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Structural studies and conductivity of [Fe(O3C4)(COO)]·H2O based H4btec (H4btec = 1,2,4,5-benzenetetracarboxylic acid)

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Open Journal of Inorganic Chemistry 2013年第4期3卷 100-108页

作者： Manel Halouani Mohamed Abdelhedi Mohamed Dammak Nathalie Audebrand lilia Ktari Laboratoire de Chimie Inorganique Faculté des Sciences de Sfax Université de Sfax Sfax Tunisia Laboratoire de Matériaux Inorganiques: Chimie Douce et Réactivité UMR 6226 Sciences Chimiques de Rennes Université Rennes 1 Rennes France

A new metal-organic hybrid compound?[Fe(O3C4)(COO)]·H2O I has been hydrothermally synthesized and characterized by single-crystal X-ray diffraction. Rust crystals crystallize in the monoclinic system, space group I2/a, a = 6.9651(2) A, b = 8.12630(10) A, c = 19.4245(2) A, β = 92.6600(10)°;V = 1098.25(4) A3;Z = 2 and Dx =3.63g/cm3. The refinement converged into R = 0.042;Rw = 0.058. The structure, determined by single crystal X-ray diffraction, consists of a network of FeO6 centers, octahedral coordinated by btec (btec = 1,2,4,5-benzenetetracarboxylic acid) anions giving rise to a two-dimensional sheet structure. In the compound I,?[Fe(O3C4)(COO)]·H2O, the FeO6 group bridged by the 1,2,4,5-benzenetetracarboxyl anion exist in a unit cell, with each anion lying about an inversion centre. One of the FeO2 adistance [1.965(2)] significantly corresponds to the shortest distance as the other and the distances found in the axial direction of compound I.

关键词： Hydrothermal Synthesis X-Ray Diffraction Crystal Structure

Patients with functional bowel disorder have disaccharidase deficiency:A single-center study from Russia

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World Journal of Clinical Cases 2021年第17期9卷 4178-4187页

作者： Saria Dbar Olga Akhmadullina Elena Sabelnikova Nikolai Belostotskiy Asfold Parfenov Svetlana Bykova Sergey Bakharev Elena Baulo Alexandra Babanova lilia Indeykina Tatyana Kuzmina Tatiana Kosacheva Aleksey Spasenov Alina Makarova Non-inflammatory Bowel Diseases Moscow Health DepartmentMoscow Clinical Scientific Center n.a.A.S.LoginovMoscow 111123Russia Moscow Health Department Moscow Clinical Scientific Center n.a.A.S.LoginovMoscow 111123Russia Pre-Clinical Research Laboratory Moscow Clinical Scientific Center Named after A.S.Loginov MHDMoscow 111123Russia Department of Bowel Pathology Moscow Health DepartmentMoscow Clinical Scientific Center n.a.A.S.LoginovMoscow 111123Russia Laboratory of Functional Diagnostics of Intestinal Diseases Moscow Health DepartmentMoscow Clinical Scientific Center n.a.A.S.LoginovMoscow 111123Russia Nutraceuticals Laboratory Moscow Health DepartmentMoscow Clinical Scientific Center n.a.A.S.LoginovMoscow 111123Russia Department of Medical Statistics Moscow Health DepartmentMoscow Clinical Scientific Center n.a.A.S.LoginovMoscow 111123Russia

BACKGROUND Functional bowel disorder(FBD)may be caused by a decrease in disaccharidase ***,the timely diagnosis of disaccharidase deficiency could lead to a better prognosis in patients with this *** To determine the potential value of intestinal disaccharidases glucoamylase,maltase,sucrase,and lactase in understanding the etiology and pathogenesis of *** A total of 82 FBD patients were *** to the Rome IV criteria(2016),23 patients had diarrhea-predominant irritable bowel syndrome(IBS),33 had functional diarrhea,10 had constipation-predominant IBS,4 had functional constipation,and 12 had mixed *** Dahlqvist method was used to measure disaccharidase activity in the brush-border membrane of mature enterocytes of the small intestine,in duodenal biopsies obtained during *** Lactase deficiency was detected in 86.5%of patients,maltase deficiency in 48.7%,sucrase deficiency in 50%,and glucoamylase deficiency in 84.1%.The activities of all enzymes were reduced in 31.7%of patients,and carbohydrase deficiency was detected in 63.5%of *** low activity of enzymes involved in membrane digestion in the small intestine was found in 95.2%of *** In 78 of the 82 patients with FBD,gastrointestinal symptoms were associated with disaccharidase deficiency.

关键词： Functional bowel disorder Irritable bowel syndrome Disaccharidase deficiency Maltase deficiency Sucrase deficiency Lactase deficiency

Effects of nanofertilizer and nano-plant hormone on soil chemical properties and microbial community in two different soil types

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Pedosphere 2023年第5期33卷 765-775页

作者： John Lester Viscara PIDE Nolissa Delmo ORGANO Andre Freire CRUZ lilia M.FERNANDO Lucille C.VILLEGAS Evelyn F.DELFIN Michelle Ann Magat CALUBAQUIB Roselle Estera MADAYAG Erlinda S.PATERNO Division of Soil Science Agricultural Systems InstituteCollege of Agriculture and Food Science(CAFS)University of the Philippines Los Baños(UPLB)CollegeLaguna 4031Philippines Graduate School of Life and Environmental Sciences Kyoto Prefectural University1-5 Shimogamohangi-choSakyo-kuKyoto 606-8522Japan Crop Biotechnology Division Institute of Crop ScienceCAFSUPLBCollegeLaguna 4031Philippines Microbiology Division Institute of Biological SciencesCollege of Arts and SciencesUPLBCollegeLaguna 4031Philippines Institute of Plant Breeding CAFSUPLBCollegeLaguna 4031Philippines Isabela State University Cabagan Campus Isabela 3328Philippines

Application of nanotechnology in agriculture has been expanded to improve crop *** impact of nanomaterials(NMs)on factors that influence the survival and function of beneficial microorganisms is a less studied aspect that needs to be better *** a few studies have assessed the effects of NMs on beneficial soil *** study was conducted to assess the effects of nanofertilizer FertiGroe?N(FG-N)and nano-plant hormone HormoGroe?auxin(HG-A)on the chemical properties and microbial communities of two contrasting soils,Lipa clay loam(CL)and Sariaya sandy loam(SL),over a 35-d incubation period in the *** and fungal communities were evaluated using amplicon sequencing analysis within the 16S and internal transcribed spacer regions,*** application of FG-N significantly decreased soil pH,but did not affect total N and available P for both soil types.A significant increase in exchangeable K was observed only in Lipa *** application of HG-A had no significant effect on soil chemical *** the bacterial community after incubation,the relative abundances of Acidobacteriia,Chthonomonadetes,and Saccharimonadia decreased,whereas Acidimicrobiia,Chloroflexia,and Gemmatimonadetes increased with FG-N application in Lipa *** application of HG-A increased the relative abundance of Rubrobacteria,Chthonomonadetes,and Chloroflexia in Lipa *** the fungal community,FG-N application increased the relative abundance of Sordariomycetes,Agaricomycetes,and Eurotiomycetes,whereas Dothideomycetes and Mortierellomycetes decreased in Lipa CL after *** Sariaya SL,FG-N application increased the relative abundance of Dothideomycetes,Eurotiomycetes,and Mortierellomycetes,but decreased that of Sordariomycetes and *** classes observed in the control samples were not detected in the HG-A treatment,but were recovered after incubation in Lipa *** microbial diversity in both soil types showed sl

关键词： amplicon sequencing bacterial community crop production fungal community microbial diversity nanomaterial nanotechnology

Novel, X-ray supported kinetic imaging of hidden-lifestyle arthropods

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Insect Science 2021年第1期28卷 281-284页

作者： Sandor Keszthelyi David Szollosi lilia Strobe Szabolcs Osvath Krisztian Szigeti Zsolt Pbnya Adam Csoka Tamas Donko Faculty of Agricultural and Environment Sciences Department of Plant Production and ProtectionInstitute of Plant ScienceKaposvar UniversityKaposvarHungary Kinepict Ltd. BudapestHungary Medicopus Nonprofit Ltd. KaposvarHungary

Dear Editor,There are several arthropods,which live and develop covertly in plant *** plant tissues surrounding them provide them with shelter during their vulnerable developing stage or ensure overwintering as well a... 详细信息

关键词： arthropod kinetic hidden

Cytokines and endothelial adhesion molecules (sVCAM-1) in preeclampsia

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Advances in Bioscience and Biotechnology 2013年第3期4卷 352-355页

作者： Aleksandr Trunov Olga Obukhova Olga Gorbenko Alya Shvayk lilia Trunova Research Center of Clinical and Experimental Medical Siberian Branch of the Russian Academy of Medical Sciences Novosibirsk Russia

In the purpose of studing the pathogenetic features of the pathological process there were investigated cytokine levels with proinflammatory and anti-inflammatory activity, and also the indicators of endothelial dysfunction in blood serum women with moderate and severe preeclampsia. There were found high concentrations of pro-inflammatory cytokines IL-1β, IL-6 and IL-8, and vascular endothelial adhesion molecule-1 (sVCAM-1), which correlated with the severity of the process. Also a significant decrease in concentrations TGF-β2 and IL-10 insevere preeclampsia was indicated, which may testify the exhaustion of adaptive mechanisms and, apparently, can be an additional diagnostic criterion for the prediction and assessment of the severity of the pathological process.

关键词： Preeclampsia Cytokines Inflammation Endothelial Dysfunction

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在夏威夷——你发现了什么?

大视野 2007年第9期 52-55页

作者： lilia Cui

【所谓旅游观光——就是人们在旅行的过程中,去发现闪光的一切……】夏威夷群岛夏威夷群岛地处太平洋中心,由火山爆发形成,总面积10923平方英里,其中海域面积为4508平方英里,陆地面积6423平方英里,总人口在2000年12月为1,211,537人。

关键词：平方英里夏威夷人火山爆发海域面积毛伊夏威夷王国黄金海岸捕鲸里长岸线总长

Nitrogen/Ammonium Concentration Response of Vegetable and Flower Crops

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Journal of Agricultural Science and Technology(B) 2014年第4期4卷 261-266页

作者： Armando Hemandez-Perez Oscar Gabriel Villegas-Torres Martha lilia Dominguez-Patifio Martha lilia Dominguez-Patino Hector Sotelo-Nava Antonio Rodriguez-Martinez Luis Alonso Valdez-Aguilar Iria Alia-Tejacal Faculty of Agricultural Sciences University Autonomous of the State of Morelos Cuernavaca 62209 Mexico Faculty of Chemical Sciences and Engineering University Autonomous of the State of Morelos Cuernavaca 62209 Mexico EngineeringandAppliedScience Research Center UniversityAutonomous of the State ofMorelos Cuernavaca 62209 Mexico Department of Horticulture University Autonomus Agrarian Antonio Narro Saltillo 25315 Mexico

Nitrogen （N） is the element with the greatest influence on the growth of vegetables and ornamentals, however, form of delivery, either as nitrate （NO3） or ammonium （NH4＋） has different effects on plant development. The NO3 is the main form of N that plants absorb, but when it is the only source of N that has slight effects on root growth, no effects over enzymatic activities, and stimulates the absorption and translocation of cations within the plant. The NH4＋ is the easiest way of assimilation but is highly toxic when the only source or with respect to the concentration of NO3 is too high. To avoid toxicity, the NH4＋ must not exceed 20% of the total N amount in the formulation, however, it is important to consider the species, variety and environmental conditions. The N as supplied also affects the resistance or susceptibility of plants to diseases, but depends on the species and the type of pathogen.

关键词： Nitrate ammonium vegetables ornamental toxicity nutrition.

A Profile of Traumatic Brain Injury within Hospital Emergency Departments—A Retrospective Study in the Republic of Moldova

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Open Journal of Preventive Medicine 2022年第9期12卷 175-189页

作者： Svetlana Cociu Angela Cazacu-Stratu lilia Chiosea Gheorghe Rojnoveanu Serghei Cebanu Corinne Peek-Asa Department of Preventive Medicine Nicolae Testemitanu State University of Medicine and Pharmacy Chisinau Republic of Moldova Valentin Ignatenco Municipal Children Hospital Chisinau Republic of Moldova Nicolae Anestiadi Department of Surgery No.1 Nicolae Testemitanu State University of Medicine and Pharmacy Chisinau Republic of Moldova Emergency Medicine Institute Chisinau Republic of Moldova Department of Epidemiology School of Public Health University of California San Diego USA

Background: Traumatic brain injury (TBI) is a critical public health and socio-economic problem throughout the world, making epidemiological monitoring of incidence, prevalence, and outcome of TBI necessary. TBI is a major cause of mortality and morbidity in adolescents, young adults, and the elderly, one of the leading causes being road traffic accidents. Methods: A retrospective study was conducted among patients with TBI within 2 medical institutions in Chisinau municipality: Emergency Medicine Institute (EMI) and Valentin Ignatenco Municipal Children’s Hospital (MCH). A questionnaire was applied, completed on the basis of medical records according to the International Classification of Diseases (ICD) 10 codes. The collection period was August 1-October 31, 2018. Data were uploaded using the existing electronic data collection tool—Red Cap and analyzed through Microsoft Excel. Data collection was performed by a resident neurosurgery and a scientific researcher. The ethics committee’s approval has been obtained. Results: There have been identified 150 patients: 57 cases (38.5%) of TBI among children and 93 cases (61.5%) among adults aged between 18 - 73 years old. A large majority (62%) of head injuries were among patients from the urban area (most in adults—60% and males—74%). The most common mechanisms of head injury were falls (53.3%) and road traffic injuries (24%), followed by assault (14.7%) and struck by/or against (8%). The distributions by place of occurrence highlighted that most injuries occurred at home (33.4%) and in transport area (25.3%). Most head injuries were registered among men 121 (81.2%) with a predominance of minor Glasgow Coma Scale (GCS) (65.1%), followed by moderate GCS (9.4%), while in women all cases with GCS minor (18.8%). Conclusion: The data obtained could be useful for the hospital administration in managing the necessary resources and for conducting information campaigns among the high-risk groups.

关键词： Traumatic Brain Injury Emergency Departments TBI Registry Prevention

Calcium Oxalate and Other Cladode Features in Opuntia ficus-indica Resistant Cultivars to Dactylopius coccus Costa

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Journal of Agricultural Chemistry and Environment 2023年第2期12卷 112-123页

作者： Yemane Kahsay Berhe Liberato Portillo Lourdes Delgado-Aceves Hilda Palacios-Juárez Ana lilia Vigueras Department of Horticulture and Beles Institute Adigrat University Tigray Ethiopia Departamento de Botánica y Zoología CUCBA-Universidad de Guadalajara Zapopan Mexico Departamento de Madera Celulosa y Papel CUCEI-Universidad de Guadalajara Zapopan Mexico

Multipurpose cactus pear plant with great potential as a source of food and livestock faced a threat from Dactylopius spp in different countries. Specifically, D. coccus is an important pest damaging significant areas in Tigray-Ethiopia. Using pest-resistant cultivars is an important element of an integrated pest management strategy, and studying the mechanisms of resistance is vital. It can be chemical or physical such as oxalate crystals and other cladode characteristics. Cladode features of six cultivars (three O. ficus-indica, two O. cochenillifera, and one O. robusta) were examined for resistance to D. coccus in a completely randomized design (CRD) with three replications. ‘Rojo Pelón’ (O. ficus-indica), ‘Robusta’ (O. robusta), and ‘Bioplástico’ (O. cochenillifera) are resistant cultivars;and ‘Atlixco’ and ‘Chicomostoc’ (O. ficus-indica) and ‘Nopalea’ (O. cochenillifera) are susceptible. Cultivars showed a significant difference in cladode weight in g, and cladode length, cladode width, and cladode thickness in cm, where cladode thickness was higher in ‘Rojo Pelón’ followed by ‘Robusta’. Calcium oxalates number per mm was higher in ‘Bioplástico’ (20.7 ± 2.08) followed by ‘Robusta’ (18.9 ± 2.31) and ‘Rojo Pelón’ (15.9 ± 0.34);and similarly, epidermis thickness found higher in ‘Bioplástico’ (0.21 ± 0.032) and ‘Robusta’ (0.19 ± 0.014), but similar with ‘Rojo Pelón’ (0.18 ± 0.026). However, cuticle thickness didn’t show a difference among cultivars. Cladode thickness, calcium oxalate number, and epidermis thickness had positive correlations with resistance. These results demonstrate that calcium oxalate number and epidermis thickness might have a positive role in D. coccus resistance in O. ficus-indica. This feeding-barring role and the insect-plant interaction need to be studied.

关键词： Cactus Pear Resistance Druses Epidermis Thickness