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Synthesis of surface controlled nickel/palladium hydride nanodendrites with high performance in benzyl alcohol oxidation

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Nano Research 2019年第6期12卷 1467-1472页

作者： Zipeng Zhao michelle M.FLORES Espinosa Jihan Zhou Wang Xue Xiangfeng Duan Jianwei miao Yu Huang Department of materials Science and Engineering University of CaliforniaLos AngelesCA 90095USA Department of Physics and Astronomy University of CaliforniaLos AngelesCA 90095USA Department of Chemistry and Biochemistry University of CaliforniaLos AngelesCA 90095USA California Nanosystems Institute University of CaliforniaLos AngelesCA 90095USA

Benzaldehyde byproduct is an imperative intermediate in the production of fine chemicals and additives.Tuning selectivity to benzaldehyde is therefore critical in alcohol oxidation reactions at the industrial level.Herein,we report a simple but innovative method for the synthesis of palladium hydride and nickel palladium hydride nanodendrites with controllable morphology,high stability,and excellent catalytic activity.The synthesized dendrites can maintain the palladium hydride phase even after their use in the chosen catalytic reaction.Remarkably,the high surface area morphology and unique interaction between nickel-rich surface and palladium hydride (β-phase) of these nanodendrites are translated in an enhanced catalytic activity for benzyl alcohol oxidation reaction.Our Ni/PdH0.43 nanodendrites demonstrated a high selectivity towards benzaldehyde of about 92.0% with a conversion rate of 95.4%,showing higher catalytic selectivity than their PdH0.43 counterparts and commercial Pd/C.The present study opens the door for further exploration of metal/metal-hydride nanostructures as next-generation catalytic materials.

关键词： benzyl alcohol selectivity benzaldehyde palladium hydride oxidation nanodendrites

Graphene oxide/multi-walled carbon nanotubes/gold nanoparticle hybridfunctionalized disposable screen-printed carbon electrode to determine Cd(II)and Pb(II)in soil

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International Journal of Agricultural and Biological Engineering 2019年第3期12卷 194-200页

作者： Hui Wang Yuan Yin Guo Zhao Fernando Bienvenido Isabel M.FLORES-Parrad Zhiqiang Wang Gang Liu Key Laboratory of modern Precision Agriculture System Integration Research Ministry of Education and Key Laboratory of Agricultural Information Acquisition TechnologyMinistry of AgricultureChina Agricultural UniversityBeijing 100083China Department of Informatics University of AlmeriaAlmeriaSpain College of Computer Science and Technology Shandong University of TechnologyZibo 255049China Research Institute of Wood Industry Chinese Academy of ForestryBeijing 100091China

Cadmium(Cd)and lead(Pb)in soil or water environment cause the ecological destruction and environmental deterioration when their contents exceed the natural background values.To trace the concentrations of Cd(II)and Pb(II),a sensitive and selective electrode was developed using disposable screen-printed carbon electrode(SPE)immobilized with a composite film of reduced graphene oxide/carboxylation multi-walled carbon nanotubes/gold nanoparticle hybrid(RGO-mWNT-AuNP)throughπ-πbind.This highly conductive nano-composite layer,“RGO-mWNT-AuNP,”was characterized by scanning electron microscopy,UV-visible spectrometer,cyclic voltammetry,and electrochemical impedance spectroscopy.Square wave stripping voltammetry was applied to RGO-mWNT-AuNP/SPE to electroplate bismuth film and monitor the Cd(II)and Pb(II)simultaneously.To obtain high current responses,the detecting parameters were optimized.Under optimized conditions,the current responses showed a linear relationship with the concentrations of Cd(II)and Pb(II)in the range from 1.0 to 80.0μg/L with a lower detection limit of 0.7μg/L and 0.3μg/L(S/N=3),respectively.Finally,the prepared electrode was further employed to detect Cd(II)and Pb(II)in soil samples with good results.

关键词： electrochemical electrode heavy metal contamination screen-printed carbon electrode graphene gold nanoparticle lead cadmium multi-walled carbon nanotube

激光冲击工艺对6061-T6铝合金侵蚀性能的影响（英文）

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Transactions of Nonferrous metals Society of China 2016年第6期26卷 1522-1530页

作者： J.IBARRA E.RODRíGUEZ O.JIméNEZ G.GómEZ-ROSAS M.FLORES J.VERDUZCO J.CHáVEZ Universidad de Guadalajara Departamento de Ingeniería de Proyectos Universidad de Guadalajara Departamento de Física Centro Universitario de Ciencias Exactas e Ingenierías

采用激光冲击工艺处理6061-T6铝合金,研究了二氧化硅砂对其侵蚀磨损性能的影响。其中冲击角为15°、30°、60°、90°,粒子速率为37和58 m/s,采用两种激光进行辐照。采用3D轮廓测量法表征了侵蚀形貌,并采用SEm研究其侵蚀机理。结果表明... 详细信息

采用激光冲击工艺处理6061-T6铝合金,研究了二氧化硅砂对其侵蚀磨损性能的影响。其中冲击角为15°、30°、60°、90°,粒子速率为37和58 m/s,采用两种激光进行辐照。采用3D轮廓测量法表征了侵蚀形貌,并采用SEm研究其侵蚀机理。结果表明,冲击角较小时,侵蚀磨损最大。侵蚀强度和侵蚀机理不受激光冲击工艺的影响,而与侵蚀的高应变速率有关。侵蚀图之间的差异是由于激光冲击工艺造成的表面粗糙度不同。最大质量损失和最大侵蚀深度分别出现在冲击角度为15°和30°时。最后,发现了明显的侵蚀机理的转移,从低角度的切割机制到90°时的凹坑形成。

关键词： 6061-T6铝合金侵蚀磨损激光冲击工艺

Cu-WC复合材料涂层的受限烧结和磨损性能（英文）

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Transactions of Nonferrous metals Society of China 2017年第10期27卷 2214-2224页

作者： J.L.CABEZAS-VILLA L.OLmOS H.J.VERGARA-HERNáNDEZ O.JIméNEZ P.GARNICA D.BOUVARD M.FLORES División de Estudios de Posgrado e Investigación Tec NM/Instituto Tecnológico de Morelia INICIT Universidad Michoacana de San Nicolás de HidalgoFco.J.Mujica S/N Universidad de Guadalajara Departamento de Ingeniería de Proyectos Univ.Grenoble Alpes CNRS SIMa P

采用固态烧结法制备Cu-WC金属基复合材料涂层。将不同体积分数(5%-30%)的WC增强颗粒与Cu颗粒混合,然后在还原性气氛和垂直膨胀计中于1000°C进行烧结。结果表明,复合材料涂层的烧结动力学受基体材料和WC颗粒的影响,WC颗粒能减缓粉末径... 详细信息

采用固态烧结法制备Cu-WC金属基复合材料涂层。将不同体积分数(5%-30%)的WC增强颗粒与Cu颗粒混合,然后在还原性气氛和垂直膨胀计中于1000°C进行烧结。结果表明,复合材料涂层的烧结动力学受基体材料和WC颗粒的影响,WC颗粒能减缓粉末径向和轴向的致密化。复合材料涂层紧实地粘附于基体上,而WC颗粒随机分布在基体中。与未添加增强剂的样品相比,添加了WC增强剂的样品的显微硬度增加,磨损量降低至原来的1/17。样品在载荷为5 N条件下的主要磨损机理为磨粒磨损,当WC增强剂的体积分数为20%时复合涂层的性能最优。

关键词：受限烧结膨胀法干滑动磨损显微硬度金属基复合材料涂层

铅鼓风炉中铜、硫、砷和锑对银分布的影响(英文)

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Transactions of Nonferrous metals Society of China 2014年第4期24卷 1202-1209页

作者： J.CHAIDEZ-FELIX A.ROmERO-SERRANO A.HERNANDEZ-RAmIREZ m.PEREZ-LABRA I.ALmAGUER-GUZmAN R.BENAVIDES-PEREZ M.FLORES-FAVELA metallurgy and materials Department IPN-ESIQIE UPALMZacatenco Academic Area of Earth Science and materials UAEH Col. CarbonerasMineral de la Reforma Servicios Administrativos Peoles S.A de C.V. Prol. Comonfort Sur 2050 Col. L. Echeverria

研究铅鼓风炉中杂质对银分布的影响。将含有不同Cu、S、As和Sb含量的铅烧结块在管式炉中于1573K下进行烧结,然后随炉冷却。烧结气氛为还原性的CO+CO2气体(p(CO)/p(CO2)=2.45)。采用SEm-EDS对所得样品进行表征。结果表明:烧结样品中含有... 详细信息

研究铅鼓风炉中杂质对银分布的影响。将含有不同Cu、S、As和Sb含量的铅烧结块在管式炉中于1573K下进行烧结,然后随炉冷却。烧结气氛为还原性的CO+CO2气体(p(CO)/p(CO2)=2.45)。采用SEm-EDS对所得样品进行表征。结果表明:烧结样品中含有5种不互溶的相,即炉渣(CaO,FeO,SiO2)、冰铜(S,Cu,Fe)、硬渣(As,Fe,Cu)、Cu-Sb相和铅块。银在Cu与Sb形成的熔体中的溶解度比在液态铅中的高。S与Cu形成冰铜,As与Cu形成硬渣。S和As能减少Cu-Sb合金的生成量,从而降低铅块中银的损失。

关键词：铅鼓风炉银铅杂质

Cerebral dopamine neurotrophic factor transfection in dopamine neurons using neurotensin-polyplex nanoparticles reverses 6-hydroxydopamine-induced nigrostriatal neurodegeneration

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Neural Regeneration Research 2022年第4期17卷 854-866页

作者： manuel A.Fernandez-Parrilla David Reyes-Corona Yazmin M.FLORES-martinez Rasajna Nadella michael J.Bannon Lourdes Escobedo minerva maldonado-Berny Jaime Santoyo-Salazar Luis O.Soto-Rojas Claudia Luna-Herrera Jose Ayala-Davila Juan A.Gonzalez-Barrios Gonzalo flores maria E.Gutierrez-Castillo Armando JEspadas-Alvarez Irma A.martínez-Dávila Porfirio Nava Daniel martinez-Fong Departamento de Fisiología Biofísica y NeurocienciasCentro de Investigación y de Estudios AvanzadosCiudad de MéxicoMéxico Programa Institucional de Biomedicina molecular Escuela Nacional de Medicina y HomeopatíaInstituto Politécnico NacionalCiudad de MéxicoMéxico Department of Biosciences IIIT-SrikakulamRajiv Gandhi University of Knowledge Technologies(RGUKT)Andhra PradeshIndia Department of Pharmacology Wayne State University School of MedicineDetroitMIUSA Departamento de Física Centro de Investigación y de Estudios AvanzadosCiudad de MéxicoMéxico Facultad de Estudios Superiores Iztacala Universidad Nacional Autónoma de MéxicoTlalnepantla de BazEdo.de MéxicoMéxico Departamento de Fisiología Escuela Nacional de Ciencias BiológicasCiudad de MéxicoMéxico Laboratorio de medicina Genómica Hospital Regional“1°de Octubre”ISSSTECiudad de MéxicoMéxico Laboratorio de Neuropsiquiatría Instituto de FisiologíaBenemérita Universidad Autónoma de PueblaPueblaPueblaMéxico Departamento de Biociencias e Ingeniería Centro Interdisciplinario de Investigaciones y Estudios sobre Medio Ambiente y DesarrolloInstituto Politécnico NacionalCiudad de MéxicoMéxico Programa de Nanociencias y nanotecnología Centro de Investigación y de Estudios AvanzadosCiudad de MéxicoMéxico

Overexpression of neurotrophic factors in nigral dopamine neurons is a promising approach to reverse neurodegeneration of the nigrostriatal dopamine system,a hallmark in Parkinson's disease.The human cerebral dopamine neurotrophic factor(h CDNF)has recently emerged as a strong candidate for Parkinson's disease therapy.This study shows that h CDNF expression in dopamine neurons using the neurotensinpolyplex nanoparticle system reverses 6-hydroxydopamine-induced morphological,biochemical,and behavioral alterations.Three independent electron microscopy techniques showed that the neurotensin-polyplex nanoparticles containing the h CDNF gene,ranging in size from 20 to 150 nm,enabled the expression of a secretable h CDNF in vitro.Their injection in the substantia nigra compacta on day 21 after the 6-hydroxydopamine lesion resulted in detectable h CDNF in dopamine neurons,whose levels remained constant throughout the study in the substantia nigra compacta and striatum.Compared with the lesioned group,tyrosine hydroxylase-positive(TH^(+))nigral cell population and TH+fiber density rose in the substantia nigra compacta and striatum after h CDNF transfection.An increase inβIII-tubulin and growth-associated protein 43 phospho-S41(GAP43 p)followed TH^(+)cell recovery,as well as dopamine and its catabolite levels.Partial reversal(80%)of drugactivated circling behavior and full recovery of spontaneous motor and non-motor behavior were achieved.Brain-derived neurotrophic factor recovery in dopamine neurons that also occurred suggests its participation in the neurotrophic effects.These findings support the potential of nanoparticle-mediated h CDNF gene delivery to develop a disease-modifying treatment against Parkinson's disease.The Institutional Animal Care and Use Committee of Centro de Investigación y de Estudios Avanzados approved our experimental procedures for animal use(authorization No.162-15)on June 9,2019.

关键词： axonal growth brain-derived neurotrophic factor gene delivery nanoparticles neuritogenesis neuronal cytoskeleton neuroregeneration neurorestoration neurotrophic therapy Parkinson's disease reinnervation substantia nigra

CT引导下自体肾脏活检:切线位穿刺路径与非切线位穿刺路径有效性和安全性对比

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国际医学放射学杂志 2017年第3期 352-352页

作者： B.Liu m.O’Dell M.FLORES J.Limback m.Kendall J.Pepe 张庆辉 Department of Radiology Florida Hospital

摘要目的总结本中心关于CT导引下肾脏皮质切线位穿刺活检的经验,并对比其与非切线位穿刺活检的有效性和安全性。材料与方法本回顾性研究经伦理委员会批准,并符合HIPAA。收集自2007年7月—2015年9月的431例CT引导肾穿刺活检病例,记录了... 详细信息

摘要目的总结本中心关于CT导引下肾脏皮质切线位穿刺活检的经验,并对比其与非切线位穿刺活检的有效性和安全性。材料与方法本回顾性研究经伦理委员会批准,并符合HIPAA。收集自2007年7月—2015年9月的431例CT引导肾穿刺活检病例,记录了标本数量、肾小球数量、并发症。肾皮质切线位穿刺:如果穿刺路径平行于肾皮质表面,深度接近肾皮质表面。满意标本的定义:光镜下至少可见10个肾小球,免疫荧光显微镜及电子显微镜下可见1个肾小球。对数据进行卡方检验、t检验、秩和检验、Logistic回归分析。结果 431次活检中,156次(36%)归类为肾皮质切线位穿

关键词：穿刺路径肾皮质切线位与非有效性 CT

Veterans utilizing a federally qualified health center: a clinical snapshot

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military medical Research 2023年第1期10卷 134-136页

作者： Thad E.Abrams Bruce Alexander Antonio flores m.Bryant Howren VHA Office of Rural Health Veterans Rural Health Resource CenterIowa CityIA 52246USA Carver College of medicine The University of IowaIowa CityIA 52242USA Center for Access Delivery Research and Evaluation(CADRE) VA Iowa City Healthcare SystemIowa CityIA 52246USA Community Health Centers of Southeastern Iowa West BurlingtonIA 52655USA Department of Behavioral Sciences and Social medicine College of MedicineFlorida State UniversityTallahasseeFL 32306USA Florida Blue Center for Rural Health Research and Policy College of MedicineFlorida State UniversityTallahasseeFL 32306USA

Dear Editor,Te Veterans Health Administration(VHA)provides healthcare for over 9 million enrolled veterans with approximately 2.7 million of those residing in rural areas[1].Te mISSION Act of 2018 emphasizes VHA collaboration with Federally Qualifed Healthcare Centers(FQHC)to serve rural residing veterans and nearly all existing collaborations involve arrangement of payment for community-based care by VHA to FQHCs.Unfortunately,there is a paucity of descriptive clinical data on existing cross-system collaborations which may help characterize these veterans and aid understanding of conditions for which they may receive treatment across systems.Such data has implications for workforce training,development,and resource allocation[2].Te objective of this report is to describe diferent clinical profles between two mutually exclusive samples:veterans engaged in FQHC only use,and VHA-enrolled veterans engaged in dual VHA and FQHC use.

关键词： Veterans Federally qualified healthcare centers Healthcare utilization Dual use mental health

Curcuma longa L. extract improves the cortical neural connectivity during the aging process

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Neural Regeneration Research 2017年第6期12卷 875-880页

作者： Gonzalo flores Laboratorio de Neuropsiquiatría Instituto de Fisiología Benemérita Universidad Autónoma de Puebla

Turmeric or Curcuma is a natural product that has anti-inflammatory, antioxidant and anti-apoptotic pharmacological properties. It can be used in the control of the aging process that involves oxidative stress, inflammation, and apoptosis. Aging is a physiological process that affects higher cortical and cognitive functions with a reduction in learning and memory, limited judgment and deficits in emotional control and social behavior. moreover, aging is a major risk factor for the appearance of several disorders such as cerebrovascular disease, diabetes mellitus, and hypertension. At the brain level, the aging process alters the synaptic intercommunication by a reduction in the dendritic arbor as well as the number of the dendritic spine in the pyramidal neurons of the prefrontal cortex, hippocampus and basolateral amygdala, consequently reducing the size of these regions. The present review discusses the synaptic changes caused by the aging process and the neuroprotective role the Curcuma has through its anti-inflammatory, antioxidant and anti-apoptotic actions.

关键词： Curcuma longa cortical curcumin hippocampus synaptic antioxidant spine connectivity cortex