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Antibacterial activity and mechanism of newly developed Zr-30Ta and Zr-25Ta-5Ti alloys against implant-associated infection

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Rare Metals 2022年第12期41卷 4176-4187页

作者： Hai-Lin Yang Akram Nasser Juaim Ling Zou meng-zhen zhu Xiao-Na Chen Chen-Xu Ma Xiong-Wen Zhou State Key Laboratory of Powder Metallurgy Central South UniversityChangsha 410083China National Clinical Research Center for Geriatric Disorders Xiangya HospitalCentral South UniversityChangsha 410008China Department of Prosthodontics Center of StomatologyXiangya HospitalCentral South UniversityChangsha 410008China Department of Prosthodontics Faculty of DentistryThamar UniversityDharmarYemen Department of Oral Implantology Xiangya Stomatological Hospital and School of StomatologyCentral South UniversityChangsha 410008China

Infection is a common problem after implantation,and the currently used Ti-based implants have insufficient antibacterial *** newly developed Zr-30Ta and Zr-25Ta-5Ti alloys exhibited good mechanical properties,low elastic moduli,and high corrosion *** this work,their antibacterial activities and antibacterial mechanisms were *** surface roughness,wettability,and charge of the alloys were evaluated using a profilometer,drop shape analyzer,and electrokinetic analyzer,*** antibacterial activity against Streptococcus mutans and Porphyromonas gingivalis was investigated using the inhibition zone assay,plate count assay,live/dead staining,and scanning electron microscopy(SEM).The reactive oxygen species release(ROS)was evaluated using the 2’7’-dichlorodihydrofluorescein diacetate(DCFH-DA)*** results demonstrated that Zr-30Ta and Zr-25Ta-5Ti alloys had favorable smooth,hydrophilic,negatively charged surfaces that decreased bacteria adhesion and prevented biofilm ***-30Ta and Zr-25Ta-5Ti alloys also exhibited a time-dependent decrease in the bacteria adhesion and ***-30Ta and Zr-25Ta-5Ti alloys were also found to induce direct membrane damage and increase ROS production,resulting in significantly better antibacterial activities than ***-30Ta and Zr-25Ta-5Ti alloys exhibited comparable antibacterial *** work suggests that the newly developed Zr-30Ta and Zr-25Ta-5Ti alloys have good antibacterial activity against Streptococcus mutans and Porphyromonas gingivalis and are promising candidate materials for dental and orthopedic implants.

关键词： Zirconium-tantalum Dental implant Antibacterial Peri-implant infection Biofilm

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Optimization of mechanical and antibacterial properties of Ti-3wt%Cu alloy through cold rolling and annealing

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Rare Metals 2022年第2期41卷 610-620页

作者： Hai-Lin Yang meng-zhen zhu Jian-Ying Wang Chen-Xu Ma Xiong-Wen Zhou Hai-Xia Xing Er-Lin Zhang Shou-Xun Ji State Key Laboratory of Powder Metallurgy Central South UniversityChangsha 410083China Department of Prosthodontics Centre of StomatologyXiangya HospitalCentral South UniversityChangsha 410008China Department of General Dentistry Peking University School and Hospital of StomatologyBeijing 100081China Key Laboratory for Anisotropy and Texture of Materials School of Materials Science and EngineeringEducation Ministry of ChinaNortheastern UniversityShenyang 110819China Brunel Centre for Advanced Solidification Technology(BCAST) Brunel University LondonUxbridge UB83PHUK

In this work,a process of cold rolling with 70%thickness reduction and different annealing temperatures was selected to regulate the microstructure of Ti-3wt%Cu *** evolution,mechanical properties and antibacterial properties of the Ti-3wt%Cu alloy under different conditions were systematically investigated in terms of X-ray diffraction(XRD),scanning electron microscope(SEM),transmission electron microscope(TEM),tensile and antibacterial *** results indicated that cold rolling could dramatically increase the ultimate tensile stress(UTS)from 520 to 928 MPa,but reduce the fracture strain from 15.3%to 3.8%.With the annealing temperature increasing from 400 to 800C for 1 h,the UTS decreased from 744 to 506 MPa and the fracture strain increased from12.7%to 24.4%.Moreover,the antibacterial properties of the Ti-3wt%Cu alloy under different conditions showed excellent antibacterial rate(>96.69%).The results also indicated that the excellent combination of strength and ductility of the Ti-3wt%Cu alloy with cold rolling and following annealing could be achieved in a trade-off by tuning the size and distribution of Ti2Cu phase,which could increase the applicability of the alloy in clinical *** importantly,the antibacterial properties maintained a good stability for the Ti-3wt%Cu alloy under different *** excellent combination of mechanical properties and antibacterial properties could make the Ti-3wt%Cu alloy a good candidate for long-term orthopaedic implant application.

关键词： Titanium alloys Mechanical properties Antibacterial property Microstructure Plastic deformation Orthopaedic implant application

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Copper release and ROS in antibacterial activity of Ti-Cu alloys against implant-associated infection

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Rare Metals 2023年第6期42卷 2007-2019页

作者： Hai-Lin Yang Ling Zou Akram Nasser Juaim Chen-Xu Ma meng-zhen zhu Fei Xu Xiao-Na Chen Yin-Zhou Wang Xiong-Wen Zhou State Key Laboratory of Powder Metallurgy Central South UniversityChangsha410083China National Clinical Research Center for Geriatric Disorders Xiangya HospitalCentral South UniversityChangsha410008China Department of Prosthodontics Center of StomatologyXiangya HospitalCentral South UniversityChangsha410008China Department of Oral Implantology Xiangya Stomatological Hospital and Xiangya School of StomatologyCentral South UniversityChangsha410008China Department of Prosthodontics Faculty of DentistryThamar UniversityDhamarYM999101Yemen Center of Stomatology Xiangya HospitalCentral South UniversityChangsha410008China

Enhancing the antibacterial properties of the currently used implant materials is a major concern of healthcare providers to minimize the impact of peri-implant infection and improve implant survival *** this study,titanium-copper sintered alloys(3 wt% and 5 wt%Cu) were developed for medical implant *** phase identification,microstructure,copper ions release,and wettability of these alloys were evaluated using X-ray diffraction(XRD),optical microscope(OM),scanning electron microscope(SEM),transmission electron microscope(TEM),energy-dispersive X-ray spectroscope(EDS),inductively coupled plasma spectroscope(ICP) and drop shape *** antibacterial activities of Ti-Cu alloys against Porphyromonas gingivalis and Streptococcus mutans were evaluated using inhibition zone assay,plate counting assay,live/dead fluorescent staining,SEM and reactive oxygen species(ROS) staining *** results demonstrated that Ti-Cu alloys are composed of α-Ti and Ti_(2)Cu phases that increased with increased Cu content of the ***-Cu alloys exhibited antibacterial activity against both bacteria species in a time-dependent *** antibacterial rates of Ti-3Cu and Ti-5Cu after72 h were 57% and 70% against Porphyromonas gingivalis and 63% and 78% against Streptococcus mutans,*** highest amount of Cu^(2+) released from these alloys was 0.3 mg·L^(-1) during the first 24 h,within the safe *** copper ions release and ROS production were suggested as the main antibacterial ***,Ti-Cu sintered alloys are promising materials for dental and orthopedic implants.

关键词： Titanium-copper alloy Antibacterial Dental implant Ti_(2)Cu Copper release

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Reducing Operation Emissions and Improving Work Efficiency Using a Pure Electric Wheel Drive Tractor

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Engineering 2024年第6期37卷 230-245页

作者： Chang-Kai Wen Wen Ren Qing-zhen zhu Chun-Jiang Zhao zhen-Hao Luo Sheng-Li Zhang Bin Xie Zhi-Jun meng Research Center of Intelligent Equipment Beijing Academy of Agriculture and Forestry SciencesBeijing 100097China State Key Laboratory of Intelligent Agricultural Power Equipment Beijing 100097China BYD Company Limited Shenzhen 518118China College of Agricultural Engineering Jiangsu UniversityZhenjiang 212013China College of Engineering China Agricultural UniversityBeijing 100083China

In response to the problems of excessive greenhouse-gas and particulate emissions and the low traction efficiency of conventional diesel tractors in the field,a purely electric wheel-side drive tractor was studied,including an electric motor drive system,a battery ballast system,and an electro–hydraulic suspension *** paper develops a dynamics model of an electric tractor-ploughing unit under complex soil conditions,leading to the proposal of an active control method for drive wheel torque and a joint control method for the traction force of the suspension system and the front-and rear-axle loads of a ***,the tractor is prototyped and assembled,and ploughing tests are carried *** ploughing results show that the active torque-distribution control method proposed in this study reduces the tractor slip by 14.83%and increases the traction efficiency by 10.28%compared with the average torquedistribution *** with the conventional traction control mode,the joint control method for traction and ballast proposed in this paper results in a 3.7%increase in traction efficiency,a 15.05%decrease in slip,and a 4.9%reduction in total drive motor energy *** study will help to improve the operation quality and traction efficiency of electric tractors in complex soil conditions.

关键词： Electric tractor Ploughing unit Torque distribution Active ballast Traction performance

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Multi-distortion suppression for neutron radiographic images based on generative adversarial network

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Nuclear Science and Techniques 2024年第4期35卷 176-188页

作者： Cheng-Bo meng Wang-Wei zhu zhen Zhang Zi-Tong Wang Chen-Yi Zhao Shuang Qiao Tian Zhang School of Physics Northeast Normal UniversityChangchun 130024China

Neutron radiography is a crucial nondestructive testing technology widely used in the aerospace,military,and nuclear ***,because of the physical limitations of neutron sources and collimators,the resulting neutron radiographic images inevitably exhibit multiple distortions,including noise,geometric unsharpness,and white ***,these distortions are particularly significant in compact neutron radiography systems with low neutron ***,in this study,we devised a multi-distortion suppression network that employs a modified generative adversarial network to improve the quality of degraded neutron radiographic *** neutron radiographic image datasets with various types and levels of distortion were built for the first time as multi-distortion suppression ***,the coordinate attention mechanism was incorporated into the backbone network to augment the capability of the proposed network to learn the abstract relationship between ideally clear and degraded *** experiments were performed;the results show that the proposed method can effectively suppress multiple distortions in real neutron radiographic images and achieve state-of-theart perceptual visual quality,thus demonstrating its application potential in neutron radiography.

关键词： Neutron radiography Multi-distortion suppression Generative adversarial network Coordinate attention mechanism

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Research status and perspectives of MXene-based materials for aqueous zinc-ion batteries

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Rare Metals 2024年第5期43卷 1867-1885页

作者： Xiao-Yu Wang Qi-Hang Yang Xin-Yan meng meng-meng zhen zhen-Zhong Hu Bo-Xiong Shen School of Energy and Environmental Engineering Hebei University of TechnologyTianjin 300071China

Aqueous zinc-ion batteries(AZIBs)as green battery systems have attracted widespread attention in large-scale electrochemical energy storage devices,owing to their high safety,abundant Zn materials,high theoretica specific capacity and low redox *** there are some thorny issues in AZIBs that hinder their practical application,such as low intrinsic electron conductivity,slow ion migration kinetics,zinc dendrites and side ***-based materials with superior conductivity,large polar surface and abundant active sites can simultaneously serve as cathode materials,electrolyte additive and protection layer of anode to regulate redox reactions of *** various materials have been used to improve electrochemical performances of AZIBs there is a lack of in-depth discussion on the regulation mechanism of MXene-based materials for *** this review,we elaborate the research progress of MXenebased materials in AZIBs,including their application in cathode materials and inhibition of zinc *** the future prospects and development directions of MXenebased materials that may improve performance of AZIBs are prospected.

关键词： MXene Aqueous zinc-ion batteries Composite materials Zinc dendrites

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Progress and challenges of electrolyte modulation in aqueous zinc-ion batteries

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Rare Metals 2024年第7期43卷 2940-2967页

作者： Qi-Hang Yang Lu-Fei Wang Xiao-Yu Wang meng-meng zhen Tianjin Key Laboratory of Clean Energy and Pollution Control School of Energy and Environmental EngineeringHebei University of TechnologyTianjin 300071China

As a new type of green battery system,aqueous zinc-ion batteries(AZIBs)have gradually become a research hotspot due to their low cost,high safety,excellent stability,high theoretical capacity(820 mAh·g^(-1))of zinc anode,and low redox potential(-0.76 V *** hydrogen electrode(SHE)).AZIBs have been expected to be an alternative to lithium-ion batteries for large-scale commercial energy storage ***,they are facing thorny issues such as degradation of cycling performance,zinc dendrites,and side *** the same time,these problems cause short cycling life of batteries,thus severely limiting their commercial *** recent years,many more researches have been conducted on the modification of anode and cathode materials of AZIBs,but there is a lack of in-depth discussion on the characteristics and mechanism of electrolyte *** this review,we will make a systematic summary of the current problems with two electrodes in AZIBs,as well as the types and functions of electrolyte ***,we further systematically describe the modulation mechanism of electrolyte additives in the performance of the cathode and *** prospects and development directions of additive modulation strategies for AZIBs electrolytes are prospected.

关键词： Electrolyte additives Aqueous zinc-ion batteries Zinc anode protection Cathode chemistry

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Status and progress of metal-supported solid oxide fuel cell: Towards large-scale manufactory and practical applications

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Energy Reviews 2024年第1期3卷 1-23页

作者： Haoran Xu Yu Han Jing zhu meng Ni zhen Yao State Key Laboratory of Clean Energy Utilization Zhejiang University38 Zheda RoadHangzhou310027China Department of Building and Real Estate Research Institute for Sustainable Urban Development(RISUD)&Research Institute for Smart Energy(RISE)Hong Kong Polytechnic UniversityHung HomKowloonHong KongChina Fakultät für Physik Universität BielefeldUniversitätsstr.2533615BielefeldGermany

Metal-supported solid oxide fuel cells(MS-SOFCs)own advantages of high performance,fast start-up,thermal cycle stability,easy sealing,and reduced material *** recent years,significant progress has been made in the development of MS-SOFCs,particularly with respect to improved electrochemical performance,long-term stability,and industrial *** studies have mainly focused on stainless steel-based MS-SOFCs,with an emphasis on the development of low-temperature preparation processes,antioxidant coatings,stable electrodes,and the direct utilization of hydrocarbon ***,Ceres Power and GE have successfully commercialized MS-SOFCs and have constant cooperated with several institutions and companies,such as Jülich Research Center,Weichai and Cummins,to promote the performance and expand the market of *** ahead,this review paper provides an outlook on future research directions in this rapidly evolving field.

关键词： Metal support Solid oxide fuel cell High performance Long-term stability

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For LEO Satellite Networks: Intelligent Interference Sensing and Signal Reconstruction Based on Blind Separation Technology

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China Communications 2024年第2期21卷 85-95页

作者： Chengjie Li Lidong zhu zhen Zhang The Key Laboratory for Computer Systems of State Ethnic Affairs Commission School of Computer Science and Technology(Southwest Minzu University)Chengdu 610000China National Key Laboratory of Science and Technology on Communications(University of Electronic Science and Technology of China) Chengdu 610000China College of Computer Science(Sichuan University) Chengdu 610000China

In LEO satellite communication networks,the number of satellites has increased sharply, the relative velocity of satellites is very fast, then electronic signal aliasing occurs from time to time. Those aliasing signals make the receiving ability of the signal receiver worse, the signal processing ability weaker,and the anti-interference ability of the communication system lower. Aiming at the above problems, to save communication resources and improve communication efficiency, and considering the irregularity of interference signals, the underdetermined blind separation technology can effectively deal with the problem of interference sensing and signal reconstruction in this scenario. In order to improve the stability of source signal separation and the security of information transmission, a greedy optimization algorithm can be executed. At the same time, to improve network information transmission efficiency and prevent algorithms from getting trapped in local optima, delete low-energy points during each iteration process. Ultimately, simulation experiments validate that the algorithm presented in this paper enhances both the transmission efficiency of the network transmission system and the security of the communication system, achieving the process of interference sensing and signal reconstruction in the LEO satellite communication system.

关键词： blind source separation greedy optimization algorithm interference sensing LEO satellite communication networks signal reconstruction

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Neuroprotective and anti-inflammatory effects of eicosane on glutamate and NMDA-induced retinal ganglion cell injury

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International Journal of Ophthalmology(English edition) 2024年第4期17卷 638-645页

作者： zhen-Kai Wu Huan-Yu Li You-Lin zhu meng-Qin Xiong Jing-Xiang Zhong Department of Ophthalmology the First Affiliated Hospital of Jinan UniversityGuangzhou 510632Guangdong ProvinceChina Changde Hospital Xiangya School of MedicineCentral South University(the First People’s Hospital of Changde City)Changde 415000Hunan ProvinceChina

AIM:To investigate the protective effects,antioxidant potential,and anti-inflammatory mechanisms of eicosane on glutamate-induced cell damage and on N-methyl-Daspartate(NMDA)-induced retinal ganglion cell(RGC)injury in a mouse model of ***:The protective effects of eicosane on the rat R28 retinal precursor cell line were assessed using cell counting kit-8 assays and Hoechst-propidium iodide *** reactive oxygen species(ROS)production was measured using the fluorescent probe 2'-7'-dichlorofluorescin diacetate and flow *** protective role of eicosane on NMDA-induced RGC injury in a mouse glaucoma model was determined by immunostaining of frozen sections of *** effects of eicosane on the metabolome of the retina in mice with NMDA-induced RGC damage were evaluated by liquid chromatographymass spectroscopy(LC-MS)and untargeted metabolomics ***:Eicosane treatment significantly attenuated glutamate-induced damage to R28 cells in *** also protected RGCs against NMDA-induced injury in a mouse glaucoma *** metabolomics analyses showed that eicosane increased multiple metabolites,including L-arginine and L-carnitine,in the ***:Eicosane has protective effects,antioxidant potential,and anti-inflammatory properties in an in vitro model of glutamate-induced cell damage and in an in vivo model of NMDA-induced RGC injury in mouse glaucoma through modulation of L-arginine and/or L-carnitine metabolism.

关键词： glaucoma metabolites eicosane

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