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活化工艺对木质活性炭纤维结构和碘吸附性能的影响

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功能材料 2013年第17期44卷 2565-2569页

作者：李冬娜马晓军天津科技大学包装与印刷工程学院天津300222

以杉木为原料,经苯酚液化、熔融纺丝、固化处理后,CO2活化制备出木质活性炭纤维,利用扫描电镜、拉曼光谱、比表面积测定对其形态结构进行了表征,并研究了活化工艺因素对其碘吸附性能的影响。结果表明,木质活性炭纤维的表面平滑,断面呈圆... 详细信息

以杉木为原料,经苯酚液化、熔融纺丝、固化处理后,CO2活化制备出木质活性炭纤维,利用扫描电镜、拉曼光谱、比表面积测定对其形态结构进行了表征,并研究了活化工艺因素对其碘吸附性能的影响。结果表明,木质活性炭纤维的表面平滑,断面呈圆形;500℃以上的木质活性炭纤维拉曼图谱都出现炭材料典型的D峰和G峰,且随着活化温度的提高,其石墨微晶尺寸La逐渐增大,R值逐渐减小;木质活性炭纤维的孔结构主要以微孔为主,其微孔率达到90%,只存在少许的中孔结构。随活化温度和活化剂用量的增加,木质活性炭纤维的碘吸附值明显增加,其收率随活化温度的升高呈现降低趋势;当活化时间增加到40min时,木质活性炭纤维的碘吸附值达到最大,而后降低。

关键词：木质活性炭纤维活化工艺结构碘吸附性能产率

A Simple and Effective Surface Defect Detection Method of Power Line Insulators for Difficult Small Objects

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Computers, materials & Continua 2024年第4期79卷 373-390页

作者： xiao Lu Chengling jiang Zhoujun ma Haitao Li Yuexin Liu State Grid jiangsu Electric Power Co. Ltd.Nanjing210024China State Grid Changzhou Power Supply Company Changzhou213003China

Insulator defect detection plays a vital role in maintaining the secure operation of power *** address the issues of the difficulty of detecting small objects and missing objects due to the small scale,variable scale,and fuzzy edge morphology of insulator defects,we construct an insulator dataset with 1600 samples containing flashovers and *** a simple and effective surface defect detection method of power line insulators for difficult small objects is ***,a high-resolution featuremap is introduced and a small object prediction layer is added so that the model can detect tiny ***,a simplified adaptive spatial feature fusion(SASFF)module is introduced to perform cross-scale spatial fusion to improve adaptability to variable multi-scale ***,we propose an enhanced deformable attention mechanism(EDAM)*** integrating a gating activation function,the model is further inspired to learn a small number of critical sampling points near reference *** the module can improve the perception of object *** experimental results indicate that concerning the dataset of flashover and breakage defects,this method improves the performance of YOLOv5,YOLOv7,and *** practical application,it can simply and effectively improve the precision of power line insulator defect detection and reduce missing detection for difficult small objects.

关键词： Insulator defect detection small object power line deformable attention mechanism

Study on the influence of pneumatic probe on the wake flow field of transonic turbine cascade

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Acta Mechanica Sinica 2024年第7期40卷 43-54页

作者： Qingdian Zhang Hongwei ma Anqi xiao Yingcun Liu junde Guo School of Energy and Power Engineering Beihang UniversityBeijing 102206China

The pneumatic probe is widely used for contact measurements in turbomachinery flow field ***,it inevitably interferes with the original flow field,leading to additional errors,particularly in wake flow fields or transonic regions with significant pressure *** study employed Reynolds-Averaged Navier-Stokes delete and high-fidelity numerical simulation to investigate the impact of an inserted pneumatic probe on the wake flow field of a transonic turbine blade and compared it to the baseline flow *** indicate that the probe causes the shock waves premature occurrence in the high subsonic wake region near the turbine blade trailing *** shock waves affect vortex shedding by thickening the boundary layer near the trailing edge and changing the shedding pattern from high-frequency-low-energy to *** addition,the extra flow loss is incurred,and the blade's heat transfer characteristic is *** research provides a reference for testing experiments in complex transonic flow fields,guiding experimental researchers to minimize instrument interference with the original flow field.

关键词： Pneumatic probe Wake flow field Transonic turbine cascade Shock wave High-fidelity numerical simulation

Development of Ti–V–Cr–Mn–Mo–Ce high-entropy alloys for high-density hydrogen storage in water bath environments

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Rare Metals 2024年第10期43卷 5229-5241页

作者： Hua-Zhou Hu Hou-Qun xiao Xin-Cong He Wen-Hao Zhou xiao-Xuan Zhang Rui-Zhu Tang jie Li Chuan-Ming ma Qing-jun Chen Key Laboratory of Rare Earths Chinese Academy of SciencesJiangxi Institute of Rare EarthsGanjiang Innovation AcademyChinese Academy of Sciences

The V-based body-centered cubic （BCC）-type hydrogen storage alloys have attracted significant attention due to their high theoretical hydrogen storage capacity of3.80 wt%.However,their practical application faces challenges related to low dehydriding capacity and poor activation *** overcome these challenges,a BCC-type Ti–V–Cr–Mn–Mo–Ce high-entropy alloy（HEA） with an effectively dehydriding capacity of 2.5 wt% above 0.1 MPa was *** introduction of Mo and conducting heat treatment,the precipitation of Ti-rich phase in HEA was successfully suppressed,resulting in improved compositional uniformity and dehydriding ***,the effective dehydriding capacity increased significantly from 0.60 wt% to 2.50 wt% a65℃,surpassing that of other types of hydrogen storage alloys under the same ***,the addition of 1 wt%Ce enabled initial hydrogen absorption at 25℃ without the need for activation at 400℃.Furthermore,Ce doping reduced the dehydriding activation energy of the Ti–V–Cr–Mn–Mo–Ce HEA from 52.71 to 42.82 kj·mol-1Additionally,the enthalpy value of dehydrogenation decreased from 46.89 to 17.96 k j·mol-1,attributed to a decrease in the hysteresis factor from 0.68 to *** findings provide valuable insights for optimizing the hydrogen storage property of HEA.

关键词： BCC structure Ce doping Heat treatment High-entropy alloys Hydrogen storage alloys

Atomic Dispersed Hetero‑Pairs for Enhanced Electrocatalytic CO_(2)Reduction

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Nano-Micro Letters 2024年第1期16卷 55-67页

作者： Zhaoyong jin Meiqi Yang Yilong Dong Xingcheng ma Ying Wang jiandong Wu jinchang Fan Dewen Wang Rongshen Xi xiao Zhao Tianyi Xu jingxiang Zhao Lei Zhang David j.Singh Weitao Zheng xiaoqiang Cui State Key Laboratory of Automotive Simulation and Control School of Materials Science and EngineeringKey Laboratory of Automobile Materials of MOEElectron Microscopy CenterJilin UniversityChangchun 130012People’s Republic of China Key Laboratory of Photonic and Electronic Bandgap materials Ministry of Educationand College of Chemistry and Chemical EngineeringHarbin Normal UniversityHarbin 150025People’s Republic of China College of Chemistry Jilin UniversityChangchun 130012People’s Republic of China Department of Physics and Astronomy and Department of Chemistry University of MissouriColumbiaMO 65211USA

Electrochemical carbon dioxide reduction reaction(CO_(2)RR)involves a variety of intermediates with highly correlated reaction and ad-desorption energies,hindering optimization of the catalytic *** example,increasing the binding of the*COOH to the active site will generally increase the*CO desorption *** this relationship may be expected to dramatically improve the intrinsic activity of CO_(2)RR,but remains an unsolved ***,we addressed this conundrum by constructing a unique atomic dispersed hetero-pair consisting of Mo-Fe di-atoms anchored on N-doped carbon *** system shows an unprecedented CO_(2)RR intrinsic activity with TOF of 3336 h−1,high selectivity toward CO production,Faradaic efficiency of 95.96%at−0.60 V and excellent *** calculations show that the Mo-Fe diatomic sites increased the*COOH intermediate adsorption energy by bridging adsorption of*COOH *** the same time,d-d orbital coupling in the Mo-Fe di-atom results in electron delocalization and facilitates desorption of*CO ***,the undesirable correlation between these steps is *** work provides a promising approach,specifically the use of di-atoms,for breaking unfavorable relationships based on understanding of the catalytic mechanisms at the atomic scale.

关键词： CO_(2)reduction reaction Atomic dispersed catalyst Hetero-diatomic pair Ad-desorption energy Linear scaling relation

Effect of Al_(2)O_(3)on the Mechanical Properties of(B_(4)C+Al_(2)O_(3))/Al Neutron Absorbing materials

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Acta Metallurgica Sinica(English Letters) 2024年第8期37卷 1411-1420页

作者： j.X.Cai B.M.Shi N.Li Y.Liu Z.G.Zhang Y.N.Zan Q.Z.Wang B.L.xiao Z.Y.ma Shi‑Changxu Innovation Center for Advanced materials Institute of Metal ResearchChinese Academy of SciencesShenyang 110016China Key Laboratory of Nuclear materials and Safety Assessment Institute of Metal ResearchChinese Academy of SciencesShenyang 110016China Nuclear Equipment Division Beijing Institute of Nuclear EngineeringChina Nuclear Power Engineering Co.Ltd.Beijing 100840China Department of materials Science School of Mechanical EngineeringShenyang UniversityShenyang 110044China

B_(4)C/Al composites are widely utilized as neutron absorbing materials for the storage and transportation of spent nuclear *** order to improve the high-temperature mechanical properties of B_(4)C/Al composites,in-situ nano-Al_(2)O_(3)was introduced utilizing oxide on Al powder *** this study,the Al_(2)O_(3)content was adjusted by utilizing spheroid Al powder with varying diameters,thereby investigating the impact of Al_(2)O_(3)content on the tensile properties of(B_(4)C+Al_(2)O_(3))/Al *** was found that the pinning effect of Al_(2)O_(3)on the grain boundaries could hinder the recovery of dislocations and lead to dislocation accumulation at high *** the result,with the increase in Al_(2)O_(3)content and the decrease in grain size,the high-temperature strength of the composites increased *** finest Al powder used in this investigation had a diameter of 1.4μm,whereas the resultant composite exhibited a maximum strength of 251 MPa at room temperature and 133 MPa at 350℃,surpassing that of traditional B_(4)C/Al composites.

关键词： Al matrix composites Neutron absorbing materials (B_(4)C+Al_(2)O_(3))/Al composites High-temperature strength

Analysis of the Current Situation and Influencing Factors of Knowledge,Attitude,and Practice of Nursing Informatics Among Intern Nursing Students

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journal of Clinical and Nursing Research 2024年第4期8卷 7-13页

作者： Ping Zhao xiao Ling ma First Affiliated Hospital of Kunming Medical university Kunming 650000Yunnan ProvinceChina Medical School Xishuangbanna Vocational and Technical CollegeJinghong 666100Yunnan ProvinceChina

Objective:To investigate the current situation of knowledge,attitude,and practice(KAP)of nursing informatics for intern nursing ***:A total of 213 intern nursing students were selected as ***:The total score of the questionnaire of knowledge dimension was 10.32±3.23;the score of attitude dimension was 58.78±6.80;the score of practice dimension was 29.06±*** regression analysis showed that further learning plans,telemedicine hospital intern experience,self-learning ability,and telecare training were the related influencing factors of KAP(Pmatics among intern nursing students was low to ***,the strengthening of school courses and skill training programs is urgently needed.

关键词： Nursing informatics KAP Influence factors Intern nurses

微波消解-ICP-OES法测定小叶榕药材中微量元素

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广西科学院学报 2014年第4期30卷 285-288页

作者：付金娥韦树根马小军中国医学科学院药用植物研究所广西分所广西南宁530023

【目的】建立一种小叶榕(Ficus microcarpa)药材中微量元素的测定方法。【方法】采用微波消解样品,电感耦合等离子体质谱法(ICP-OES)测定小叶榕药材中12种微量元素的含量。【结果】电感耦合等离子体质谱法测定药材中微量元素的含量线性... 详细信息

【目的】建立一种小叶榕(Ficus microcarpa)药材中微量元素的测定方法。【方法】采用微波消解样品,电感耦合等离子体质谱法(ICP-OES)测定小叶榕药材中12种微量元素的含量。【结果】电感耦合等离子体质谱法测定药材中微量元素的含量线性好、操作简便、快速准确、灵敏度高。小叶榕药材中含量丰富的微量元素,从高到低依次为Mg、Fe、Al、Mn、Zn等。【结论】建立了微波消解-ICP-OES测定小叶榕药材中多种微量元素的分析方法。

关键词：小叶榕微量元素电感耦合等离子体发射光谱仪

Clinicopathological significance and immunotherapeutic outcome of claudin 18.2 expression in advanced gastric cancer:A retrospective study

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Chinese journal of Cancer Research 2024年第1期36卷 78-89页

作者： Changsong Qi xiaoyi Chong Ting Zhou Mingyang ma jifang Gong Miao Zhang jian Li jun xiao xiaohui Peng Zhen Liu Zonghai Li Lin Shen xiaotian Zhang State Key Laboratory of Holistic Integrative management of Gastrointestinal Cancers Beijing Key Laboratory of Carcinogenesis and Translational ResearchDepartment of Gastrointestinal OncologyPeking University Cancer Hospital&InstituteBeijing 100142China Key Laboratory of Carcinogenesis and Translational Research(Ministry of Education/Beijing) Department of Gastrointestinal OncologyPeking University Cancer Hospital&InstituteBeijing 100142China CARsgen Therapeutics Co. LtdShanghai 200231China CARsgen Life Sciences Co. LtdShanghai 200131China

Objective: Immunotherapeutic outcomes and clinical characteristics of claudin 18 isoform 2 positive(CLDN18.2-positive) gastric cancer(GC) vary in different clinical studies, making it difficult to optimize antiCLDN18.2 therapy. We conducted a retrospective analysis to explore the association of CLDN18.2 expression with clinicopathological characteristics and immunotherapeutic outcomes in ***: A total of 536 advanced GC patients from 2019 to 2021 in the CT041-CG4006 and CT041-ST-01clinical trials were included in the analysis. CLDN18.2 expression on ≥40% of tumor cells(2+, 40%) and CLDN18.2 expression on ≥70% of tumor cells(2+, 70%) were considered the two levels of positively expressed GC. The clinicopathological characteristics and immunotherapy outcomes of GC patients were analyzed according to CLDN18.2 expression ***: CLDN18.2 was expressed in 57.6%(cut-off: 2+, 40%) and 48.9%(cut-off: 2+, 70%) of *** death-ligand 1(PD-L1) and CLDN18.2 were co-expressed in 19.8% [combined positive score(CPS)≥1, CLDN18.2(cut-off: 2+, 40%)] and 17.2% [CPS≥5, CLDN18.2(cut-off: 2+, 70%)] of ***18.2 expression positively correlated with younger age, female sex, non-gastroesophageal junction(nonGEj), and diffuse phenotype(Punotherapy-related progression-free survival(ir PFS) were inferior in the CLDN18.2-positive ***: CLDN18.2-positive GC is associated with poor prognosis and worse immunotherapeutic outcomes. The combination of anti-CLDN18.2 therapy, anti-PD-L1/PD-1 therapy, and chemotherapy for GC requires further investigation.

关键词： Gastric cancer claudin18.2 CT041 PD-L1 immunotherapy