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Size Dependent Physical Properties of Nanostructured α-Fe_2O_3 Thin Films Grown by Successive Ionic Layer Adsorption and Reaction Method for Antibacterial Application

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Journal of Materials Science & Technology 2015年第1期31卷 1-9页

作者： A.u.ubale M.R.Belkhedkar Nanostructured Thin Film Materials Laboratory Department of PhysicsGovt.Vidarbha Institute of Science and Humanities Department of Physics Shri Shivaji College

Thin films of nanostructured α-FeOwith thickness of 1 56,203 and 251 nm were deposited by successive ionic layer adsorption and reaction(SILAR) method onto glass substrates using FeCl-6HO and NaOH as cationic and anionic *** X-ray diffraction studies revealed that,α-FeOthin films are nanocrystalline in nature with rhombohedral *** morphological properties were investigated by field emission scanning electron and atomic force *** optical studies showed that α-FeOexhibits direct as well as indirect optical band gap *** electrical resistivity of α-FeOat 305 K decreases from 11.76×102 to9.46 × 10~2 Ω cm as film thickness increases from 156 to 251 *** thermo-emf measurements confirmed that α-FeOexhibits n-type *** nanocrystalline α-FeOexhibits antibacterial character against Staphylococcus aureus and its efficiency increases from 37.50%to 87.50%depending on crystallite size.

关键词： Thin films Nanostructures AFM(atomic force microsc

Synthesis of 4-aminoantipyrine Schiff bases and their antimicrobial activities

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Journal of Chinese Pharmaceutical Sciences 2018年第11期27卷 753-766页

作者： Olatunde S.Oladeji Monisola I.Ikhile Carine M.D.Fotsing Messai mamo Patrick G.Ndungu Derek T.Ndinteh Department of Applied Chemistry Faculty of Science University of Johannesburg

Various compounds of 4-aminoantipyrine Schiff bases(M1–M12) were synthesized via a condensation reaction of 4-aminoantipyrine with different benzaldehydes through a conventional method of refluxing the mixture for 3–4 h. The synthesized Schiff bases were characterized by using elemental analyses, FT-IR, uV-Vis, Mass, 1 H and 13 C NMR spectroscopy. The antimicrobial activity of the synthesized Schiff bases was investigated against 12 bacterial strains(Mycobacterium smegmatis, Bacillus cereus, Bacillus subtilis, Enterococcus faecalis, Staphylococcus epidermidis, Klebsiella pneumonia, Escherichia coli, Enterobacter cloacae, Klebsiella oxytoca, Proteus vulgaris, Enterobacter aerogenes, and Pseudomonas aeruginosa), and antifungal activities were tested against seven fungal strains(Aspergillus flavus, Aspergillus carbonarious, Aspergillus parasiticus, Aspergillus fumigatus, Aspergillus niger, Fusarium verticillioides and Fusarium proliferatum). The antimicrobial activities of the synthesized compounds were compared with standard streptomycin and nalidixic acid. The results obtained from antibacterial assay indicated that M1–M12 inhibited potential growth of Proteus vulgaris with minimum inhibitory concentrations(MICs) ranging from 15.6–250 μg/mL compared with the standard nalidixic acid with an MIC of 500 μg/mL. Moreover, we could conclude that most of the tested compounds experienced mild to low activities at 15.6 μg/mL. Their activities could be attributed to their low concentration s. The antifungal analysis showed that the tested fungi were not sensitive to the prepared Schiff bases at the prepared concentration of 500 μg/mL. Therefore, we recommended further analysis on both cytotoxicity and minimum bactericidal concentration(MBC) to ascertain their potential effects against human cells.

关键词： 4-Aminoantipyrine Antibacterial Schiffbases Antifungal Synthesis Inhibition

Genome-wide identification and in silico gene expression analysis of the related to ABI3/VP1(RAV)transcription factor family in barley(Hordeum vulgare L.)

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BIOCELL 2021年第6期45卷 1673-1685页

作者： CÜNEYT uÇARLI Department of Molecular Biology and Genetics Istanbul UniversityIstanbul34134Turkey

RAV(Related to ABI3/VP1)transcription factors are unique members of the AP2-ERF superfamily with AP2 and B3 domains and play important roles in the regulation of seed germination,plant growth,and stress *** the study,7 RAV genes,named HvRAVs,were identified in barley based on the available genome *** five of the seven HvRAVs were located on chromosome 3,HvRAV5 and HvRAV7 were located on chromosome 1 and 4,*** of the predicted HvRAVs were intron-less,except HvRAV2,which had one *** proteins have shown basic,instable,and hydrophilic *** AP2 domain specific RAYD and WLG motifs were detected in all HvRAV ***,B3 repression domain,R/KLFGV,is also found in the C-terminal of *** were found to have stress-related cis-acting elements,including MYB,MYC,and ***2 was predicted to have no GARE motifs,TATCCCA or TAACAA(G/A),and *** drought conditions,the expression level of HvRAVs did not significantly change in a drought-sensitive barley genotype,whereas HvRAV5 and HvRAV7 were dramatically down-regulated in a drought-tolerant *** of HvRAV5 was also inhibited by ***7 was strongly induced by plant pathogen *** HvRAV6 was induced by exogenous gibberellin application and during the germination ***,HvRAV6 transcript was detected higher than other HvRAVs in all stress and control conditions as well as during *** silico analyses have shown that HvRAVs play a role in response to different abiotic and biotic stresses as well as in plant ***,the extensive biological roles of HvRAV genes in plant development and in response to abiotic and biotic stresses need further investigation.

关键词： Barley RAV AP2 domain B3 domain AP2/ERF family Cis-acting elements

Traveling wave solutions for shallow water equations

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Journal of Ocean Engineering and Science 2017年第1期2卷 28-33页

作者： u.M.Abdelsalam Department of Mathematics Faculty of ScienceFayoum UniversityAl FayoumEgypt

An extended homogeneous balance method is suggested in this *** on computerized symbolic computation and the homogeneous balance method,new exact traveling wave solutions of nonlinear partial differential equations(PDEs)are *** shallow-water equations represent a simple yet realistic set of equations typically found in atmospheric or ocean modeling applications,we consider the exact solutions of the nonlinear generalized shallow water equation and the fourth order Boussinesq *** this method,with the aid of Mathematica,many new exact traveling wave solutions are successfully obtained.

关键词： Extended homogeneous balance method Shallow water equation Boussinesq equation Traveling wave solutions

Institute of Energy Process Engineering and Chemical Engineering (IEC), Tu Bergakademie Freiberg: Towards a Circular Carbon Economy

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Clean Energy 2019年第4期3卷 316-323页

作者： Freiberg, T u Bergakademie Reiche Zeche Fuchsmuehlenweg 9 Freiberg 09599 Germany

1 History of the Institute of Energy Process Engineering and Chemical Engineering(IEC)The history of IEC dates back to 1918,when the Lignite Foundation of the State of Saxony was founded to develop pro-cesses and technologies for lignite utilization in *** 1919,the precursor department of IEC with a focus on the thermochemical conversion of lignite was established.

关键词： Saxon IEC Carbon

Laser Surface Texturing of Co–Cr–Mo Alloy for Biomedical Applications:A Case Study for the Effects of Process Parameters on Surface Properties

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Journal of Bionic Engineering 2023年第5期20卷 1967-1984页

作者： Şefika Kasman İbrahim Can uçar Sertan Ozan Department of Mechanical Engineering Dokuz Eylul UniversityIzmir35397Turkey Department of Mechanical Engineering Yozgat Bozok UniversityYozgat66100Turkey

This study presents a comprehensive approach to applying texturing processes created by engraving on the surface of CoCr28Mo alloy workpieces using a 20 W pulsed nanosecond fiber *** hatch strategy and distance,frequency,and scan speed were control parameters for texturing *** effectiveness of the parameters in terms of roughness and contact angle of the texturized surface was *** roughness and contact angle were analyzed using variance analysis to identify each variable's *** has been determined that the roughness of the texture defined by the hatch strategy plays a decisive role in the wettability behavior of the surface;however,the scan speed,frequency,and hatch distance which are among the laser surface texturing conditions are influential in the roughness and contact *** scan speed and hatch distance while decreasing frequency resulted in smoother surfaces,increasing the contact *** having rough surfaces produced with different processing conditions exhibit a super hydrophilic *** contact angle is most sensitive to the hatch distance;however,the frequency has the least influence on the contact *** most and least efficient surface roughness parameters are revealed to be scan speed and hatch distance,respectively.

关键词： Laser surface texturing Co-Cr-Mo alloy Surface roughness Wettability Bionic

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电子鼻同步检测花生霉菌及霉菌毒素

食品科学 2022年第12期43卷 310-316页

作者：王蓓沈飞何学明蒋雪松袁建方勇胡秋辉邱伟芬 mamo Firew Tafesse 南京财经大学食品科学与工程学院江苏省现代粮食流通与安全协同创新中心江苏南京210023 南京林业大学机械电子工程学院江苏南京210037 巴赫达尔大学生物技术研究所埃塞俄比亚亚的斯亚贝巴5954

利用电子鼻技术,建立了花生受不同霉菌感染后的霉变程度及毒素含量的同步快速检测方法。花生经辐照灭菌后接种5种常见霉菌(3种产毒菌株、2种非产毒菌株),于培养箱(26℃、相对湿度80%)中培养6 d。每天取出不同霉菌污染的样品采集电子鼻信... 详细信息

利用电子鼻技术,建立了花生受不同霉菌感染后的霉变程度及毒素含量的同步快速检测方法。花生经辐照灭菌后接种5种常见霉菌(3种产毒菌株、2种非产毒菌株),于培养箱(26℃、相对湿度80%)中培养6 d。每天取出不同霉菌污染的样品采集电子鼻信号,同时测定其菌落总数和黄曲霉毒素B_(1)(aflatoxin B_(1),AFB_(1))含量,建立不同霉菌感染下霉变程度及毒素含量定性判别模型。主成分分析结果显示不同霉菌污染下有一定的聚类趋势,且污染样品位于可接受样品的上方;利用线性判别分析和偏最小二乘判别分析整体准确率达到80%以上,其中根据产毒菌株和非产毒菌株分类正确率高于95.7%,根据AFB_(1)含量分类正确率90%以上,根据菌落总数分类正确率较低。所有模型中假阴性均低于17%。因此,电子鼻技术对不同霉菌感染下的霉变程度及毒素含量的测定具有可行性。未来研究应继续扩大样品数量,补充受其他更多霉菌侵染及不同品种的花生样品,同时考虑实际情况,以提高模型的准确性和稳定性。

关键词：花生电子鼻霉变黄曲霉毒素B_(1)

Relationship between magnetic parameters and heavy element contents of arable soil around a steel company,Nanjing

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Science China Earth Sciences 2010年第3期53卷 411-418页

作者： BLAHA u ROESLER W APPEL E Institute for Geosciences University of Tübingen

Magnetic parameters and element contents were determined in core NJ008 collected from the uppermost ca. 40 cm in a steel company in southwest Nanjing. The results showed that magnetic susceptibility (χ), saturation isothermal remanent magnetization (SIRM) and anhysteretic remanent magnetization (ARM) were enhanced in the uppermost 20 cm, with a mean magnetic susceptibility value of 112.5×10-8 m3 kg-1. Below 20 cm, χ decreased sharply with a mean value of 27.8×10-8m3 kg-1. Low-coercivity minerals such as magnetite dominate in arable soils, while the relative content of antiferromagnetic minerals increases below 20 cm. Heavy metals (Ni, Cu, Fe, Pb, V, and Zn) have similar vertical trends as χ. Principal component analysis reveals common high loadings of the same factor for magnetic concentration parameters (χ, ARM, and SIRM) and elements (Ni, Cu, Fe, Pb, V, and Zn) with an excellent linear correlation (0.69≤R≤0.98) between them. Magnetic susceptibility of paddy soil core NJ013, which had the same parent material as NJ008 but was far from pollution sources, showed stable values of magnetic concentration parameters along the whole core. Absolute values correspond to the so-called magnetic background value (below 20 cm) of NJ008. This indicates that pesticide and fertilizer had little effect on magnetic signals of the upper part of core NJ008 and the extremely enhanced magnetic concentration parameters originate from the steel company emission. Although, the arable soil does not reveal the pollution history and transportation due to annual ploughing, the significant linear relationship between magnetic concentration parameters and heavy metal contents suggests that magnetic parameters can serve as a proxy for quickly detecting soil metallic pollution and estimating the extent of contamination.

关键词： steel company soil heavy metal magnetic parameters

ASYMMETRIC SYNTHESIS——ENANTIOSELECTIVE SYNTHESIS OF (R)-α-AMINO ACIDS uSING L-ISOLEuCINE AS CHIRAL AuXILIARY REAGENT

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Science China Chemistry 1984年第6期27卷 566-571页

作者：蒋耀忠,u.SCHLLKOPF,u.GROTH Chengdu Institute of Organic Chemistry Academia Sinica Institute of Organic Chemistry Gottingen university Federal Republic of Germany Institute of Organic Chemistry Gottingen university Federal Republic of Germany

Enantioselective synthesis of (R)-α-amino acids via heterocyclic intermediate-(3S)-2,5-dimethoxy-3-see-butyl-3, 6-dihydropyrazine (5), using L-isoleucine as chiral auxiliaryreagent and glycine as raw meterial, has been studied. The alkylation of compound 5 withbutyllithium affords its lithium derivative (6) according to the cardanion mechanism. Then 6reacts with alkyl halide RX (7) to give the alkylated products (8) with very high diastereo-selectivity. In this reaction, the group R of 7 enters trans to the see-butyl group at C-3, i. *** (R)-configuration is induced at C-6 of 8. After hydrolysis the (R)-α-amino acid methylesters (9) are obtained.

关键词： OCH HZ ASYMMETRIC SYNTHESIS ENANTIOSELECTIVE SYNTHESIS OF AMINO ACIDS uSING L-ISOLEuCINE AS CHIRAL AuXILIARY REAGENT CDC HCI 占一 CHC ABX