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Novel method for the preparation of Cs-containing FAU（Y） catalysts for aniline methylation

Frontiers of Chemical Science and Engineering 2018年第1期12卷 70-76页

作者： Olga A. Ponomareva Polina A. Shaposhnik marin. vo belova Boris A. Kolozhvari Irina I. Ivanova Department of Chemistry Lomonosov Moscow State University Moscow 119991 Russia A.V. Topchiev Institute of Petrochemical Synthesis Moscow Russia

Cs-containing FAU（Y）-type zeolite catalysts were prepared by conventional and novel ion exchange procedures followed by incipient wetness impregnation with CsOH. The novel ion exchange procedure involved hydrothermal treatment of NaY zeolite in aqueous solution of CsCl at 140-200 ℃ for 6-24 h. The samples were characterized by low-temperature nitrogen adsorption, X-ray fluorescence analysis, X-ray powder diffraction, scanning electron microscopy, 23Na, 27Al and 133Cs magic angle spinning nuclear magnetic resonance, CO2 and NH3-Temperature programmed desorption. The results show that hydrothermal treatment at 200 ℃ allows to obtain higher degrees of ion-exchange （up to 83%） with respect to conventional method giving maximum 66%- 69%. Catalytic properties of Cs-containing FAU（Y） were studied in aniline methylation. The yield of Nomethylani- line is shown to correlate with catalyst＇s basicity. The best catalyst performance was achieved over the catalyst with the highest ion-exchange degree impregnated with CsOH. The selectivity to N-methylaniline over this catalyst reached 96.4%.

关键词： FAU(Y) zeolite ion exchange with cesium aniline alkylation N-methylaniline

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Heart rate variability to assess ventilatory thresholds in professional basketball players

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Journal of Sport and Health Science 2017年第4期6卷 468-473页

作者： Domingo Jesús Ramos-Campo Jacobo A. Rubio-Arias Vicente Avila-Gandia Cristian marin.Pagan Antonio Luque Pedro E. Alcaraz Department of Physical Activity and Sport Science Faculty of Sports Catholic University ofMurcia Murcia 30107 Spain Department of Physiology Catholic University ofMurcia Murcia 30}07 Spain UCAM Research Center for High Performance Sport Mureia 30107 Spain

Purpose: The aim of this study was to determine if heart rate variability(HRV) during incremental test could be used to estimate ventilatory threshold(VT) in professional basketball players, with sufficient precision to be used in their training. Furthermore, the second aim was to analyse the association between HRV and 3 methods of VT determination by gas ***: Twenty-four professional basketball players(age: 23.4 ± 4.9 years; height: 195.4 ± 9.8 cm; body mass: 92.2 ± 11.9 kg) performed an incremental running test to exhaustion. First ventilatory threshold(VT1) was determined by ventilatory equivalent(VE) and HRV and second ventilatory threshold(VT2) was determined by 3 methods of gases analysis(V-slope, VE and gas exchange ratio(R), and HRV). Pearson's coefficient(r) was used to detect differences between data and the strength of each relationship. The mean of absolute differences and Bland–Altman analysis were used to evaluate whether there was ***: The results showed no significant differences in HR and oxygen consumption(vo2) at VT1 between the 2 methods. Furthermore, no significant differences among the methods of gases analysis and HRV were observed in speed, HR, and vo2 at VT2. Moreover, VTs estimated using HRV and gas methods were significantly correlated. Correlation in HR values was higher between R and HRV(r = 0.96) and VE and HRV(r = 0.96) than V-slope and HRV(r = 0.90).Conclusion: These findings provide a practical, inexpensive approach for evaluating specific training loads when determining VT2 in basketball players. Therefore, HRV is an alternative method to determine VT2 without the application of expensive technology that limits its use to laboratories.

关键词： Anaerobic threshold Basketball Oxygen uptake Performance Training Ventilatory threshold

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Study of the production of Λ_b^0 band ~0 hadrons in pp collisions and first measurement of the Λ_b^0→J/ψpK^- branching fraction

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Chinese Physics C 2016年第1期40卷 1-16页

作者： O.Kochebina M.Kolpin I.Komarov R.F.Koopman P.Koppenburg M.Kozeiha L.Kravchuk K.Kreplin M.Kreps G.Krocker P.Krokovny F.Kruse W.Krzemien W.Kucewicz M.Kucharczyk V.Kudryavtsev A.K.Kuonen K.Kurek T.Kvaratskheliya D.Lacarrere G.Lafferty A.Lai D.Lambert G.Lanffanchi C.Langenbruch B.Langhans T.Latham C.Lazzeroni R.Le Gac J.van Leerdam J.-P.Lees R.Lefevre A.Leflat J.Lefrancois E.Lemos Cid O.Leroy T.Lesiak B.Leverington Y.Li T.Likhomanenko M.Liles R.Lindner C.Linn F.Lionetto B.Liu X.Liu D.Loh I.Longstaff J.H.Lopes D.Lucchesi M.Lucio Martinez H.Luo A.Lupato E.Luppi O.Lupton A.Lusiani F.Machefert F.Maciuc O.Maev K.Maguire S.Malde A.Malinin G.Manca G.Mancinelli P.Manning A.Mapelli J.Maratas J.F.Marchand U.Marconi C.marin.Benito P.marin. J.Marks G.Martellottil M.Martin M.Martinelli D.Martinez Santos F.Martinez Vidal D.Martins Tostes A.Massafferri R.Matev A.Mathad Z.Mathe C.Matteuzzi A.Mauri B.Maurin A.Mazurov M.McCann J.McCarthy A.McNab R.McNulty B.Meadows F.Meier M.Meissner D.Melnychuk M.Merk E Michielin D.A.Milanes M.-N.Minard D.S.Mitzel J.Molina Rodrigue I.A.Monroy S.Monteil M.Morandin P.Morawski A.Morda M.J.Morello J.Moron A.B.Morris R.Mountain F.Muheim D.Miiller J.Muller K.Muller V.Muller M.Mussini B.Muster P.Naik T.Nakada R.Nandakumar A.Nandi I.Nasteva M.Needham N.Neri S.Neubert N.Neufeld M.Neuner A.D.Nguyen T.D.Nguyen C.Nguyen-Mau V.Niess R.Niet N.Nikitin T.Nikodem D.Ninci A.Novoselov D.P.O'Hanlon A.Oblakowska-Mucha V.Obraztsov S.Ogilvy O.Okhrimenko R.Oldeman C.J.G.Onderwater B.Osorio Rodrigues J.M.Otalora Goicochea A.Otto P.Owen A.Oyanguren A.Palano F.Palombo M.Palutan J.Panman A.Papanestis M.Pappagallo L.L.Pappalardo C.Pappenheimer C.Parkes G.Passaleva G.D.Patel M.Patel C.Patrignani A.Pearce A.Pellegrino G.Penso M.Pepe Altarelli S.Perazzini P.Perret L.Pescatore K.Petridis A.Petrolini M.Petruzzo E.Picatoste Olloqui B.Pietrzyk T:.Pilar D.Pinci A.Pistone A.Piucci S.Playfer M.Plo Casasus T.Poikela F.Polci A.Poluektov I.Polyakov E.Polycarpo A.Popov D.Popov B.Popovici C.Potterat E.Price J.D.Price J.Prisciandaro A.Pritchard Centro Brasileiro de Pesquisas Ffsicas(CBPF) Rio de JaneiroBrazil Universidade Federal do Rio de Janeiro(UFRJ) Rio de JaneiroBrazil Center for High Energy Physics Tsinghua UniversityBeijingChina LAPP Universite Savoie Mont-BlancCNRS/IN2P3Annecy-Le-VieuxFrance Clermont Universite Universite Blaise PascalCNRS/IN2P3LPCclermont-FerrandFrance CPPM Aix-Marseille UniversitYCNRS/IN2P3MarseilleFrance LAL Universite Paris-SudCNRS/IN2P3OrsayFrance LPNHE Universite Pierre et Marie CurieUniversite Paris DiderotCNRS/IN2P3ParisFrance Fakultat Physik Technische Universitat DortmundDortmundGermany Max-Planck-lnstitut fur Kernphysik(MPIK) HeidelbergGermany Physikalisches Institut Ruprecht-Karls-Universitat HeidelbergHeidelbergGermany School of Physics University College DublinDublinIreland Sezione INFN di Bari BariItaly Sezione INFN di Bologna BolognaItaly Sezione INFN di Cagliari CagliariItaly Sezione INFN di Ferrara FerraraItaly Sezione INFN di Firenze FirenzeItaly Laboratori Nazionali dell'INFN di Prascati FrascatiItaly Sezione INFN di Genova GenovaItaly Sezione INFN di Milnno Bicocca MilunoItaly Sezione INFN di Milano MilanoItaly Sezione INFN di Padova PadovaItaly Sezione INFN di Pisa PisaItaly Sezione INFN di Roma Tor Vergata RomaItaly Sezione INFN di Roma La Sapienza RomaItaly Henryk Niewodniczanski Institute of Nuclear Physics Polish Academy of Sciences Krak6wPoland AGH-University of Science and Technology Faculty of Physics and Applied Computer ScienceKrakowPoland National Center for Nuclear Research(NCBJ) WarsawPoland Horia Hulubei National Institute of Physics and Nuclear Engineering Bucharest-MagureleRomania Petersburg Nuclear Physics Institute(PNPI) GatchinaRussia Institute of Theoretical and Experimental Physics(ITEP) MoscowRussia Institute of Nuclear Physics Moscow State University(SINP MSU)MoscowRussia Institute for Nuclear Research of the Russian Academy of Sciences(INR RAN) MoscowRussia Budker Institute of Nuclear Physics(SB RAS)and Novosibirsk State University No

The product of the ∧0/b （-B/0） differential production cross-section and the branching fraction of the decay ∧0/b→ J/ψ pK-（-B/0→ J/ψ-K＊（892）0）is measured as a function of the beauty hadron transverse momentum, PT, and rapidity, y. The kinematic region of the measurements is pT〈20 GeV/c and 2.0 〈g〈*** measurements use a data sample corresponding to an integrated luminosity of 3fb-1 collected by the LHCb detector in pp collisions at centre-of-mass energies √s=7 TeV in 2011 and √s=8 TeV in 2012. Based on previous LHCb results of the fragmentation fraction ratio,f∧0/b/fd,the branching fraction of the decay ∧0/b→ J/ψ pK-is measured to be B（∧0/b→ J/ψ pK-）=（3.17±0.04±0.07±0.34＋0.45/-0.28）×10-4,where the first uncertainty is statistical, the second is systematic, the third is due to the uncertainty on the branching fraction of the decay -B/0 →J/ψ-K＊（892）0,and the fourth is due to the knowledge of f∧0/b/*** sum of the asymmetries in the production and decay between ∧0/b and ∧0/bis also measured as a function of PT and *** previously published branching fraction of ∧0/b→ J/ψ pπ-,relative to that of ∧0/b→ J/ψ pK-,is updated. The branching fractions of ∧0/b→P＋c（→ J/ψp）K-are determined.

关键词： production cross-section branching fraction b hadrons proton-proton collisions

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