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HPLC combined with chemometrics for quality control of Huamoyan Granules or Capsules

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Chinese Herbal Medicines 2024年第3期16卷 449-456页

作者： minhang Dou Jiayi Huang Mimi Yu Huahua Li Yang Song Ziwei Peng Shouying Du Jie Bai School of Chinese Materia Medica Beijing University of Chinese MedicineBeijing 100029China Beijing Institute for Drug Control NMPA Key Laboratory for Quality Evaluation of Traditional Chinese Medicine(Traditional Chinese Patent Medicine)Beijing Key Laboratory of Analysis and Evaluation on Chinese MedicineBeijing 102206China

Objective:Huamaoyan Granules(HMYG)and Huamaoyan Capsules(HMYC)are Chinese patent medicines with different dosage forms of the same *** to the different preparation process,the chemical composition of these Chinese patent medicines varies greatly among different forms,but there were few studies on the difference comparison and quality control of *** order to improve the effectiveness and safety in its clinical application,an idea combining high performance liquid chromatography(HPLC)and chemometrics was put forward to study the quality control of Chinese patent medicines in different dosage forms of the same ***:The differential markers of HMYG and HMYC were explored based on HPLC fingerprint and chemometrics including orthogonal projections to latent structures-discriminant analysis(OPLS-DA),principal component analysis(PCA),and hierarchical cluster analysis(HCA).Finally,the quantitative analysis method of related components was established by ***:A quality control method for HMYG and HMYC was ***,the chemical components of HMYG and HMYC were systematically analyzed by HPLC *** exploration showed that there were 20 characteristic peaks and 57 common ***,the potential differential markers between HMYG and HMYC were explored by chemometrics,and the differential markers were screened after intersection with the 20 characteristic ***,HPLC quantitative analysis methods for nine components were established,including seven differential markers(neochlorogenic acid,protocatechualdehyde,chlorogenic acid,cryptochlorogenic acid,caffeic acid,rosmarinic acid and salvianolic acid A).The results of HPLC quantitative analysis showed that the contents of eight components in HMYG and HMYC samples were significantly *** to the above results,the differential markers between HMYG and HMYC screened based on HPLC fingerprint and chemometrics can effectively characterize the differ

关键词： chemometrics Chinese patent medicine high performance liquid chromatography fingerprint Huamoyan Granules/Capsules quality control synovitis

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长直管道预混气体爆燃波系演化过程研究

中国安全科学学报 2024年第3期34卷 55-62页

作者：胡洋陶红宋民航吕硕张海霞华北科技学院安全工程学院河北廊坊065201 应急管理部工业安全事故分析与监测预警重点实验室河北廊坊065201

为减少工业场所可燃气体生产、运输和储存过程中气体爆炸事故的发生,利用自主搭建的200 mm×200 mm×35 m方形管道和直径为90 mm、长度为10 m的圆形管道,在相同的初始条件下,运用体积分数为9.5%的甲烷/空气预混气体开展爆炸试验,结合压... 详细信息

为减少工业场所可燃气体生产、运输和储存过程中气体爆炸事故的发生,利用自主搭建的200 mm×200 mm×35 m方形管道和直径为90 mm、长度为10 m的圆形管道,在相同的初始条件下,运用体积分数为9.5%的甲烷/空气预混气体开展爆炸试验,结合压力、火焰传感器对其进行研究。结果表明:2种不同尺度、不同截面的管道中波系演化过程是相同的,点火后火焰由层流向湍流转变,火焰加速导致压缩波相互追赶,最终形成强激波;速度在2种长直管道中的变化趋势相同,都经历了加速—减速—再加速—再减速的过程,方管和圆管中火焰速度最大分别达到69和35.7 m/s,第一道压缩波经壁面反射后压力上升至117%和114%;当反射波与火焰阵面耦合作用时,方管和圆管中火焰速度分别降至73%和93%;体积分数相同的条件下,2种长直管道中第一道压缩波的最大压力值相近,方管中为65.45 kPa,圆管中为67.09 kPa。

关键词：长直管道预混气体爆燃波系演化压力波

降低分散相破碎的低剪切阀技术路线及研发进展

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化工设备与管道 2024年第3期61卷 94-103页

作者：宋民航王子兴杨宏燕华北科技学院安全工程学院北京101601 中海油石化工程有限公司山东济南250101 北京工业大学信息学部北京100124

阀门作为应用于石化等行业的关键设备之一,通过调整阀门开度调节液流流量。在多相流分离领域,位于分离器上游的阀门容易造成分散相剪切破碎,形成更加细小的液滴,甚至出现乳化现象,增加了分离难度。文章聚焦于降低分散相破碎的低剪切阀,... 详细信息

阀门作为应用于石化等行业的关键设备之一,通过调整阀门开度调节液流流量。在多相流分离领域,位于分离器上游的阀门容易造成分散相剪切破碎,形成更加细小的液滴,甚至出现乳化现象,增加了分离难度。文章聚焦于降低分散相破碎的低剪切阀,从影响液滴破碎及最大稳定液滴直径的关键物理因素出发,包括单位质量平均能量耗散率、液流能量耗散体积等,对降低液滴破碎的可行性路径进行总结,具体包括减小流经阀门液流的流场紊乱、增加油滴聚结结构,以及增大液流能量耗散体积。在此基础上,分析了多种典型低剪切阀门的结构特点及实际性能,并总结了低剪切阀的发展趋势,为新型低剪切阀开发及优化设计,以及规模化推广应用提供理论及技术支撑。

关键词：低剪切阀结构设计分散相剪切破碎液滴聚结

新型电力系统专用传感与边缘智能关键技术及其展望

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高电压技术 2024年第8期50卷 3324-3338页

作者：余涛梁敏航罗庆全蓝超凡王艺澎潘振宁华南理工大学电力学院广州510641

电力物联网在电力系统的实时传感、透明感知与全局调控中发挥着重要作用。随着新型电力系统的不断演化,传统的设备传感与静态独立的智能系统难以应对多样化业务需求激增、多元化数据爆发式增长、传感器通信可靠性差与能效低下和算法模... 详细信息

电力物联网在电力系统的实时传感、透明感知与全局调控中发挥着重要作用。随着新型电力系统的不断演化,传统的设备传感与静态独立的智能系统难以应对多样化业务需求激增、多元化数据爆发式增长、传感器通信可靠性差与能效低下和算法模型迭代成本高等难题。因此,高度多元集成、绿色持续可靠、云边端深度协同的新型电力系统专用传感与边缘智能有望成为新范式。该文首先以新型电力系统专用传感与边缘智能的基本内涵为基础,构建了专用传感与边缘智能融合贯通的体系架构。然后重点阐述了国产化高频新型传感技术、绿色供能的高性能嵌入式芯片技术、高可靠性灵活组网技术、轻量化模型推理技术、云边协同资源共享技术和在线学习持续迭代技术。并进一步展望了专用传感与边缘智能在数据治理、隐私保护、软件定义硬件、业务-算力微服务、多层分布式泛在智能和电力大模型等发展方向,以期为新型电力系统建设提供参考。

关键词：新型电力系统电力物联网专用传感边缘智能云边协同

基于大语言模型的新型电力系统用户特性立体应用模式初探

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高电压技术 2024年第7期50卷 2833-2848页

作者：余涛王艺澎罗庆全蔡新雷刘熙鹏梁敏航华南理工大学电力学院广州510640 广东省电网智能量测与先进计量企业重点实验室广州510640 广东电网有限责任公司电力调度控制中心广州510600

随着新型负荷的广泛接入与虚拟电厂建设的不断推进,新型电力系统中多元的负荷结构与频繁的网荷交互使得用户特性应用在数据融合、特性挖掘和业务赋能面临关键挑战。因此,该文首先深入分析了用户特性的研究现状,以此为基础提出了新型电... 详细信息

随着新型负荷的广泛接入与虚拟电厂建设的不断推进,新型电力系统中多元的负荷结构与频繁的网荷交互使得用户特性应用在数据融合、特性挖掘和业务赋能面临关键挑战。因此,该文首先深入分析了用户特性的研究现状,以此为基础提出了新型电力系统用户特性立体应用模式,贯通了“多源数据-多维特性-多元模块-多样业务”的应用链路。然后,针对该模式实践中海量多源数据可用性差、特性刻画灵活性低、业务贯通复杂性高的核心技术难题,立足于近期大语言模型备受关注的显著能力与智能体应用范式,分别在自适应数据治理、对话式数据交互、自动数据分析与机器学习、多智能体应用系统架构方面提出了解决方案。进一步,更通过用电数据库交互与业扩报装接入优化的案例表明所提方案能够自动化、智能化、个性化地开展用户特性应用,有望在实际中应对用户侧业务面临的关键挑战。最后,对大语言模型赋能用户侧海量资源管控以及系统智能水平跃升进行了展望。

关键词：新型电力系统用户特性立体应用大语言模型智能体

Characterization of a strain of Sphingobacterium sp. and its degradation to herbicide mefenacet

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Journal of Environmental Sciences 2004年第2期16卷 343-347页

作者： YEYang-fang minhang DUYu-feng CollegeofLifeScience ZhejiangUniversityHangzhou310029China. EnvironmentProtection＆DetectionCenterStationofNingbo Ningbo315010China

A bacterium(designated strain Y1) degrading acetanilide herbicide mefenacet was isolated from aerobic sludge. Based on the analyses of partial 16S rRNA gene, cellular fatty acid and BIOLOG-GN, and general physiological and biochemical characteristics, strain Y1 was identified as Sphingobacterium multivolum. Strain Y1 was able to degrade mefenacet used as sources of carbon and energy. Degradation of mefenacet was accompanied by producing the metabolites N-methylaniline and an unidentified compound with molecular weight 205, indicating a metabolic pathway of mefenacet initiated by hydrolysis of amido bond.

关键词： herbicide mefenacet Sphingobacterium biodegradation

Effect　of　Land　Use　History　on　Methane　Emission　and　Methanogenic　Flora　in　Flooded　Soils

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Pedosphere 1996年第1期6卷 73-80页

作者： minhang CHENMEICI 等 DepartmentofEnvironmentalScience ZhejiangAgriculturalUniversityHangzhou310029China DepartmentofEnvi

The characteristics of methane emission were compared among six types of upland and paddy soils developed from different parent materials with distinct physics and chemical properties after planting rice. The fluxes of methane emission in submerged soils from the upland were obviously lower than those from the paddy rice field. The flux of methane emission in the paddy soil developed from fluvo-aquic soil was the largest among all the types of soils. Planting of rice was helpful to emission of methane in soils. The amounts of various groups of methanogenic flora were conformed with the deferences among the fluxes of methane emission in various types of soils. Methane formation was observed in each type Of air-dried soils stored for a long time after addition of water and incubation at 35℃.

关键词： air-dried soil methane emission methanogenic flora methanogensis

船用低振动噪声三相异步电动机冷却风扇流场分析

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电机技术 2024年第2期 1-5页

作者：徐敏航何兰香韩素芳海军驻上海地区第四军事代表室 201108 上海电器科学研究所(集团)有限公司 200063

文章以JYZC-132L-2型二极立式电动机冷却风扇为例,借助CFD软件,对两款铸铝风扇的流场进行仿真分析。从风扇的气流涡旋、风扇损耗和效率等方面考虑,提出优化建议,为低振动噪声电动机冷却风扇设计提供理论依据。

关键词：低振动噪声湍流模型压力脉动

Effect of dissolved oxygen on electrochemical corrosion behavior of 2205 duplex stainless steel in hot concentrated seawater

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Journal of Materials Science & Technology 2021年第7期66卷 177-185页

作者： Hongtao Zeng Yong Yang minhang Zeng Moucheng Li Institute of Materials School of Materials Science and EngineeringShanghai UniversityShanghai 200072China

The corrosion behavior of 2205 duplex stainless steel was investigated in hot concentrated seawater with different dissolved oxygen(DO) concentration by electrochemical measurement techniques and surface analysis methods. DO obviously enhances the cathodic reaction process, the formation of passive film and polarization resistance. With increasing the DO concentration from 0.34 to 3.06 mg L^(-1), the relative contents of Fe_(2)O_(3) and Cr_(2)O_(3) and the Cr-enrichment gradually enlarge in the passive film. The higher DO concentrations result in lower defect densities and thicker of space charge layers in the passive films,whichmayeffectively inhibit the intrusion of aggressive chloride ions. The increment inDOconcentration clearly increases the pitting potential, but decreases the repassivation potential. It may weaken both the occurrence and repassviation tendencies of stable pitting corrosion.

关键词： Dissolved oxygen Pitting corrosion 2205 duplex stainless steel Hot concentrated seawater Passivation