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Combined effect of WS_(2) and Ti_(3)C_(2)T_(x) MXene favors oil-based ultra-low friction on rough steel-steel interface at elevated temperatures

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Science China(Technological Sciences) 2024年第7期67卷 1991-2002页

作者： LIU YangQin CHEN Lei WANG Yang qian linmao Tribology Research Institute State Key Laboratory of Rail Transit Vehicle SystemSchool of Mechanical EngineeringSouthwest Jiaotong UniversityChengdu 610031China Key Laboratory of Advanced Technologies of Materials(Ministry of Education) Research Institute of Frontier ScienceSouthwest Jiaotong UniversityChengdu 610031China

The lubrication performance of liquids is severely restricted and is degraded in high-temperature environments. Stable and reliable lubrication in high temperature environments has been a long-standing goal in various industrial fields. In this study,WS_(2)and Ti_(3)C_(2)T_(x)MXene nanoflakes were used as oil-based lubricant additives to generate ultra-low friction and even superlubricity(friction coefficient of ~0.007) at elevated temperatures(400℃), which has hitherto not been achieved by both individual pristine materials, WS_(2)and Ti_(3)C_(2)T_(x)MXene. Viscosity and thermogravimetric characterization revealed improvements in the high-temperature rheological properties and thermal stability of the lubricating base oil, indicating improved loadbearing and continuous lubrication capabilities at elevated temperatures. X-ray photoelectron spectroscopy, transmission electron microscopy, and atomic force microscopy demonstrated that the formation of an iron/titanium/tungsten-rich oxide lubricious thin film at the sliding interface reduced the interfacial shear stress, which was responsible for the observed friction and wear reductions at high contact pressures(> 1.1 GPa). Although the titanium/tungsten oxide film was gradually removed after prolonged sliding, a sufficiently thick iron oxide film maintained a low friction coefficient for at least 2 h. The improved surface quality facilitates the achievement of ultra-low friction and reduced wear. The proposed lubrication methodology has a broad utilization potential as a wear-reduction strategy across various industrial fields at elevated temperatures.

关键词： ultra-low friction high-temperature wear reduction lubricating additive tungsten disulfide MXene

Influence of Film Thickness on Nanofabrication of Graphene Oxide

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Nanomanufacturing and Metrology 2024年第2期7卷 13-25页

作者： Chuan Tang Lei Chen linmao qian Tribology Research Institute The State Key Laboratory of Rail Vehicle SystemSchool of Mechanical EngineeringSouthwest Jiaotong UniversityChengdu 610031China

Nanofabrication of two-dimensional materials through mechanical machining is normally influenced by not only process parameters such as load and velocity but also intrinsic properties such as strength and ***,we examined the effects of graphene oxide(GO)film thickness on nanofabrication on the plane surfaces and at the step edges using scanning probe microscope *** material removal of GO initiates at the load above a critical value,which strongly depends on film thickness and *** the increase in film thickness,the critical load decreases monotonically on the plane surfaces but increases gradually at the step ***,the critical load for the GO monolayer at the step edges is at least 25 times lower than that on the plane surfaces,and the gap decreases to around 3 times when GO thickness increases to four ***,mechanical nanofabrication initiating from the GO step edge allows producing various nanopatterns under extremely low loads around 1 ***,the GO nanostructures are deoxidized by annealing at 800°C in high-purity argon to restore their highly functionalized conjugated structures,which are supported by X-ray diffraction and Raman *** work provides a novel approach to fabricating graphene-like nanostructures by deoxidizing GO after nanofabrication,which holds significant potential for applications in graphene-based devices.

关键词： Graphene oxide Nanofabrication Film thickness step edge Nanopattern Deoxidized treatment

Simulation model optimization for bonnet polishing considering consistent contact area response

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Frontiers of Mechanical Engineering 2024年第4期19卷 87-105页

作者： Yanjun HAN Haiyang ZHANG Menghuan YU Jinzhou YANG linmao qian School of Mechanical Engineering Southwest Jiaotong UniversityChengdu 610031China Institute of Data Science Maastricht UniversityMaastricht 6229ENthe Netherlands

Simulation model optimization plays a crucial role in the accurate prediction of material removal function in bonnet polishing processes,but model complexity often poses challenges to the practical implementation and efficiency of these *** paper presents an innovative method for optimizing simulation model parameters,focusing on achieving consistent contact area and the accurate prediction of the material removal function while preventing increase in model ***,controllable and uncontrollable factors in bonnet simulations are analyzed,and then a simplified contact model is developed and applied under constant force *** characterize the bonnet's contact performance,a contact area response curve is introduced,which can be obtained through a series of single spot contact ***,a rubber hyperelastic parameter optimization model based on a neural network is proposed to achieve optimal matching of the contact area between simulation and *** average deviation of the contact area under different conditions was reduced from 22.78%before optimization to 3.43%after optimization,preliminarily proving the effectiveness of the proposed simulation optimization ***,orthogonal experiments are further conducted to validate the proposed *** comparison between the experimental and predicted material removal functions reveals a high consistency,validating the accuracy and effectiveness of the proposed optimization method based on consistent contact *** research provides valuable insights into enhancing the reliability and effectiveness of bonnet polishing simulations with a simple and practical approach while mitigating the complexity of the model.

关键词： bonnet polishing simulation contact area tool influence function optimization

Two material removal modes in chemical mechanical polishing:mechanical plowing *** bonding

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Friction 2024年第5期12卷 897-905页

作者： Yuan WU Liang JIANG Wenhui LI Jiaxin ZHENG Yushan CHEN linmao qian Tribology Research Institute State Key Laboratory of Rail Transit Vehicle SystemSouthwest Jiaotong UniversityChengdu610031China

With the rapid development of semiconductors,the number of materials needed to be polished sharply *** material properties vary significantly,posing challenges to chemical mechanical polishing(CMP).Accordingly,the study aimed to classify the material removal *** on the CMP and atomic force microscopy results,the six representative metals can be preliminarily classified into two groups,presumably due to different material removal *** the tribology perspective,the first group of Cu,Co,and Ni may mainly rely on the mechanical plowing *** adding H_(2)O_(2),corrosion can be first enhanced and then suppressed,affecting the surface mechanical ***,the material removal rate(MRR)and the surface roughness increase and *** comparison,the second group of Ta,Ru,and Ti may primarily depend on the chemical bonding *** H_(2)O_(2)can promote oxidation,increasing interfacial chemical ***,the MRR increases,and the surface roughness decreases and levels *** addition,CMP can be regulated by tuning the synergistic effect of oxidation,complexation,and dissolution for mechanical plowing,while tuning the synergistic effect of oxidation and ionic strength for chemical *** findings provide mechanistic insight into the material removal mechanism in CMP.

关键词： Chemical mechanical polishing corrosion wear material removal mode mechanical plowing chemical bonding

Role of interfacial water in adhesion,friction,and wear--A critical review

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Friction 2021年第1期9卷 1-28页

作者： Lei CHEN linmao qian Tribology Research Institute State Key Laboratory of Traction PowerSouthwest Jiaotong UniversityChengdu 610031China

Surficial water adsorption and interfacial water condensation as natural phenomena that can alter the contact status of the solid interface and tribological performances are crucial in all length scales,i.e.,from earthquakes to skating at the macroscale level and even to micro/nano-electromechanical systems(M/NEMS)at the microscale/nanoscale *** water exhibits diverse structure and properties from bulk water because of its further interaction with solid *** this paper,the evolutions of the molecular configuration of the adsorbed water layer depending on solid surface chemistry(wettability)and structure,environmental conditions(i.e.,relative humidity and temperature),and experimental parameters(i.e.,sliding speed and normal load)and their impacts on tribological performances,such as adhesion,friction,and wear,are systematically *** on these factors,interfacial water can increase or reduce adhesion and friction as well as facilitate or suppress the tribochemical wear depending on the water condensation kinetics at the interface as well as the thickness and structure of the involved interfacial water.

关键词： water adsorption water condensation adhesion friction tribochemical wear

Friction-Induced Nanofabrication: A Review

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Chinese Journal of Mechanical Engineering 2021年第2期34卷 26-51页

作者： Bingjun Yu linmao qian Tribology Research Institute State Key Laboratory of Traction PowerSouthwest Jiaotong UniversityChengdu 610031China

As the bridge between basic principles and applications of nanotechnology,nanofabrication methods play significant role in supporting the development of nanoscale science and engineering,which is changing and improving the production and lifestyle of the *** lithography and other alternative technologies,such as nanoimprinting,electron beam lithography,focused ion beam cutting,and scanning probe lithography,have brought great progress of semiconductor industry,IC manufacturing and micro/nanoelectromechanical system(MEMS/NEMS)***,there remains a lot of challenges,relating to the resolution,cost,speed,and so on,in realizing high-quality products with further development of *** of the existing techniques can satisfy all the needs in nanoscience and nanotechnology at the same time,and it is essential to explore new nanofabrication *** a newly developed scanning probe microscope(SPM)-based lithography,friction-induced nanofabrication provides opportunities for maskless,flexible,low-damage,low-cost and environment-friendly processing on a wide variety of materials,including silicon,quartz,glass surfaces,and so *** has been proved that this fabrication route provides with a broad application prospect in the fabrication of nanoimprint templates,microfluidic devices,and micro/nano optical *** paper hereby involved the principals and operations of friction-induced nanofabrication,including friction-induced selective etching,and the applications were reviewed as well for looking ahead at opportunities and challenges with nanotechnology *** present review will not only enrich the knowledge in nanotribology,but also plays a positive role in promoting SPM-based nanofabrication.

关键词： Scanning probe microscope Tip-based lithography Friction-induced nanofabrication Friction-induced selective etching

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微纳尺度固体超滑研究进展

摩擦学学报（中英文） 2024年第4期44卷 437-459页

作者：孙军辉张鑫张金璐葛蒲宇程子文蒲吉斌鲁志斌钱林茂西南交通大学机械工程学院牵引动力国家重点实验室四川成都610031 中国科学院兰州化学物理研究所固体润滑国家重点实验室甘肃兰州730000 中国科学院宁波材料技术与工程研究所中科院海洋新材料与应用技术重点实验室浙江宁波315201

超润滑,指摩擦阻力极低的状态,是润滑技术发展追求的终极目标.超滑能够大幅度减小甚至消除滑动界面的摩擦磨损、抑制摩擦能量耗散,有效延长运动部件的可靠性和服役寿命,具有重要的基础研究和工程应用价值.鉴于微纳尺度固体超滑是实现宏... 详细信息

超润滑,指摩擦阻力极低的状态,是润滑技术发展追求的终极目标.超滑能够大幅度减小甚至消除滑动界面的摩擦磨损、抑制摩擦能量耗散,有效延长运动部件的可靠性和服役寿命,具有重要的基础研究和工程应用价值.鉴于微纳尺度固体超滑是实现宏观工程超滑的基础,是可能解决现代制造业超精密、微型化发展面临严重摩擦磨损瓶颈问题的有效途径,因此有必要对学术界目前实现微纳尺度固体超滑的原理和典型方法进行探讨,深化认识固体超滑的实现策略,提高摩擦学研究服务现代文明的支撑能力.从早期的生活生产经验总结,到近代的机械啮合理论、黏着学说乃至当代原子分子水平摩擦理论,人们对摩擦和润滑的认识不断提高,但都不曾回避“摩擦总是伴随着动能/机械能消耗”的观点,即摩擦是界面滑动发生能量耗散的力学体现,滑动势垒的存在是滑动产生摩擦阻力的本征原因.因此,本文中将围绕如何降低滑动势垒、减小摩擦耗散的思辨理念,介绍当前固体超滑研究的发展和现状,着重探讨实现微纳尺度超滑的一般策略,简要综述学术界目前典型固体超润滑的原理和方法等.首先,介绍了结构超滑的提出、发展及其应用;其次,探讨了连续滑动超低摩擦行为的基础原理及应用等;此外,阐述了近年来提出的压力诱导超滑的理念,着重从现象发现、基本原理、试验观测方法及其可能的基础和应用价值等方面,介绍了压力诱导超滑的研究进展.最后,从基础研究和应用技术开发方面提出了超滑研究可能需要加强的几方面内容.以期通过当前综述,丰富学术界对超润滑的基本问题、科学意义及其应用价值的认识,阐明固体超滑的微观机理、实现策略,指出固体超滑面临的挑战及发展方向,助力固体超润滑从基础研究向工程应用迈进.

关键词：超润滑超低摩擦结构超滑连续滑动压力诱导超滑

Mechanochemical reactions of GaN-Al_(2)O_(3) interface at the nanoasperity contact:Roles of crystallographic polarity and ambient humidity

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Friction 2022年第7期10卷 1005-1018页

作者： Jian GUO Jian GAO Chen XIAO Lei CHEN linmao qian School of Mechanical Engineering University of South ChinaHengyang 421001China Tribology Research Institute State Key Laboratory of Traction PowerSouthwest Jiaotong UniversityChengdu 610031China Advanced Research Center for Nanolithography(ARCNL) Science Park 106Amsterdam 1098XGthe Netherlands Technology and Equipment of Rail Transit Operation and Maintenance Key Laboratory of Sichuan Province Southwest Jiaotong UniversityChengdu 610031China

Mechanochemical reactions of the GaN-Al_(2)O_(3) interface offer a novel principle for scientific and technological merits in the micro-/nano-scale ultra-precision surface *** this work,the mechanochemical reactions on Ga-and N-faced GaN surfaces rubbed by the Al_(2)O_(3) nanoasperity as a function of the environmental humidity were *** results indicate that the N-face exhibits much stronger mechanochemical removal over the relative humidity range of 20%-80%than the *** water molecules in environmental conditions significantly promotes the interfacial mechanochemical reactions and hence accelerates the atomic attrition on *** hypothesized mechanism of the selective water-involved mechanochemical removal is associated with the dangling bond configuration,which affects the mechanically-stimulated chemical reactions via altering the activation energy barrier to form the bonding bridge across the sliding *** findings can enrich the understanding of the underlying mechanism of mechanochemical reactions at GaN-Al_(2)O_(3) interface and a broad cognition for regulating the mechanochemical reactions widely existing in scientific and engineering applications.

关键词： crystallographic polarity ambient humidity mechanochemical removal GaN-Al_(2)O_(3)interface

Detecting van der Waals forces between a single polymer repeating unit and a solid surface in high vacuum

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Nano Research 2019年第1期12卷 57-61页

作者： Wanhao Cai Chen Xiao linmao qian Shuxun Cui Key Laboratory of Advanced Technologies of Materials(Ministry of Education) Southwest Jiaotong UniversityChengdu 610031China

Ubiquitous van der Waals(vdW)forces are very importa nt for nano *** the vdW forces between two surfaces(or two layers)have been measured for several decades,a direct detection at the single-molecule level is still ***,we report a novel method to solve this problem in high vacuum by means of AFM-based sin gle-molecule force spectroscopy(SMFS).Solve nt molecules and surface adsorbed water are removed thoroughly under high vacuum so that the situation is greatly simplified.A constant force plateau can be observed when a polymer chain is peeled off from a substrate in high ***,the vdW forces between one polymer repeating unit and the substrates can be *** experimental results show that the vdW forces(typical range:21-54 pN)are dependent on the species of substrates and the size of polymer repeating unit,which is in good accordance with the theoretical *** is expected that this novel method can be applied to detect other non-covalent interactions(such as hydrogen bond andπ-πstacking)at the single-molecule level in the future.

关键词： van der Waals forces high vacuum atomic force microscopy single-molecule studies polymer desorption