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Oxidation behavior of FeV_(2)O_(4)and FeCr_(2)O_(4)particles in the air:Nonisothermal kinetic and reaction mechanism

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International Journal of Minerals,Metallurgy and Materials 2024年第8期31卷 1839-1848页

作者： Junyi Xiang Xi Lu Luwei Bai Hongru rao Sheng Liu Qingyun Huang Shengqin Zhang Guishang pei Xuewei Lü School of Metallurgy and Materials Engineering Chongqing University of Science and TechnologyChongqing 401331China Department of Materials Science and Engineering Seoul National UniversitySeoul 08826Rep.of Korea College of Materials Science and Engineering Chongqing UniversityChongqing 400044China

High-temperature oxidation behavior of ferrovanadium(FeV_(2)O_(4))and ferrochrome(FeCr_(2)O_(4))spinels is crucial for the application of spinel as an energy material,as well as for the clean usage of high-chromium vanadium ***,the nonisothermal oxidation behavior of FeV_(2)O_(4)and FeCr_(2)O_(4)prepared by high-temperature solid-state reaction was examined by thermogravimetry and X-ray diffraction(XRD)at heating rates of 5,10,and 15 K/*** apparent activation energy was determined by the Kissinger-Akahira-Sunose(KAS)method,whereas the mechanism function was elucidated by the Malek ***,in-situ XRD was conducted to deduce the phase transformation of the oxidation mechanism for FeV_(2)O_(4)and FeCr_(2)O_(4).The results reveal a gradual increase in the overall apparent activation energies for FeV_(2)O_(4)and FeCr_(2)O_(4)during *** stages of the oxidation process are observed based on the oxidation conversion rate of each *** oxidation mechanisms of FeV_(2)O_(4)and FeCr_(2)O_(4)are complex and have distinct *** particular,the chemical reaction controls the entire oxidation process for FeV_(2)O_(4),whereas that for FeCr_(2)O_(4)transitions from a three-dimensional diffusion model to a chemical reaction *** to the in-situ XRD results,numerous intermediate products are observed during the oxidation process of both compounds,eventually resulting in the final products FeVO_(4)and V2O_(5)for FeV_(2)O_(4)and Fe_(2)O_(3)and Cr_(2)O_(3)for FeCr_(2)O_(4),respectively.

关键词： FeV_(2)O_(4) FeCr_(2)O_(4) oxidation nonisothermal kinetics mechanism

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Selective leaching of lithium from spent lithium-ion batteries using sulfuric acid and oxalic acid

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International Journal of Minerals,Metallurgy and Materials 2024年第4期31卷 688-696页

作者： Haijun Yu Dongxing Wang Shuai rao Lijuan Duan Cairu Shao Xiaohui Tu Zhiyuan Ma Hongyang Cao Zhiqiang Liu Institute of Advanced Wear&Corrosion Resistant and Functional Materials Jinan UniversityGuangzhou 510632China Institute of Resources Utilization and Rare Earth Development Guangdong Academy of SciencesGuangzhou 510650China State Key Laboratory of Separation and Comprehensive Utilization of Rare Metals Guangzhou 510650China Guangdong province Key Laboratory of Rare Earth Development and Application Guangzhou 510650China

Traditional hydrometallurgical methods for recovering spent lithium-ion batteries(LIBs)involve acid leaching to simultaneously extract all valuable metals into the *** methods usually are followed by a series of separation steps such as precipitation,extraction,and stripping to separate the individual valuable *** this study,we present a process for selectively leaching lithium through the synergistic effect of sulfuric and oxalic *** optimal leaching conditions(leaching time of 1.5 h,leaching temperature of 70°C,liquid-solid ratio of 4 mL/g,oxalic acid ratio of 1.3,and sulfuric acid ratio of 1.3),the lithium leaching efficiency reached89.6%,and the leaching efficiencies of Ni,Co,and Mn were 12.8%,6.5%,and 21.7%.X-ray diffraction(XRD)and inductively coupled plasma optical emission spectrometer(ICp-OES)analyses showed that most of the Ni,Co,and Mn in the raw material remained as solid residue oxides and *** study offers a new approach to enriching the relevant theory for selectively recovering lithium from spent LIBs.

关键词： selective leaching oxalic acid sulfuric acid spent lithium-ion batteries

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Extreme Weather Disruptions and Emergency preparedness Among Older Adults in Ohio: An Eight-County Assessment

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International Journal of Disaster Risk Science 2024年第2期15卷 213-225页

作者： Smitha rao Fiona C.Doherty Anthony Traver Marisa Sheldon Emma Sakulich Holly Dabelko‑Schoeny College of Social Work The Ohio State UniversityColumbusOH 43210USA Age Friendly Innovation Center College of Social WorkThe Ohio State UniversityColumbusOH 43210USA College of public Health The Ohio State UniversityColumbusOH 43210USA

The disproportionate risks and impacts of climate change and extreme weather on older adults are increasingly evident. While especially true in disaster-prone areas, human-caused climate change introduces an element of uncertainty even in previously identified “safe” regions such as the Midwestern United States. Using a cumulative disadvantage and vulnerability-informed framework and descriptive statistics from multiple data sources, this article provides an overview of climate impacts, vulnerabilities, and county-level characteristics, focusing on older adults living in Central Ohio. A comparative multiple-case study methodology was used to triangulate regionally representative primary and secondary data sources to examine state and county-level measures of vulnerability, emergency preparedness, and disruptions caused by extreme weather among older adults across eight counties in Central Ohio. Seventy-eight percent of older adults in the sample reported being prepared for emergencies per Federal Emergency Management Agency guidelines. Older adults in Union County reported the highest rates of preparedness, while those in Fayette County reported the lowest. County-level rates of disruption of life activities by extreme weather ranged widely. Among the most rural in the region, Fayette County emerged as uniquely disadvantaged, with the lowest median income, the most vulnerable across multiple social vulnerability dimensions, and the most reported disruptions to life activities from extreme weather. County profiles offer a snapshot of existing vulnerabilities, socioeconomic conditions, special needs, preparedness, and current disruptions among older adults in the region and can inform resource mobilization across community and policy contexts.

关键词： Disaster preparedness Extreme weather Midwestern United States Older adults Regional assessment Social vulnerability

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Small extracellular vesicles from hypoxia-preconditioned bone marrow mesenchymal stem cells attenuate spinal cord injury via miR-146a-5p-mediated regulation of macrophage polarization

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Neural Regeneration Research 2024年第10期19卷 2259-2269页

作者： Zeyan Liang Zhelun Yang Haishu Xie Jian rao Xiongjie Xu Yike Lin Chunhua Wang Chunmei Chen Department of Neurosurgery Fujian Medical University Union HospitalFuzhouFujian ProvinceChina Fujian Neurosurgical Institute FuzhouFujian ProvinceChina

Spinal cord injury is a disabling condition with limited treatment *** studies have provided evidence suggesting that small extracellular vesicles(SEVs)secreted by bone marrow mesenchymal stem cells(MSCs)help mediate the beneficial effects conferred by MSC transplantation following spinal cord ***,hypoxia-preconditioned bone marrow mesenchymal stem cell-derived SEVs(HSEVs)exhibit increased therapeutic *** thus explored the role of HSEVs in macrophage immune regulation after spinal cord injury in rats and their significance in spinal cord *** or HSEVs were isolated from bone marrow MSC supernatants by density gradient *** administration to rats via tail vein injection after spinal cord injury reduced the lesion area and attenuated spinal cord *** regulate macrophage polarization towards the M2 phenotype in vivo and in *** RNA sequencing and bioinformatics analyses of SEVs and HSEVs revealed that mi R-146a-5p is a potent mediator of macrophage polarization that targets interleukin-1 receptor-associated kinase *** mi R-146a-5p expression in HSEVs partially attenuated macrophage *** data suggest that HSEVs attenuate spinal cord inflammation and injury in rats by transporting mi R-146a-5p,which alters macrophage *** study provides new insights into the application of HSEVs as a therapeutic tool for spinal cord injury.

关键词： bone marrow mesenchymal stem cells hypoxia preconditioning interleukin-1 receptor-associated kinase 1 macrophages mesenchymal stem cells small extracellular vesicles spinal cord injury

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Ocean wave directional spectrum estimation using spatio-temporal array of acoustic ranging and current measurement

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Chinese Journal of Acoustics 2024年第3期43卷 311-331页

作者： rao Liang DENG Kai ZHANG Zhaowei WANG Changhong Institute of Acoustics Chinese Academy of SciencesBeijing100190 University of Chinese Academy of Sciences Beijing100049 Beijing Engineering Technology Research Center of Ocean Acoustic Equipment Beijing100190

An approach to estimate ocean wave directional spectrum using spatio-temporal array of acoustic ranging and current measurement is proposed,and the 5-beam acoustic Doppler current profiler(ADCp)constructs a spatio-temporal array of acoustic ocean surface elevation tracking and acoustic Doppler current velocity measuring for directional wave *** on the linear wave theory and the space-time equivalence principle,the time-space transfer function applicable to the spatio-temporal array is proposed,and then the time delay term is compensated in the calculation of the covariance *** method can reduce the error of the directional spectrum *** results show that for the low signal-to-noise ratio from 0 dB to 5 dB,compared with the 4-beam synchronous array method,this method has a smaller root-mean-square error of the peak estimation of the directional *** field test shows that,compared with the 4-beam synchronous array method,the 5-beam spatio-temporal array method improves the kurtosis index of the directional spectrum from 2.31 to 2.80,and the correlation coefficient between the peak wave direction results of the ADCp and the buoy is increased from 0.80 to 0.83 in mild wave ***,the spatio-temporal array method can increase the degree of freedom of wave measurement,reduce the minimum aperture of the array,and increase the upper cut-off frequency of the estimable directional spectrum.

关键词： spectrum ocean directional

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Detection of a temporal salient object benefits from visual stimulus-specific adaptation in avian midbrain inhibitory nucleus

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Integrative Zoology 2024年第2期19卷 288-306页

作者： Jiangtao WANG Xiaoping rao Shuman HUANG Zhizhong WANG Xiaoke NIU Minjie ZHU Songwei WANG Li SHI Department of Automation Zhengzhou University School of Electrical EngineeringZhengzhouChina State Key Laboratory of Magnetic Resonance and Atomic and Molecular physics National Center for Magnetic Resonance in WuhanKey Laboratory of Magnetic Resonance in Biological SystemsInnovation Academy for Precision Measurement Science and TechnologyChinese Academy of SciencesWuhanChina Department of Automation Tsinghua UniversityBeijingChina

Food and predators are the most noteworthy objects for the basic survival of wild animals,and both are often deviant in both spatial and temporal domains and quickly attract an animal’s *** stimulus-specific adaptation(SSA)is considered a potential neural basis of salient sound detection in the temporal domain,related research on visual SSA is limited and its relationship with temporal saliency is *** avian nucleus isthmi pars magnocellularis(Imc),which is central to midbrain selective attention network,is an ideal site to investigate the neural correlate of visual SSA and detection of a salient object in the time ***,the constant order paradigm was applied to explore the visual SSA in the Imc of *** results showed that the firing rates of Imc neurons gradually decrease with repetitions of motion in the same direction,but recover when a motion in a deviant direction is presented,implying visual SSA to the direction of a moving ***,enhanced response for an object moving in other directions that were not presented ever in the paradigm is also *** verify the neural mechanism underlying these phenomena,we introduced a neural computation model involving a recoverable synaptic change with a“center-surround”pattern to reproduce the visual SSA and temporal saliency for the moving *** results suggest that the Imc produces visual SSA to motion direction,allowing temporal salient object detection,which may facilitate the detection of the sudden appearance of a predator.

关键词： adaptation attention model pigeon saliency

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physiological Mechanism of Exogenous Selenium in Alleviating Mercury Stress on pakchoi(Brassica campestris L.)

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phyton-International Journal of Experimental Botany 2024年第5期93卷 951-962页

作者： Chengxu Qian Qiangwen Chen Leiyu Jiang Xiaoyan Yang Shen rao Weiwei Zhang Feng Xu College of Horticulture and Gardening Yangtze UniversityJingzhou434025China Enshi Se-Run Material Engineering Technology Co. Ltd.Enshi445000China Henry Fok School of Biology and Agricultural Shaoguan UniversityShaoguan512005China National R&D for Se-Rich Agricultural products processing Technology Wuhan Polytechnic UniversityWuhan430023China

The objective of this study was to explain the physiological mechanisms through which Na_(2)SeO_(3) mitigates the growth and developmental inhibition of pakchoi under HgCl_(2)*** results showed that treatment with HgCl_(2)(40 mg L^(−1))led to reduced biomass,dwarfing,root shortening,and root tip necrosis in *** to control(CK),the activities of superoxide dismutase(SOD)and peroxidase(pOD)in Hg treatment increased,and the content of malondialdehyde(MDA)also dramatically increased,which negatively impacted the growth of *** concentrations of Na_(2)SeO_(3)(0.2 mg L^(−1))significantly increased the content of soluble sugars compared with control,while chlorophyll,soluble proteins,free amino acids,and vitamin C had no significant *** results of the mixed treatments with HgCl_(2)and Na_(2)SeO_(3) suggested that selenium may be able to reduce the toxicity of mercury in *** biomass,plant height,root length,chlorophyll content,soluble protein,other physiological indicators,and proline showed significant increases compared with the HgCl_(2)***,the MDA content and mercury accumulation in pakchoi *** results revealed the antagonistic effects of selenium and mercury in ***,a theoretical basis for studying pakchoi’s mercuryexcreted and selenium-rich cultivation technology was provided.

关键词： Selenium mercury stress pakchoi physiological properties antioxidant enzymes

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Direct detection of C9orf72 hexanucleotide repeat expansions by nanopore biosensor

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Chinese Chemical Letters 2024年第5期35卷 351-354页

作者： Xinqiong Li Guocheng rao Xi peng Chan Yang Yanjing Zhang Yan Tian Xianghui Fu Jia Geng State Key Laboratory of Biotherapy and Cancer Center West China HospitalSichuan University and Collaborative Innovation Center of BiotherapyChengdu 610041China Division of Endocrinology and Metabolism West China School of Medicine/West China HospitalSichuan UniversityChengdu 610041China Department of Endocrinology and Metabolism Affiliated Hospital of North Sichuan Medical CollegeNorth Sichuan Medical CollegeNanchong 637000China Division of Endocrinology and Metabolism National Clinical Research Center for GeriatricsState Key Laboratory of Biotherapy and Cancer CenterWest China HospitalSichuan University and Collaborative Innovation Center of BiotherapyChengdu 610041China Department of Laboratory Medicine State Key Laboratory of BiotherapyMed-X Center for ManufacturingWest China HospitalSichuan University and Collaborative Innovation CenterChengdu 610041China Tianfu Jincheng Laboratory City of Future MedicineChengdu 641400China

Diagnostic C9orf72 hexanucleotide repeat expansions(C9-HRE)is essential for the early and accurate diagnosis of amyotrophic lateral sclerosis(ALS)and will provide support for the prognosis and gene therapy of *** the present study,by combining catalytic hairpin assembly(CHA)with Mycobacterium smegmatis porin A(MspA)nanopore,a new nanopore-based strategy for the detection of C9-HRE was *** than 30 repeats of C9-HRE could be detected via this method,and the results have the potential to help distinguish between patients and healthy ***,the method demonstrated its great specificity for C9-HRE by identifying other repeat *** the high selectivity,this approach had been successfully used to detect C9-HRE in cell and blood samples with high *** detection strategy is user-friendly and has a strong anti-interference ability,thus providing a powerful tool for clinical diagnosis.

关键词： MspA nanopore C9orf72 HRE Detection Biosensor Catalytic hairpin assembly

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Dimethylamine oxalate manipulating CspbI_(3) perovskite film crystallization process for high efficiency carbon electrode based perovskite solar cells

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Journal of Energy Chemistry 2024年第6期93卷 221-228,I0006页

作者： Wenran Wang Xin peng Jianxin Zhang Jiage Lin Rong Huang Guizhi Zhang Huishi Guo Zhenxiao pan Xinhua Zhong Huashang rao Key Laboratory for Biobased Materials and Energy of Ministry of Education College of Materials and EnergySouth China Agricultural UniversityGuangzhou 510642GuangdongChina College of Chemistry and Civil Engineering Shaoguan UniversityShaoguan 512005GuangdongChina Guangdong provincial Key Laboratory of Utilization and Conservation of Food and Medicinal Resources in Northern Region Shaoguan UniversityShaoguan 512005GuangdongChina

Crystallization process determines the quality of perovskite films and the performances of resultant perovskite solar cells(pSCs).Dimethylamine oxalate has been proven as a multifunctional modulator,and is explored as an efficient additive in manipulating the crystallization process of CspbI_(3) perovskite *** one hand,oxalate serves as the precipitator that facilitates the nucleation process of *** larger size of intermediate is conductive to the larger size and smaller grain boundaries of resultant *** the other hand,in subsequent annealing process,the phase conversion and growth process of transient perovskite can be decelerated due to the strong interactions of oxalate with both dimethylamine cation(DMA^(+))and pb^(2+).Due to the optimized crystallization kinetics,the morphology and quality of CspbI_(3) perovskite films are comprehensively improved with lower defect concentrations,and charge recombination loss is effectively *** from the optimized crystal quality of perovskite films,the carbon electrode-based CspbI_(3) pSCs exhibit a champion efficiency of 18.48%.This represents one of the highest levels among all hole transport layer-free inorganic perovskite solar cells.

关键词： Solar cells perovskite CspbI_(3) Carbon electrodes Oxalate

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Enhanced detection algorithm for apple bruises using structured light imaging

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ARTIFICIAL INTELLIGENCE IN AGRICULTURE 2024年第1期11卷 50-60页

作者： Zhu, Haojie Yang, Lingling Wang, Yu Wang, Yuwei Hou, Wenhui rao, Yuan Liu, Lu Anhui Agr Univ Coll Engn Hefei 230036 Peoples R China Anhui Agr Univ Key Lab Agr Sensors Minist Agr & Rural Affairs Hefei 230036 Peoples R China Chinese Acad Sci Hefei Inst Technol Innovat Engn Hefei 230094 Peoples R China

Bruising reduces the edibility and marketability of fresh apples, inevitably causing economic losses for the apple industry. However, bruises lack obvious visual symptoms, which makes it challenging to detect them using imaging techniques with uniform or diffuse illumination. This study employed the structured light imaging (SLI) technique to detect apple bruises. First, the grayscale reflection images were captured under phase-shifted sinusoidal illumination at three different wavelengths (600, 650, and 700 nm) and six different spatial frequencies (0.05, 0.10, 0.15, 0.20, 0.25, and 0.30 cycles mm-1). Next, the grayscale reflectance images were demodulated to produce direct component (DC) images representing uniform diffuse illumination and amplitude component (AC) images revealing bruises. Then, by quantifying the contrast between bruised regions and sound regions in all AC images, it was found that bruises exhibited the optimal contrast when subjected to sinusoidal illumination at a wavelength of 700 nm and a spatial frequency of 0.25 mm-1. In the AC image with optimal contrast, the developed h-domes segmentation algorithm to accurately segment the location and range of the bruised regions. Moreover, the algorithm successfully accomplished the task of segmenting central bruised regions while addressing the challenge of segmenting edge bruised regions complicated by vignetting. The average Intersection over Union (IoU) values for the three types of bruises were 0.9422, 0.9231, and 0.9183, respectively. This result demonstrated that the combination of SLI and the h-domes segmentation algorithm was a viable approach for the effective detection of fresh apple bruises. (c) 2023 The Authors. publishing services by Elsevier B.V. on behalf of KeAi Communications Co., Ltd. This is an open access article under the CC BY-NC-ND license (http://***/licenses/by-nc-nd/4.0/).

关键词： Apple bruises Bruise enhancement Image segmentation Structured illumination COMpUTER VISION DETECTION DEFECTS IMAGES SYSTEM DAMAGE

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