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Particle formulation of hydroalcoholic rosemary (Rosmarinus officinalis L.) extracts using a spouted bed

Particuology 2020年第4期18卷 26-34页

作者： D.Peshev E.Eichner m.goslinska S.Pietsch Y.Trambabova T.Terzieva N.Georgieva S.Heinrich Department of Chemical Engineering University of Chemical Technology and Metallurgy1576 SofiaBulgaria Institute of Solids Process Engineering and Particle Technology Hamburg University of Technology21073 HamburgGermany Department of Biotechnology University of Chemical Technology and Metallurgy1576 SofiaBulgaria

In this study,spouted bed technology was applied to the protection and functionalization of polyphenolic rosemary extracts.First,solid-liquid extraction was performed at 25℃with ethanol-water.The ethanol-water ratio was chosen to obtain high phenolic acid and diterpene concentrations in the extract.The selected solvent composition gave liquid extracts that could be directly added to a coating mixture for feeding into a spouted bed apparatus.Thus,no preliminary solvent exchange or evaporation of the extraction solvent to dryness was required.Food grade Paselli mD 6 maltodextrin and HiCap 100 modified starch were used as inert core and shell materials in the spouted bed encapsulation process under mild operating conditions.The antioxidant activity of the fresh extract was retained during processing,which indicated that the active constituents were preserved and quantitatively transferred into the encapsulated formulations,which were readily soluble in water.The obtained powders were composed of nearly spherical particles.Their compositions,water solubilities,and particle morphologies make them a strong candidate for food and beverage applications as natural antioxidants,preservatives,or functional ingredients.

关键词： Particle Polyphenolic rosemary extract Encapsulation Spouted bed Bioactive Antioxidant

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Novel technique for measurement of coating layer thickness of fine and porous particles using focused ion beam

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Particuology 2019年第1期17卷 190-198页

作者： m. goslinska I. Selmer C. Kleemann U.Kulozik I. Smirnova S. Heinrich Hamburg University of Technology Institute of Solids Process Engineering and Particle TechnologyDenickestr1521073 HamburgGermany Hamburg University of Technology Institute of Thermal Separation ProcessesEiJ^endorfer Str. 3821073 HamburgGermany Technical University of munich Chair of Food and Bioprocess EngineeringWeihenstephaner Berg 185354 FreisingGermany

A novel technique for the measurement of the coating layer thickness of fine particles was developed in this work based on cross-sectioning of micrometre-sized single coated particles using focused ion beam (FIB) milling. This technique was tested on two batches of aerogel particles coated with thin coatings in a spouted bed. The FIB milling procedure consisted of two steps. First, the desired part of the coated particle was removed using a high ion beam current. The resulting cross-sectioned area was then polished using a lower ion beam current to make the cross-section clearly visible. The FIB milling process was controlled with simultaneous scanning electron microscopy (SEm). Afterwards, the coating layer thickness was evaluated using the SEm images. The coating layer was successfully applied on the porous aerogel microparticles in the spouted bed. The coating uniformity of the highly porous particles increased with increasing sprayed coating solution amount, with up to 91% of the particle pores being covered. The FIB-cross-sectioning technique using an ion beam of 2.50 nA for the first milling and 0.43 nA for polishing of the surface resulted in successful generation of cross-sections of representative particles with a visible particle core and coating layer. A coating layer thickness of approximately 700 nm was achieved on particles with sizes of below 45 μm.

关键词： Coating layer thickness Focused ion beam microparticle Aerogel Spouted bed Dilute spouting

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