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ⅢA-ⅡB multicomponent perovskite rare earth ferrites with promising electromagnetic wave absorption properties

Journal of Rare Earths 2024年第6期42卷 1118-1127,I0005页

作者： Yanyan He Tao Chen Yanyu Pan minzhong huang Kaixian Wang Liyan Xue Yazhu Li Fengzhi Tan Fan Yang Tongkuan Xu Heng Chen School of Light Industry and Chemical Engineering Dalian Polytechnic UniversityDalian116034China Xiamen Institute of Rare EarthMaterials Haixi InstitutesChinese Academy of SciencesXiamen36021China Fujian Institute of Research on the Structure of Matter Chinese Academyof SciencesFuzhou350002China Fujian Science&Technology Innovation Laboratory for Optoelectronic Information of China Fuzhou350108China Xiamen Key-Laboratoryof Rare Earth Photoelectric Functional Materials Xiamen Institute of Rare Earth MaterialsHaixi InstituteChinese Academy of SciencesXiamen361021China Key Laboratory of Rare Earths Ganjiang Innovation AcademyChinese Academy of SciencesGanzhou3410ooChina

Perovskite-type rare-earth ferrites(REFeO_(3))are promising materials for absorbing electromagnetic(EM)wave ***,insufficient dielectric loss and poor impedance matching are key factors that limit the broader implementation of REFeO_(3).Herein,a series of multicomponent perovskite-type ferrites with strong EM wave absorption capabilities was *** the synergistic effect of chemical constitution regulation and entropy regulation,optimization of the dielectric loss and impedance matching is achieved by strengthening the structural defect mechanism,thus further adjusting the EM wave absorption *** with(LaGdSmNdBa)FeO_(3)(HE-1)and(LaGdPrSmNdBa)FeO_(3)(HE-2),(LaGdBa)FeO_(3)(ME-1)and(LaGdSmBa)FeO_(3)(ME-2)exhibit favorable performance,with optimal minimum reflection loss(RL_(min))of-56.35 dB(at 11.12 GHz)and-63.25 dB(at 7.22 GHz)and effective absorption bandwidth(EAB)of 4.46 and 4.72 GHz,*** multicomponent design provides a new strategy for the development of EM wave absorption materials.

关键词： Rare earths Multicomponent design Rare earth ferrites Entropy regulation Electromagnetic wave absorption

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High-entropy rare earth stannate ceramics:Acid corrosion resistant radiative cooling materials with high atmospheric transparency window emissivity and high near-infrared solar reflectivity

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Journal of Advanced Ceramics 2024年第5期13卷 630-640页

作者： Tao Chen Yanyan He Yanyu Pan Kaixian Wang minzhong huang Liyan Xue Yazhu Li Fan Yang Yanchun Zhou Heng Chen Fujian Institute of Research on the Structure of Matter Chinese Academy of SciencesFuzhou 350002China College of Chemistry and Materials Science Fujian Normal UniversityFuzhou 350117China Xiamen Institute of Rare Earth Materials Haixi InstitutesChinese Academy of SciencesXiamen 361021China Fujian Science&Technology Innovation Laboratory for Optoelectronic Information of China Fuzhou 350108China Xiamen Key Laboratory of Rare Earth Photoelectric Functional Materials Xiamen Institute of Rare Earth MaterialsHaixi InstitutesChinese Academy of SciencesXiamen 361021China Key Laboratory of Rare Earths Ganjiang Innovation AcademyChinese Academy of SciencesGanzhou 341000China School of Materials Science and Engineering Zhengzhou UniversityZhengzhou 450001China

In response to the development of the concepts of“carbon neutrality”and“carbon peak”,it is critical to developing materials with high near-infrared(NIR)solar reflectivity and high emissivity in the atmospheric transparency window(ATW;8–13μm)to advance zero energy consumption radiative cooling *** regulate emission and reflection properties,a series of high-entropy rare earth stannate ceramics(HE-RE_(2)Sn_(2)O_(7):(Y_(0.2)La_(0.2)Nd_(0.2)Eu_(0.2)Gd_(0.2))_(2)Sn_(2)O_(7),(Y_(0.2)La_(0.2)Sm_(0.2)Eu_(0.2)Lu_(0.2))_(2)Sn_(2)O_(7),and(Y_(0.2)La_(0.2)Gd_(0.2)Yb_(0.2)Lu_(0.2))_(2)Sn_(2)O_(7))with severe lattice distortion were prepared using a solid phase reaction followed by a pressureless sintering method for the first *** distortion is accomplished by introducing rare earth elements with different cation radii and *** as-synthesized HE-RE_(2)Sn_(2)O_(7)ceramics possess high ATW emissivity(91.38%–95.41%),high NIR solar reflectivity(92.74%–97.62%),low thermal conductivity(1.080–1.619 W·m^(−1)·K^(−1)),and excellent chemical *** the one hand,the lattice distortion intensifies the asymmetry of the structural unit to cause a notable alteration in the electric dipole moment,ultimately enlarging the ATW *** the other hand,by selecting difficult excitation elements,HE-RE_(2)Sn_(2)O_(7),which has a wide band gap(Eg),exhibits high NIR solar ***,the multi-component design can effectively enhance radiative cooling ability of HE-RE_(2)Sn_(2)O_(7)and provide a novel strategy for developing radiative cooling materials.

关键词： radiative cooling materials high-entropy ceramics(HECs) rare earth stannate(RE_(2)Sn_(2)O_(7)) high atmospheric transparency window emissivity high near-infrared(NIR)solar reflectivity

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Solid-phase extraction and separation of indium with P_(2)O_(4)-UiO-66-MOFs (di-2-ethylhexyl phosphoric acid-UiO-66-metal-organic frameworks)

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Journal of Environmental Sciences 2023年第5期127卷 833-843页

作者： Wan-Yi Zeng minzhong huang Minglai Fu Key Laboratory of Urban Pollutant Conversion Institute of Urban EnvironmentChinese Academy of SciencesXiamen 361021China University of Chinese Academy of Sciences Beijing 100049China School of Electromechanical Engineering Guangdong University of TechnologyGuangzhou 510006China Xiamen Key Laboratory of Municipal and Industrial Solid Waste Utilization and Pollution Control College of Civil EngineeringHuaqiao UniversityXiamen 361021China

Compared with the traditional liquid–liquid extraction method,solid-phase extraction agents are of great significance for the recovery of indium metal due to their convenience,free of organic solvents,and fully exposed *** this study,P_(2)O_(4)(di-2-ethylhexyl phosphoric acid)was chemically modified by using UiO-66 to form the solid-phase extraction agent P_(2)O_(4)-UiO-66-MOFs(di-2-ethylhexyl phosphoric acid-UiO-66-metal-organic frameworks)to adsorb In(Ⅲ).The results show that the Zr of UiO-66 bonds with the P-OH of P_(2)O_(4) to form a composite P_(2)O_(4)-UiO-66-MOF,which was confirmed by X-ray photoelectron spectroscopy(XPS)and Fourier transform infrared spectroscopy(FT-IR).The adsorption process of indium on P_(2)O_(4)-UiO-66-MOFs followed pseudo first-order kinetics,and the adsorption isotherms fit the Langmuir adsorption isotherm *** adsorption capabilities can reach 192.8 mg/*** five consecutive cycles of adsorption-desorption-regeneration,the indium adsorption capacity by P_(2)O_(4)-UiO-66-MOFs remained above 99%.The adsorption mechanism analysis showed that the P=O and P-OH of P_(2)O_(4) molecules coated on the surface of P_(2)O_(4)-UiO-66-MOFs participated in the adsorption reaction of *** this paper,the extractant P_(2)O_(4) was modified into solid P_(2)O_(4)-UiO-66-MOFs for the first *** work provides a new idea for the development of solid-phase extractants for the recovery of indium.

关键词： P_(2)O_(4)-UiO-66-MOFs(di-2-Ethylhexyl phosphoric acid-UiO-66-metal-organic frameworks) Solid-phase extraction Adsorption Indium(III)

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High-entropy(Sm_(0.2)Eu_(0.2)Gd_(0.2)Dy_(0.2)Er_(0.2))_(2)Hf_(2)O_(7) ceramic with superb resistance to radiation-induced amorphization

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Journal of Materials Science & Technology 2023年第24期155卷 1-9页

作者： Jingxin Wu Meng Zhang Zhanqiang Li minzhong huang Huiming Xiang Liyan Xue Zhengming Jiang Zhigang Zhao Lianfeng Wei Yong Zheng Fan Yang Guang Ran Yanchun Zhou Heng Chen School of Rare Earths University of Science and Technology of China Hefei 230026 China Ganjiang Innovation Academy Chinese Academy of Sciences Ganzhou 341000 China Xiamen Institute of Rare Earth Materials Haixi Institute Chinese Academy of Sciences Xiamen 361021 China Fujian Province Joint Innovation Key Laboratory of Fuel and Materials in Clean Nuclear Energy System Fujian Institute of Research on the Structure of Matter Chinese Academy of Sciences Fuzhou 350002 China Fujian Science & Technology Innovation Laboratory for Optoelectronic Information of China Fuzhou 350108 China Science and Technology on Advanced Functional Composite Laboratory Aerospace Research Institute of Materials & Processing Technology Beijing 100076 China The Key Nuclear Fuel and Nuclear Materials Laboratory of China Nuclear Power Institute of China Chengdu 610213 China China Rare Earth Group Co. Ltd. Chengdu 610213 China College of Energy Xiamen University Xiamen 361102 China School of Materials Science and Engineering Zhengzhou University Zhengzhou 450001 China

Nuclear engineering materials are required to possess outstanding extreme environmental tolerance and irradiation resistance.A promising novel pyrochlore-type of(Sm_(0.2)Eu_(0.2)Gd_(0.2)Dy_(0.2)Er_(0.2))2 Hf_(2)O_(7)high-entropy ceramic(HE-RE2 Hf_(2)O_(7))for control rod was prepared by solid-state reaction *** ion irradiation of HE-RE_(2) Hf_(2)O_(7)with 400 keV Kr+at 400℃was investigated using a 400 kV ion implanter and compared with single-component pyrochlore Gd2 Hf_(2)O_(7)to evaluate the irradiation *** HE-RE2 Hf_(2)O_(7),the phase transition from pyrochlore to defective fluorite is revealed after irradiation at 60 *** irradiation at 120 dpa,it maintained crystalline,which is comparable to Gd2 Hf_(2)O_(7)but superior to the titanate pyrochlores previously ***,the lattice expansion of HE-RE2 Hf_(2)O_(7)(_(0.2)2%)is much lower than that of Gd2 Hf_(2)O_(7)(0.62%),indicating excellent irradiation damage *** tests displayed an irradiation-induced increase in hardness and a decrease in elastic modulus by about 2.6%.Irradiation-induced segregation of elements is observed on the surface of irradiated *** addition,HE-RE2 Hf_(2)O_(7)demonstrates a more sluggish grain growth rate than Gd2 Hf_(2)O_(7)at 1200℃,suggesting better high-temperature *** linear thermal expansion coefficient of HE-RE2 Hf_(2)O_(7)is 10.7×10-6 K-1 at 298–1273 *** general,it provides a new strategy for the design of the next advanced nuclear engineering materials.

关键词： High-entropy ceramic Rare earth hafnate Ion irradiation Amorphization resistance High temperature stability Nuclear safety

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基于DLP技术打印制备聚合物转化陶瓷基复合材料的研究

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陶瓷学报 2023年第1期44卷 154-162页

作者：欧俊黄民忠黄瑶姜知水伍尚华广东工业大学机电工程学院广东广州510006 广东捷成科创电子股份有限公司广东肇庆526060

将含惰性填料(Si3N4晶须)的陶瓷前驱体/光敏树脂浆料经数字光处理(DLP)3D打印技术成功制备出了复杂结构的生坯,经热解后生坯转化为聚合物转化陶瓷基复合材料,并能完好地保持其形貌和结构。引入的填料不仅可以避免大块生坯在热解过程中崩... 详细信息

将含惰性填料(Si3N4晶须)的陶瓷前驱体/光敏树脂浆料经数字光处理(DLP)3D打印技术成功制备出了复杂结构的生坯,经热解后生坯转化为聚合物转化陶瓷基复合材料,并能完好地保持其形貌和结构。引入的填料不仅可以避免大块生坯在热解过程中崩塌,还能有效降低陶瓷材料的线性收缩率和失重率,并且其作为增强相可以显著提高复合材料的力学性能。当填料含量为10 wt.%时,复合材料的抗弯强度可达(160.9±19.7)MPa。此外,还讨论了填料含量对复合材料微观结构和孔隙率的影响,发现过量的填料会导致复合材料孔隙缺陷增加,基体连续性降低,从而降低复合材料的力学性能。

关键词： 3D打印陶瓷前驱体复合材料力学性能

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苏云金芽胞杆菌3-羟基丁酮代谢基因簇的转录调控

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微生物学报 2015年第9期55卷 1144-1153页

作者：黄闽忠彭琦张杰高继国宋福平东北农业大学生命科学学院黑龙江哈尔滨150030 中国农业科学院植物保护研究所植物病虫害生物学国家重点实验室北京100193

【目的】通过分析苏云金芽胞杆菌(Bacillus thuringiensis)3-羟基丁酮代谢基因簇aco的转录调控和acoR突变体的表型特征,明确aco基因簇的转录调控机制和对芽胞产量及Cry蛋白产量的影响。【方法】通过生物信息学方法分析aco基因簇的结构,R... 详细信息

【目的】通过分析苏云金芽胞杆菌(Bacillus thuringiensis)3-羟基丁酮代谢基因簇aco的转录调控和acoR突变体的表型特征,明确aco基因簇的转录调控机制和对芽胞产量及Cry蛋白产量的影响。【方法】通过生物信息学方法分析aco基因簇的结构,RT-PCR分析基因簇的转录单元,采用同源重组技术敲除苏云金芽胞杆菌HD73菌株的acoR基因,利用启动子融合lac Z的方法分析启动子的转录活性。利用总蛋白定量确定Cry1Ac蛋白产量。【结果】aco基因簇由aco ABCL 4个基因组成,形成一个转录单元。aco基因簇的启动子Paco A转录活性在sig L(编码Sigma 54因子)和acoR突变体中均明显降低。acoR基因的缺失对菌体生长和Cry1Ac蛋白产量无显著影响,但使菌体运动能力减弱,使芽胞产量略有下降,并且不能利用3-羟基丁酮。【结论】aco操纵子受Sigma 54控制,并由AcoR激活,aocR基因的缺失影响菌体对3-羟基丁酮的利用,但对Cry蛋白产量无显著影响。

关键词：苏云金芽胞杆菌 3-羟基丁酮 acoR Sigma 54

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基于空间灰度重心推进的线结构光中心提取

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电子测量技术 2024年第2期47卷 44-50页

作者：卜民众吴国新黄金鹏左云波刘秀丽北京信息科技大学现代测控技术教育部重点实验室北京100192 北京信息科技大学机电工程学院北京100192

利用线结构光对工件进行三维测量时,快速、准确提取激光光条中心是测量系统的关键技术之一。提出一种基于空间灰度重心推进的激光中心提取方法。该方法基于激光条纹空间灰度重心向前推进,结合八邻域判定法进行光条空间区域的选取,接着... 详细信息

利用线结构光对工件进行三维测量时,快速、准确提取激光光条中心是测量系统的关键技术之一。提出一种基于空间灰度重心推进的激光中心提取方法。该方法基于激光条纹空间灰度重心向前推进,结合八邻域判定法进行光条空间区域的选取,接着对选取的区域进行新的空间灰度重心坐标提取;在完成整幅图像提取后,采取3σ准则剔除异常中心点,最终获得激光中心坐标信息。实验结果表明,所提算法对不同类型条纹的适用性强,提取效果稳定。提取中心均方根误差为0.492pixel,相较于提取精度最优的Steger改进算法提升了9.8%,提取速度提高了5倍;相较于处理速度最优的内部推进算法,在保持提取速度基础上,提取精度提升了24.1%。同时,所提算法极大增强了对欠曝光光条图像的处理能力,有效降低了环境对线结构光测量的限制。

关键词：测量线结构光空间灰度重心 3σ准则

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核壳结构β-NaYF_4:Yb^(3+),Tm^(3+)/TiO_2的制备及光催化性能

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环境科学与技术 2015年第4期38卷 60-64页

作者：黄民忠陈建炜戴乐阳付明来集美大学轮机工程学院福建厦门361021 中国科学院城市环境研究所福建厦门361021

核壳结构纳米复合材料β-Na YF4∶Yb3+,Tm3+/Ti O2的制备分为2个步骤:首先通过高温热分解法制备由上转换发光材料β-Na YF4∶Yb3+,Tm3+组成的核;再由钛酸四丁酯(TBOT)在表面活性剂聚乙烯吡咯烷酮K-30(PVP)作用下水解而成的壳。测试表明,... 详细信息

核壳结构纳米复合材料β-Na YF4∶Yb3+,Tm3+/Ti O2的制备分为2个步骤:首先通过高温热分解法制备由上转换发光材料β-Na YF4∶Yb3+,Tm3+组成的核;再由钛酸四丁酯(TBOT)在表面活性剂聚乙烯吡咯烷酮K-30(PVP)作用下水解而成的壳。测试表明,β-Na YF4∶Yb3+,Tm3+/Ti O2是由β型六方相结构Na YF4纳米粒子和无定形结构的Ti O2组成。这种核壳结构纳米复合材料可以吸收近红外光(NIR),其中β-Na YF4∶Yb3+,Tm3+可以吸收近红外光,而后通过上行转换发出紫外光,通过激发Ti O2产生活性基团,达到催化降解有机污染物的目的。为了验证其光催化活性,在980 nm激光照射下将其用于罗丹明B(Rh B)的降解,结果证明该复合材料可以达到一定的降解效果。因此,核壳结构纳米复合材料β-Na YF4∶Yb3+,Tm3+/Ti O2是一种新型的近红外光催化剂,其能有效地扩展光催化剂对太阳能光谱的响应区域,提高太阳光的利用率,在未来Ti O2的光催化或者能源利用领域有着广阔的应用前景。

关键词：上转换 β-Na YF4∶Yb3+ Tm3+/Ti O2 光催化近红外

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对黏虫具有杀虫活性的Bt蛋白筛选及分析

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植物保护 2016年第3期42卷 30-35,62页

作者：杨素娟黄闽忠李艳秋周子珊江幸福高继国程云霞张杰东北农业大学生命科学学院哈尔滨150030 中国农业科学院植物保护研究所植物病虫害生物学国家重点实验室北京100193

为筛选对黏虫[Mythimna separata(Walker)]具有毒杀作用的苏云金芽胞杆菌杀虫蛋白,本研究提取Cry1类、Cry2类、Cry9类及Vip3A类等11种蛋白,通过人工饲料喂毒方法对黏虫进行生物活性测定。结果表明,Cry1Ac、Cry1Ab、Cry2Ab、Cry1Be及Cry... 详细信息

为筛选对黏虫[Mythimna separata(Walker)]具有毒杀作用的苏云金芽胞杆菌杀虫蛋白,本研究提取Cry1类、Cry2类、Cry9类及Vip3A类等11种蛋白,通过人工饲料喂毒方法对黏虫进行生物活性测定。结果表明,Cry1Ac、Cry1Ab、Cry2Ab、Cry1Be及Cry1Bb蛋白对黏虫具有杀虫活性,其致死中浓度依次为5.09、17.71、26.75、27.42及43.93μg/g;Cry9Aa、Cry9Eb、Cry9Ee蛋白对黏虫生长具有抑制作用,其浓度为10μg/g时的体重抑制率分别为78.4%、79.0%、86.9%,浓度为100μg/g时的体重抑制率分别为92.8%、95.7%、96.7%;Cry1Ba、Cry1Ca和Vip3Aa蛋白对黏虫无显著活性。本研究为黏虫的生物防治奠定了基础,并为抗虫转基因作物的研究提供优良的候选基因。

关键词：苏云金芽胞杆菌 Cry蛋白黏虫杀虫活性生长抑制

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Relationship between thermal anomalies in Tibetan Plateau and summer dust storm frequency over Tarim Basin,China

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Journal of Arid Land 2013年第1期5卷 25-31页

作者： Yong ZHAO HongJun LI AnNing huang Qing HE Wen HUO minzhong WANG Institute of Desert Meteorology China Meteorological Administration Urumqi 830002 China School of Atmospheric Sciences Nanjing University Nanjing 210093 China

The dust storm is the most important and frequent meteorological disaster over Tarim Basin, which causes huge damages on local social economics. How to predict the springtime and summertime dust storm oc- currence has become a hot issue for meteorologists. This paper employed the data of dust storm frequency and 10-m wind velocity at 35 stations over Tarim Basin and the reanalysis data from the National Center for Environ- mental Prediction and the National Center for Atmospheric Research （NCEP/NCAR） during 1961-2007 to study the relationship between dust storm frequency （DSF） in summer over Tarim Basin and the thermal anomalies in Tibetan Plateau in May by using the statistical methods, such as Empirical Orthogonal Function （EOF）, correlation and binomial moving average. The results show when negative anomalies in Tibetan Plateau and positive anomalies in its southern region are present along 30~N （the second mode of surface temperature anomalies by EOF decomposition） in May, the time coefficient （PC2） plays an important role in summer DSF variation and has a close relation with the summer DSF at both inter-annual and decadal time scales. When negative anomalies in Tibetan Plateau and positive anomalies are present in its southern region （PC2 in positive phase）, there is an anomalous anticyclone in North China, which weakens the northwest wind and is not beneficial for cold air moving from high latitude to the Tarim Basin, and the circulation pattern is hard to result in dust storm weather. Furthermore, the sea level pressure （SLP） increased over Tarim Basin and the direction of SLP gradient reversed, which resulted in the 10-m wind velocity slowing down, so the DSF decreased. From above all, it can be conclude that the thermal anomalies in Tibetan Plateau in May has important effects on the summertime dust storm frequency over Tarim Basin and the PC2 can be used as a prediction factor for the summertime dust storm occurrence.

关键词： dust storm frequency thermal anomalies Tarim Basin Tibetan Plateau

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