperatively estimate the states of a linear time-invariant(LTI)*** such a setting,a new type of adversary might affect the observation process by impersonating the identity of the regular node,which is a violation of communication *** adversaries also inherit the capabilities of Byzantine nodes,making them more powerful threats called smart *** show how asynchronous networks are vulnerable to smart spoofing *** the estimation scheme considered in this paper,information flows from the sets of source nodes,which can detect a portion of the state variables each,to the other follower *** regular nodes,to avoid being misguided by the threats,distributively filter the extreme values received from the nodes in their *** conditions based on strong robustness are proposed to guarantee the *** simulation scenarios are provided to verify the results.

关键词： Cyber-physical systems Smart spoofing Distributed resilient algorithm Secure observers

Non-linear Semigroup of a Class of Abstract Semilinear Functional Differential Equations with a Non-Dense Domain

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Acta Mathematica Sinica,English Series 2004年第5期20卷 933-942页

作者： mostafa ADIMY mostafa LAKLACH Khalil EZZINBI Département de Mathématiques Appliquées U RS 2055 C.N.R.SUniversité de PauAvenue de l'Université64000 PauFrance Département de Mathématiques Faculté des Sciences SemlaliaB.P.2390MarrakeshMorocco

In this work,we are concerned with a general class of abstract semilinear autonomous functional differential equations with a non-dense domain on a Banach *** objective is to study,using the Crandall-Liggett approach,... 详细信息

关键词： Non-linear semigroup Semilinear functional differential equation Hille-Yosida operator Crandall-Ligget t approach

Nucleic Acid Metabolism, Proline Concentration and Antioxidants Enzyme Activity in Canola (Brassica nupus L.) Under Salinity Stress

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Agricultural Sciences in China 2010年第4期9卷 504-511页

作者： mostafa Heidari Department of Agronomy and Plant Breeding University of ZabolZabol P.O. Box 98615-538 Iran

Seedling of five canola genotypes, Hyola 308, Hyola 401, Hyola 60, Option 50 and RGS003, were grown in Hoagland nutrient solution containing S1 = 0, S2 = 100, S3 = 200 and S4 = 300 mmol L-1 NaCl in controlled environment. Proline, antioxidant activities like catalase （CAT）, ascobrate peroxidase （APX） and guaiacol peroxidase （GPX） and some enzyme activities of nucleic acid metabolism were determined in shoot and root 20 days after induction of salinity stress. Results showed application of stress significantly affected plant growth components such as fresh （FW） and dry weight （DW） of canola genotypes. Among the genotypes, RGS003 had the highest reduction of FW and DW in S3 treatment. By increasing NaCl levels from 0 to 300 mmol L-1, the activity of two antioxidant enzymes （APX and CAT） in shoot and root increased but GPX in all of genotypes decreased. The increase in salinity stress, increased proline concentration in both root and shoot tissues of canola genotypes. Hyola 401 genotype had the maximum concentration of proline in root and shoot in S3 treatment. Along with increased salinity stress in all of the studied plants, salinity significantly increased the level of the total nucleic acid and the activity of DNase I in all of salinity treatments and at the S3 level, RGS003 had the maximum concentration of nucleolytic enzyme.

关键词： antioxidant activity proline salinity nucleolytic enzyme canola