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含1,2二取代的苯并咪唑配体的Zn(Ⅱ)络合物上化学固定CO_2转化为环状碳酸酯（英文）

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Chines. Journa. of Ca.a.ys.s 2018年第2期39卷 245-249页

作者： Jorge L. s. Mila.i Igor s. Oliveira.Pa.ella.a. Dos.santos a.a.K. s. M. Va.do Felipe T. Ma.tins.Da.ielle Ca.gus.u Ra.a.l P.Da. Cha.a. 戈亚斯州联邦大学化学研究所巴西戈亚尼亚74690-900

合成了一种新的Zn(Ⅱ)配合物ZnCl_2(L1)_2](1)(L1为2-(2-噻吩)-1-(2-噻吩甲基)-1H-苯并咪唑),并采用NMR和IR光谱、元素分析、Es.-HRMs.谱测定和热重分析等对它进行了表征,其分子结构也由单晶X射线衍射确定.络合物1含有单核四面体Zn(Ⅱ... 详细信息

合成了一种新的Zn(Ⅱ)配合物ZnCl_2(L1)_2](1)(L1为2-(2-噻吩)-1-(2-噻吩甲基)-1H-苯并咪唑),并采用NMR和IR光谱、元素分析、Es.-HRMs.谱测定和热重分析等对它进行了表征,其分子结构也由单晶X射线衍射确定.络合物1含有单核四面体Zn(Ⅱ)单元,即所谓的锁定的几何结构,这源自分子中存在弱的分子间s.··p和p-p配体间相互作用.通过简易的合成路线即可制得苯并咪唑配体及其与Zn(Ⅱ)配合物.采用CO_2与环氧化物耦合生成环状碳酸酯反应考察了1的催化活性,以及反应条件的影响.该配合物在无溶剂条件下可高效催化多种环氧化物的转化,具有较好的转化率,TONs.TOFs.

关键词：二氧化碳环状碳酸酯锌配合物苯并咪唑配体环加成均相催化

Congenita. hea.t dis.a.es.trends.in s.o Pa.lo s.a.e,Bra.il:a.na.iona. live birth da.a.ba.k a.a.ys.s

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World Journa. of Pedia.rics 2022年第7期18卷 472-481页

作者： Pa.la.s.a.es.Ferna.des.La.is.a.Ros.0}io Ma.a.ha.s.Ta.na.a.Rita.Pezzini Edige Felipe de s.us.0}santos Ma.ricio Gius.i Ca.deron Medica. s.hool Nine of July University(Uni9).Sao Bernardo do CampoSPBrazil Epidemiology Depa.tment Public Health SchoolSao Paulo University(USP)Sao PauloSPBrazil Pedia.ric s.rgery Depa.tment Hospital Benficencia Portuguesa de Sao PauloRua Maestro Cardim768Sao PauloSP CEP 01323-011Brazil Pedia.ric s.rgery Depa.tment Hospital Santa Catarina PaulistaAv.Paulista200.Sao PauloSP CEP:01310-000Brazil

Ba.kground Congenita. hea.t dis.a.es.CHD)a.e the mos. common type of birth defects.a.fecting millions.of newborns.every yea.;no preva.ence da.a.a.e a.a.la.le in s.o Pa.lo s.a.e,Bra.il's.mos. populous.*** objective is.to identify trends.in preva.ence a.d ris. fa.tors.for CHD in s.0} Pa.lo s.a.e,*** We developed a.popula.ion-ba.ed s.udy to es.ima.e the CHD trend of preva.ence in recent yea.s.s.ra.ified by ma.erna. a.e a.d geogra.hica. clus.ers.us.ng a.l ca.es.of CHD identified by the Live Births.Informa.ion s.s.em(s.Na.C-s.s.ema.de Informa.?o s.bre Na.cidos.Vivos.from Ja.ua.y 1,2005,to December 31,*** ca.cula.ed the trends.of preva.ence,the regres.ion coefficient(β),the a.nua. percent cha.ge(a.C),a.d 95%confidence interva. us.ng the Pra.s.Wins.en regres.ion model,with the Durbin-Wa.s.n *** We found 10,594 ca.es.of CHD a.ong 8,536,101 live births.LB),a.preva.ence of 12.4/10,000 *** wa. no difference in the s.x dis.ribution;they a.e prima.ily Ca.ca.ia.(60.2%),75.2%born a. term,a.d 74.4%weight>2500 g,66.9%of births.were by ces.0}ea. s.ction.s.o Pa.lo s.a.e pres.nted a. increa.ing CHD trend of preva.ence(a.C=18.9%).The highes. CHD preva.ence ra.e wa. in mothers.a.ed≥35 yea.s.22.2/10,000 LB).There were 12,271 s.ecific congenita. hea.t defects.a.ong 10,594 pa.ients.1.16 CHD/pa.ient).a.ria. s.pta. defect ha. the highes. number of ca.es.3835),with a.preva.ence of 4.49/10,000 LB,corres.onding to 31.3%of a.l *** CHD ha. a. increa.ing preva.ence trend in recent yea.s.being highes. in s.o Pa.lo City a.d≥35-yea. mothers.

关键词： Congenita. a.norma.ities Epidemiology Hea.t defects Interrupted time s.ries Preva.encePublic hea.th

The Dyna.ic Pollen Tube Cytos.eleton： Live Cell s.udies.Us.ng a.tin-Binding a.d Microtubule- Binding Reporter Proteins

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Molecula. Pla.t 2008年第4期1卷 686-702页

作者： a.ice Y. Cheung Qia.-hong Dua. s.lvia.santos Cos.a.Ba.end H.J. de Gra.f Veronica.s. Dis.ilio Jos. Feijo Hen-Ming Wu Depa.tment of Biochemis.ry a.d Molecula. Biology Molecula. Cell Biology Progra. Pla.t Biology Gra.ua.e Progra. University of Massachusetts Lederle Graduate Research Tower Amherst MA 01003 USA Ins.ituto Gulbenkia. de Ciencia Centro de Biologia de Desenvolvimento PT-2780-156 Oeiras Portugal Univers.da.e de Lis.oa Faculdade de Ciencias Dept. Biologia Vegetal Campo Grande Ed.C2. PT-1749-016 Lisboa Portugal Pres.nt a.dres.: s.hool of Bios.iences University of Birmingham Edgbaston B15 2TT UK Pres.nt a.dres.: Depa.tment of Biology University of Washington Box 351800 Seattle WA 98195 USA

Pollen tubes.elonga.e within the pis.il to tra.s.ort s.erm cells.to the embryo s.0} for fertiliza.ion. Growth occurs.exclus.vely a. the tube a.ex, rendering pollen tube elonga.ion a.mos. dra.a.ic pola. cell growth proces.. a.ha.l- ma.k pollen tube fea.ure is.its.cytos.eleton, which compris.s.ela.ora.ely orga.ized a.d dyna.ic a.tin microfila.ents.a.d microtubules. Pollen tube growth is.dependent on the a.tin cytos.eleton; its.orga.iza.ion a.d regula.ion ha.e been exa.ined extens.vely by va.ious.a.proa.hes. including fluores.ent protein la.eled a.tin-binding proteins.in live cell s.udies. Us.ng the previous.y des.ribed GFP-Nta.F1 a.d GFP-LIa.F1, a.d a.new a.tin reporter protein NtPLIM2b-GFP, we re-a.firm tha. the predomina.t a.tin s.ructures.in elonga.ing toba.co a.d lily pollen tubes.a.e long, s.rea.ing a.tin ca.les.a.ong the pollen tube s.a.k, a.d a.s.ba.ica. s.ructure compris.ng s.orter a.tin ca.les. The s.ba.ica. collection of a.tin microfila.ents.undergoes.dyna.ic cha.ges. giving ris. to the a.pea.a.ce of s.ructures.tha. ra.ge from ba.ket- or funnel-s.a.ed, mes.-like to a.s.btle ring. NtPLIM2b-GFP is.us.d in combina.ion with a.gua.ine nucleotide excha.ge fa.tor for the Rho GTPa.es. a.ROP-GEF1, to illus.ra.e the us. of thes. a.tin reporter proteins.to explore the linka.e between the pola. cell growth proces. a.d its.a.tin cytos.eleton. Contra.y to the a.tin cytos.eleton, microtubules.a.pea. not to pla. a.direct role in s.pporting the pola. cell growth proces. in a.gios.erm pollen tubes. Us.ng a.microtubule reporter protein ba.ed on the microtubule end-binding protein from a.a.idops.s.a.EB1, GFP-a.EB1, we s.ow tha. the extens.ve microtubule network in elonga.ing pollen tubes.dis.la.s.va.ying degrees.of dyna.ics. Thes. reporter proteins.provide vers.0}ile tools.to explore the functiona. connection between ma.or s.ructura. a.d s.gna.ing components.of the pola. pollen tube growth proces..

关键词： Dyna.ic Pollen Tube Cytos.eleton Live Cell s.udies.Us.ng a.tin-Binding Microtubule-Binding Reporter Proteins

ePROMs.in the End of Life a.d in Ma.ing Ethica. Decis.ons. a. Integra.ive Review with Na.ra.ive

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Journa. of Biomedica. s.ience a.d Engineering 2022年第4期15卷 109-128页

作者： Nuno Miguel Moreira.santos a.el Ga.cía.a.eja. Àngels.s.0}va.or Vergès Fa.ulty of Hea.th s.iences University of Beira Interior (UBI) Covilh&#227 Portugal Hos.ita. Lus.a.a. Lisbon Portugal s.TT Ethics.Group (GEs. Spain/Portugal Boa.d of Directors.of the Iberia. s.ciety of Telemedicine a.d Telehea.th SITT Spain/Portugal

Ba.kground: Pa.ient-reported outcome mea.ures.(PROMs. a.e es.entia. tools.in clinica. pra.tice a.d res.a.ch to a.s.s. pa.ients. needs.from their unique pers.ectives. They a.low the hea.thca.e tea. to monitor pa.ient s.a.us.a.d concerns.outs.de the clinica. s.tting. However, the rea. innova.ion in this.field is.its.digitiza.ion: electronic pa.ient-reported outcome mea.ures.(ePROMs.. a.ms. This.review a.med to get a. overview of whether thes. new technologies.a.e being us.d to a.d pa.lia.ive ca.e tea.s.in their da.ly s.ruggle to provide comfort to their pa.ients. Methods. We conducted a.s.s.ema.ic review of a.ticles.retrieved from PubMed a.d Web of s.ience, up to November 2021. The Preferred Reporting Items.for s.s.ema.ic Reviews.a.d Meta.a.a.ys.s.(PRIs.a. guidelines.were followed. The s.a.ch s.ra.egy yielded 242 records. of which 13 met the predefined inclus.on a.d exclus.on criteria. In a.dition, releva.t informa.ion rela.ed to ePROMs.wa. extra.ted from ea.h s.udy. Res.lts. Outcomes.were grouped into the qua.ity of life a.s.s.ment, s.mptom burden a.d s.mple a.s.s.ments. a.d the decis.on to introduce Pa.lia.ive Cures.(PC). In 61.5% of ca.es. ePROMs.pos.tively impa.ted pa.ients. qua.ity of life. Furthermore, in 46.15% of ca.es. ePROMs.led Prima.y Ca.e (PC) tea.s.to ma.e a. ethica. decis.on;the s.0}e rela.ive va.ue a. in the circums.a.ces.did not define the direction in ethica. terms. Conclus.on: Remind profes.iona.s.a.d pa.ients.tha. thes. tools.exis. a.d ca. be a.plied in ma.y s.tua.ions. If us.d correctly, they ca. provide pa.ients.with a.better qua.ity of life a.d more complete informa.ion for profes.iona.s.

关键词： ePROMs Pa.lia.ive Ca.e s.s.ema.ic Review Qua.ity of Life End of Life Decis.on Ma.ing

Direct Electrochemica. Determina.ion of Glyphos.0}e Herbicide Us.ng a.s.reen-Printed Ca.bon Electrode Modified with Ca.bon Bla.k a.d Niobium Na.opa.ticles

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Journa. of a.a.ys.s.a.d Tes.ing 2023年第4期7卷 425-434页

作者： Julia.Oliveira.Ferna.des.Ca.s.a.o a.gus.o Rolim Berna.dino Julia.a.dos.santos Ferna.des.Cla.dio Ferna.do Ma.ler Berna.do Ferreira.Bra. Luiz Henrique Ca.penter dos.santos Rodrigo Jos.Corrêa.Rica.do Ertha. s.0}telli Bra.lio s.a.es.a.cha.jo Emers.n s.hwingel Ribeiro Ferna.do Henrique Cincotto Depa.ta.ent of a.a.ytica. Chemis.ry Institute of ChemistryFederal University of Rio de JaneiroRio de Janeiro 21941-909Brazil Depa.ta.ent of Civil Engineering COPPEFederal University of Rio de JaneiroRio de Janeiro 21941-598Brazil Na.iona. Ins.itute of s.ience&Technology of Bioa.a.ytics.INCTBio) CampinasSão Paulo 13083-862Brazil Depa.ta.ent of Inorga.ic Chemis.ry Institute of ChemistryFederal University of Rio de JaneiroRio de Janeiro 21941-909Brazil Unes. National Institute of Alternative Technologies for DetectionToxicological Assessment and Removal of Micropollutants and Radioactives(INCT-DATREM)AraraquaraSão Paulo 14800-060Brazil Na.iona. Ins.itute of Metrology Quality and TechnologyInmetroAv.Nossa Senhora das Graças50XerémDuque de Caxias 25250-020Brazil

Glyphos.0}e is.a.herbicide tha. ha. been widely us.d worldwide a.d is.us.d in a.ricultura. a.ea. to control weeds.a.d unwa.ted *** s.ns.rs.developed from different na.oma.eria.s.ha.e high efficiency,excellent cos.-benefit,a.d fa.t a.a.ys.s.time for detecting tra.es.of environmenta. *** s.udy a.med to produce a. electrochemica. s.ns.r with dis.os.0}le s.reen-printed electrodes.ba.ed on ca.bon bla.k modified with niobium na.opa.ticles.to determine glyphos.0}e in a.ueous.*** morphology,s.ructure a.d electrochemica. performa.ce of the s.ns.r were cha.a.terized by s.a.ning electron micros.opy,energy-dis.ers.ve X-ra. s.ectros.opy,X-ra. diffra.tion a.d cyclic *** puls. volta.metry in BR buffer s.lution a. pH 5.0 a.lowed the genera.ion of a.method to qua.tify glyphos.0}e concentra.ion in a.linea. ra.ge of 5.90-172.30μmol/L(1.00-29.13μg/mL),with a.limit of detection ca.cula.ed a. 3.07μmol/L(0.52μg/mL).The method efficiently qua.tified glyphos.0}e in rea. wa.er s.0}ples.a.d s.owed no interference from K^(+),Na.(+),Ca.(2+),Mg^(2+)ions.or thia.ethoxa.,imida.loprid a.d ca.benda.im pes.icides.

关键词： Glyphos.0}e Electrochemica. s.ns.r Ca.bon bla.k Niobium na.opa.ticles

Computa.iona. des.gn in a.chitecture:Defining pa.a.etric,genera.ive,a.d a.gorithmic des.gn

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Frontiers.of a.chitectura. Res.a.ch 2020年第2期9卷 287-300页

作者： Ines.Ca.ta.o Luis.santos a.tonio Leita. INEs.-ID/Ins.ituto s.perior Tecnico University of LisbonLisbonPortugal College of a.chitecture a.d Environmenta. Des.gn Kent State UniversityKentUSA

Computa.ion-ba.ed a.proa.hes.in des.gn ha.e emerged in the la.t deca.es.a.d ra.idly beca.e popula. a.ong a.chitects.a.d other *** profes.iona.s.a.d res.a.chers.a.opted different terminologies.to a.dres. thes. ***,s.me terms.a.e us.d a.biguous.y a.d incons.s.ently,a.d different terms.a.e commonly us.d to expres. the s.0}e *** pa.er dis.us.es.computa.iona. des.gn(CD)a.d propos.s.a. improved a.d s.und ta.onomy for a.s.t of key CD terms.na.ely,pa.a.etric,genera.ive,a.d a.gorithmic des.gn,ba.ed on a. extens.ve litera.ure review from which different definitions.by va.ious.a.thors.were collected,a.a.yzed,a.d compa.ed.

关键词： a.gorithmic des.gn Computer-a.ded des.gn Computa.iona. des.gn Genera.ive des.gn Pa.a.etric des.gn

Ha.mochroma.os.s.revis.ted

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World Journa. of Hepa.ology 2022年第11期14卷 1931-1939页

作者： a.ine Morga. a.va.enga.Pierre Bris.ot Pa.lo Ca.eb Junior Lima.santos Depa.tment of Pha.ma.ology-Es.ola.Pa.lis.a.de Medicina Universidade Federal de São PauloSão Paulo 04044-020Brazil Univers.ty of Rennes. Rennes 35065France

Ha.mochroma.os.s.is.a.genetic dis.a.e ca.s.d by hepcidin deficiency,res.ons.ble for a. increa.e in intes.ina. iron *** is.a.s.cia.ed with homozygos.ty for the HFE ***282Tyr ***,ra.e ca.es.of ha.mochroma.os.s.non-HFE ha.mochroma.os.s.ca. a.s. be ca.s.d by pa.h-ogenic va.ia.ts.in other genes.s.ch a. HJV,Ha.P,TFR2 a.d s.C40a.).a.working group of the Interna.iona. s.ciety for the s.udy of Iron in Biology a.d Medicine(BIOIRON s.ciety)ha. concluded tha. the cla.s.fica.ion ba.ed in different molecula. s.btypes.is.difficult to be a.opted in clinica. pra.tice a.d ha. propos.d a.new cla.s.fica.ion a.proa.hing clinica. ques.ions.a.d molecula. *** a.m of the pres.nt review is.to provide a. upda.e on cla.s.fica.ion,pa.hophys.ology a.d thera.eutic recommenda.ions.

关键词： Ha.mochroma.os.s Iron overloa. HFE Molecula. dia.nos.s Hepcidin

Engine Performa.ce a.d Exha.s. Emis.ions.of Pea.ut Oil Biodies.l

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Journa. of s.s.a.na.le Bioenergy s.s.ems 2013年第4期3卷 272-286页

作者： Bjorn s. santos s.rgio C. Ca.a.eda.Jewel a. Ca.unita. Depa.tment of Biologica. a.d a.ricultura. Engineering Texas A & M University College Station USA

The engine performa.ce a.d exha.s. emis.ions.of biodies.l produced from pea.ut oil mus. be eva.ua.ed to a.s.s. its.potentia. a. a. a.terna.ive dies.l fuel. In this.s.udy, two dies.l engines.ra.ed a. 14.2 kW (s.a.l) a.d 60 kW (la.ge) were opera.ed on pure pea.ut oil biodies.l (PME) a.d its.blends.with a.reference dies.l (REFDIEs.L). Res.lts.s.owed tha. compa.a.le power a.d torque were delivered by both the s.a.l a.d la.ge engines.when ra. on pure PME tha. on REFDIEs.L while bra.e-s.ecific fuel cons.mption (Bs.C) wa. found to be higher in pure PME. Higher exha.s. concentra.ions.of nitrogen oxides.(NOx), ca.bon dioxide (CO2) a.d tota. hydroca.bons.(THC) a.d lower ca.bon monoxide (CO) emis.ions.were obs.rved in the s.a.l engine when us.ng pure PME. Lower CO2, CO a.d THC emis.ions.were obta.ned when running the la.ge engine with pure PME. Blends.with low PME percenta.e s.owed ins.gnifica.t cha.ges.in both engine performa.ce a.d exha.s. emis.ions.a. compa.ed with the reference dies.l. Compa.is.n with s.ybea. biodies.l indica.es.s.mila. engine performa.ce. Thus. blends.of PME with dies.l ma. be us.d a. a.s.pplementa. fuel for s.ea.y-s.a.e non-roa. dies.l engines.to ta.e a.va.ta.e of the lubricity of biodies.l a. well a. contributing to the goa. of lowering the dependence to petroleum dies.l.

关键词： Biodies.l Pea.ut Oil Engine Performa.ce Exha.s. Emis.ions

Development a.d ps.chometric eva.ua.ion of the nurs. beha.ior towa.d confirmed a.d s.s.ected HIV/a.Ds.pa.ients.(NB-Cs.a.) s.a.e

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Frontiers.of Nurs.ng 2022年第1期9卷 103-113页

作者： Ja.et a.exis.De los.santos Norberto Milla.Cyruz Tuppa. Leodoro La.ra.ue Depa.tment of Nurs.ng Visayas State UniversityViscaLeyte 6521Philippines Gra.ua.e s.hool St Paul University PhilippinesTuguegaraoCagayan Valley 3500Philippines Depa.tment of s.a.is.ics Visayas State UniversityViscaLeyte 6521Philippines College of Hea.th a.lied a.d Medica. Profes.ions University of San AgustinTuguegaraoIloiloVisayas 5000Philippines Funda.enta.s.a.d a.minis.ra.ion Depa.tment Sultan Qaboos UniversityMuscatMuscat 112Oman

There is.a.s.a.city of litera.ure dis.us.ing nurs.s. beha.iors.towa.d ca.ing for s.s.ected or confirmed huma. immunodeficiency virus.(HIV)/a.quired immunodeficiency s.ndrome (a.Ds. pa.ients. The development of a.s.a.e s.ecific to mea.ure nurs.s. beha.iors.will a.low hea.th ins.itutions.to a.s.s. the dis.os.tion of their nurs.s.in terms.of HIV ca.e. This.s.udy a.ms.to pres.nt the rigors.of developing a.d va.ida.ing a.relia.le ins.rument to contextua.ize thes. nurs.s. beha.iors. This.s.udy utilized a.s.quentia. explora.ory mixed method des.gn to develop the NB-Cs.a. s.a.e. Thema.ic a.a.ys.s.wa. done on the qua.ita.ive da.a.from the interviews.with pers.ns.living with HIV/a.Ds.(PLHa. from which items.were s.lected to be included in the s.a.e. Explora.ory fa.tor a.a.ys.s.wa. utilized to extra.t the fa.tors.a.d Cronba.h’s.a.pha.wa. us.d to a.s.s. the relia.ility of the ins.rument. Four fa.tors.were extra.ted a.d a.e ca.egorized a. either ca.ing or dis.rimina.ory beha.iors. Thes. include: (1) s.rvice-oriented, (2) openha.ded, (3) perceptive, a.d (4) dis.rimina.ory. The s.a.e ha. a. interna. cons.s.ency of 0.73. The s.a.e s.ows.a.cepta.le ps.chometric properties. hence ca. be us.d to a.s.s. the nurs.s. beha.iors.in ca.ing for confirmed or s.s.ected HIV clients. The s.a.e ma. be us.d by hea.th ins.itutions.to determine the qua.ity of the pa.ient ca.e provided by their nurs.s.to clients.with confirmed or s.s.ected HIV .

关键词： ca.ing beha.iors HIV/a.Ds.ca.e nurs.ng s.a.e development s.quentia. explora.ory mixed method des.gn