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Efficient and selective recovery of Gd(Ⅲ)via polyethyleneimine modification of lanthanum-based metal-organic frameworks

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Journal of Rare Earths 2024年第1期42卷 210-219,I0007页

作者： wenhao li lijinhong Huang Bin Xiao Xiaoguang Duan Haike li Lang li Wanfu Huang Ganzhou Key Laboratory of Basin Pollution Simulation and Control Jiangxi University of Science and TechnologyGanzhou341000China Innovation Center for Water Quality Security Technology at Ganjiang River Basin Jiangxi University of Science and TechnologyGanzhou341000China Faculty of Science and Engineering WA School of Mines:MineralsEnergy and Chemical EngineeringCurtin UniversityWAAustralia School of Architecture and Design Jiangxi University of Science and TechnologyGanzhou341000China School of Resources and Architectural Engineering Gannan University of Science and TechnologyGanzhou341000China School of Chemical Engineering and Advanced Materials The University of AdelaideAdelaideSA5005Australia School of Resource and Environmental Engineering Jiangxi University of Science and TechnologyGanzhou341000China

With the development of the economy and the increasing demand for environmental protection,the efficient and selective recovery of Gd(Ⅲ)from actual wastewater is of critical *** this work,lanthanum-based metal-organic framework(LaBDC)materials were prepared by a hydrothermal method,and then polyethyleneimine(PEI)and LaBDC were combined by an impregnation method to form a novel LaBDC@xPEI *** prepared materials were characterized using Fourier transfo rm infrared spectroscopy(FTIR),X-ray diffraction(XRD),scanning electron microscopy(SEM),energy dispersive X-ray spectroscopy(EDX),B runauer-Emmett-Teller(BET),thermogravimetric analysis(TGA)and X-ray photoelectron spectroscopy(XPS).Experiments show that LaBDC@50%PEI has the highest adsorption capacity(181.77 mg/g)among lanthanum-based MOFs with different PEI loadings at pH=5.5,which is about 5.1 times that of bare *** adsorption isotherm analysis shows that LaBDC@50%PEI follows the Langmuir *** addition,the adsorption kinetics of LaBDC@50%PEI follows a pseudo-second-order kinetic model,indicating that the adsorption process is chemical *** is worth noting that LaBDC@50%PEI maintains good adsorption performance and stability after three recycling tests,and exhibits excellent selectivity in cation interference ***,the LaBDC@50%PEI composites possess good stability and hold great promises in rapid recovery of Gd(Ⅲ)from practical aqueous environments.

关键词： Wet-impregnation method Polyethylene imine Metaleorganic frameworks Lanthanum Recovery of Gd(Ⅲ) Rare earths

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Ultrathin organic solvent nanofiltration membrane with polydopamine-HKUST-1 interlayer for organic solvent separation

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Journal of Environmental Sciences 2024年第7期141卷 182-193页

作者： Haike li Xindong li Guozai Ouyang lijinhong Huang Lang li wenhao li Wanfu Huang Duokun li Ganzhou Key Laboratory of Basin Pollution Simulation and Control Jiangxi University of Science and TechnologyGanzhou 341000China Innovation Center for Water Quality Security Technology at Ganjiang River Basin Jiangxi University of Science and TechnologyGanzhou 341000China School of Architecture and Design Jiangxi University of Science and TechnologyGanzhou 341000China WA School of Mines:Minerals Energy and Chemical EngineeringCurtin UniversityWA 6845Australia School of Materials Science and Engineering Tiangong UniversityTianjin 300387China

Polydopamine(PDA)and metal-organic skeleton HKUST-1 were co-deposited on the base membrane of hexamethylenediamine(HDA)-crosslinked polyetherimide(PEI)ultrafiltration membrane as the interlayer,and high-throughput organic solvent nanofiltration membrane(OSN)was prepared by interfacial polymerization and solvent activation *** polyamide(PA)layer surface roughness from 28.4 nm in PA/PEI to 78.3 nm in PA/PDA-HKUST-10.6/PEI membrane,reduced the thickness of the separation layer from 79 to 14 nm,and significantly improved the hydrophilic,thermal and mechanical *** flux of the PA/PDA-HKUST-10.6/PEI membrane in a 0.1 g/L Congo Red(CR)ethanol solution at 0.6 MPa test pressure reached 21.8 L/(m^(2)·hr)and the rejection of CR was 92.8%.Solvent adsorption test,N,N-dimethylformamide(DMF)immersion experiment,and long-term operation test in ethanol showed that the membranes had high solvent *** solvent flux test demonstrated that,under the test pressure of 0.6 MPa,the flux of different solvents ranked as follows:methanol(56.9 L/(m^(2)·hr))>DMF(39.6 L/(m^(2)·hr))>ethanol(31.2 L/(m^(2)·hr))>IPA(4.5 L/(m^(2)·hr))>N-hexane(1.9 L/(m^(2)·hr)).The ability of the membranes to retain dyes in IPA/water dyes solution was also *** flux of the membrane was 30.4 L/(m^(2)·hr)and the rejection of CR was 91.6%when the IPA concentration reached 50%.This OSN membrane-making strategy is economical,environment-friendly and efficient,and has a great application prospect in organic solvent separation systems.

关键词： Interfacial polymerization Organic solvent nanofiltration Interlayer Metal-organic frameworks Polydopamine

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Functional near-infrared spectroscopy in non-invasive neuromodulation

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Neural Regeneration Research 2024年第7期19卷 1517-1522页

作者： Congcong Huo Gongcheng Xu Hui Xie Tiandi Chen Guangjian Shao Jue Wang wenhao li Daifa Wang Zengyong li Beijing Advanced Innovation Center for Biomedical Engineering Key Laboratory for Biomechanics and Mechanobiology of Ministry of EducationSchool of Biological Science and Medical EngineeringBeihang UniversityBeijingChina Beijing Key Laboratory of Rehabilitation Technical Aids for Old-Age Disability National Research Center for Rehabilitation Technical AidsBeijingChina School of Mechatronic Engineering and Automation Foshan UniversityFoshanGuangdong ProvinceChina School of Rehabilitation Engineering Beijing College of Social AdministrationBeijingChina Key Laboratory of Neuro-functional Information and Rehabilitation Engineering of the Ministry of Civil Affairs BeijingChina

Non-invasive cerebral neuromodulation technologies are essential for the reorganization of cerebral neural networks,which have been widely applied in the field of central neurological diseases,such as stroke,Parkinson’s disease,and mental *** significant advances have been made in neuromodulation technologies,the identification of optimal neurostimulation paramete rs including the co rtical target,duration,and inhibition or excitation pattern is still limited due to the lack of guidance for neural *** r,the neural mechanism unde rlying neuromodulation for improved behavioral performance remains poorly ***,advancements in neuroimaging have provided insight into neuromodulation *** near-infrared spectroscopy,as a novel non-invasive optical brain imaging method,can detect brain activity by measuring cerebral hemodynamics with the advantages of portability,high motion tole rance,and anti-electromagnetic *** functional near-infra red spectroscopy with neuromodulation technologies offe rs an opportunity to monitor the cortical response,provide realtime feedbac k,and establish a closed-loop strategy integrating evaluation,feedbac k,and intervention for neurostimulation,which provides a theoretical basis for development of individualized precise neuro *** aimed to summarize the advantages of functional near-infra red spectroscopy and provide an ove rview of the current research on functional near-infrared spectroscopy in transcranial magnetic stimulation,transcranial electrical stimulation,neurofeedback,and braincomputer ***,the future perspectives and directions for the application of functional near-infrared spectroscopy in neuromodulation are *** conclusion,functional near-infrared spectroscopy combined with neuromodulation may promote the optimization of central pellral reorganization to achieve better functional recovery form central nervous system

关键词： brain-computer interface cerebral neural networks functional near-infrared spectroscopy neural circuit neurofeedback neurological diseases neuromodulation non-invasive brain stimulation transcranial electrical stimulation transcranial electrical stimulation

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Enhanced thermoelectric properties of Cu_(3)SbSe_(4)-based materials by synergistic modulation of carrier concentration and phonon scattering

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Journal of Materiomics 2024年第2期10卷 339-347页

作者： Sitong Wei Zhen Ji wenhao li Shuqi Zheng Qing Wang Zhiliang li Lu Yu Sitong Luo Weiyu Song College of New Energy and Materials China University of PetroleumBeijing102249China College of Science China University of PetroleumBeijing102249China Key Laboratory of High-precision Computation and Application of Quantum Field Theory of Hebei Province College of Physics Science and TechnologyHebei UniversityBaoding071002China

Cu_(3)SbSe_(4),a copper-based sulfide free of rare earth elements,has received extensive attention in ther-moelectric ***,its low carrier concentration restricts its widespread *** this study,a microwave-assisted solution synthesis method was used to produce samples of Cu_(3)SbSe_(4),which enabled the formation of CuSe in situ and increased the *** the use of first-principles cal-culations,structural analysis,and performance evaluation,it was found that CuSe can enhance the carrier concentration and that induced nano-defects have a positive effect on reducing the lattice thermal ***,doping with Sn decreases the band gap of the system and moves the Fermi level into the valence band,increasing the carrier concentration to 1.15×10^(-20)cm^(-3).Finally,the zT value of the Cu_(3)Sb_(0.98)Sn_(0.02)Se_(4)sample was achieved at 1.05 at 623 K when the theoretical yield of a single synthesis was 10 mmol.

关键词： Cu_(3)SbSe_(4) Carrier concentration Phonon scattering Synergistic modulation

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Drag reduction capacity of multi-scale and multi-level riblet in turbulent flow

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Biosurface and Biotribology 2024年第1期10卷 7-15页

作者： Dengke Chen wenhao li Yichen Zhao Jinhai liu Xianxian Cui Zehui Zhao Xiaolin liu Huawei Chen College of Transportation Ludong UniversityYantaiShandongChina School of Mechanical Engineering and Automation Beihang UniversityBeijingChina Advanced Innovation Center for Biomedical Engineering Beihang UniversityBeijingChina

For high-speed moving objects,drag reduction has been a prolonged major *** address this problem,passive and negative strategies have been proposed in the preceding *** integration of creatures and nature has been continuously perfected during biological *** structure characteristics,material properties,and special functions of marine organisms can provide inexhaustible inspirations to solve this intractable problem of drag ***,a simple and low-cost laser ablation method was proposed.A multi-scale and multi-level riblet(MSLR)surface inspired by the denticles of the sharkskin was fabricated by controlling the density of the laser path and ablation *** morphology and topographic features were characterised using an electron microscope and a scanning white-light interfering ***,the drag reduction capacity of the bionic riblet surface was measured in a circulating water ***,the mechanism of drag reduction was analysed by the computational fluid dynamics(CFD)*** results show that the MSLR surface has a stable drag reduction capacity with an increase in Reynold(Re)number which was contributed by high-low velocity stripes formed on the MSLR *** study can provide a reference for fabricating spatial riblets with efficient drag reduction at different values of Re and improving marine antifouling.

关键词： BIOMIMICS BIONIC STRUCTURE DRAG REDUCTION

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基于运动合成的旋转变速运动建模及其驱动机构演变

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纺织学报 2024年第9期45卷 220-227页

作者：袁汝旺李文豪天津工业大学机械工程学院天津300387 天津工业大学天津市现代机电装备重点实验室天津300387

为满足织机开口运动停—升—停的工艺特性及其动力学性能,提出一种基于运动合成的旋转变速运动规律构造方法。从组合机构角度提出旋转变速运动驱动机构及其演变,建立不同驱动机构的相对运动传递函数模型。采用目标优化法对旋转变速机构... 详细信息

为满足织机开口运动停—升—停的工艺特性及其动力学性能,提出一种基于运动合成的旋转变速运动规律构造方法。从组合机构角度提出旋转变速运动驱动机构及其演变,建立不同驱动机构的相对运动传递函数模型。采用目标优化法对旋转变速机构尺寸参数进行设计,在相同的中心距半径和转子臂初始位置的情况下建立优化函数并进行求解。仿真结果表明:偏移系数是影响旋转变速运动的关键参数,且变速运动静止时间、相对位移和速度峰值随偏移系数增加而减小;传递函数是影响旋转变速机构运动特性的重要参数,当偏移系数为0.4147时,随传动比的减小,转子臂相对位移减小,同时影响旋转变速机构凸轮特性,传动比大于0.9后不能满足旋转变速机构约束条件;用导杆滑块机构和铰接四杆机构对齿轮机构进行代换,可近似实现变速规律相对运动的传递,其传动误差分别为0.010、0.003 rad;通过减小中心距对铰接四杆机构重新优化可以提高旋转变速机构传动性能,满足高速运动需求。

关键词：运动合成旋转变速运动驱动变速机构偏移系数目标优化织机开口

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High-performance SiO_(x)/MgO_(x)electron-selective contacts for crystalline silicon solar cells

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Science China Materials 2024年第9期67卷 2866-2872页

作者： Kun li Kun Gao Xinyu Wang Xinliang Lou Dacheng Xu Chunfang Xing wenhao li Haicheng li Xinbo Yang College of Energy Soochow Institute for Energy and Materials InnovationS(SIEMIS)Soochow UniversitySuzhou215006China Institute of Functional Nano&Soft Materials Soochow UniversitySuzhou215123China

High carrier recombination loss at the metal and silicon contact regions is one of the dominant factors constraining the power conversion efficiency(PCE)of crystalline silicon(c-Si)solar *** compound-based carrier-selective contacts are being intensively developed to address this *** this work,we present a high-performance electron-selective SiO_(x)/MgO_(x)contact for c-Si solar *** SiO_(x)/MgO_(x)stack is prepared by thermally-grown SiO_(x)(∼0.7 nm)and thermally-evaporated MgO_(x)(~1.0 nm).The electron selectivity of SiO_(x)/MgO_(x)contact is investigated by measuring the surface passivation and the contact resistivity(ρ_(c))on the c-Si *** results demonstrate that optimized SiO_(x)/MgO_(x)contact displays a very lowρ_(c)(3.4 mΩcm^(2))and a good surface passivation on an n-type c-Si surface simultaneously.A high PCE of 21.1%is achieved on an n-type c-Si solar cell featuring a full-area SiO_(x)/MgO_(x)rear contact.

关键词： crystalline silicon solar cell electron-selective contact magnesium oxide

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基于单胞孔隙结构的多孔泡沫界面对流换热系数研究

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工程热物理学报 2024年第9期45卷 2724-2731页

作者：李文浩范蓉蓉武汉理工大学汽车工程学院武汉430070 现代汽车零部件技术湖北省重点实验室武汉430070

界面对流换热系数是采用局部热非平衡模型研究多孔泡沫流动传热过程的一个关键参数。本文采用体中心切球法构造多孔泡沫单胞孔隙结构来模拟多孔泡沫真实物理结构,在孔隙结构下进行流动换热过程的数值模拟,计算对流换热系数,并与文献中... 详细信息

界面对流换热系数是采用局部热非平衡模型研究多孔泡沫流动传热过程的一个关键参数。本文采用体中心切球法构造多孔泡沫单胞孔隙结构来模拟多孔泡沫真实物理结构,在孔隙结构下进行流动换热过程的数值模拟,计算对流换热系数,并与文献中实验研究获取的努塞尔数对比以验证数值模拟准确性,然后对不同孔隙结构的多孔泡沫流动换热过程进行数值模拟计算,利用数据拟合建立界面对流换热系数准则关联式。基于建立的界面对流换热系数准则关联式,对多孔泡沫在局部热平衡及局部热非平衡两种假设下的流动传热过程进行宏观数值模拟,并与文献实验值进行对比,结果进一步验证了所建立关联式的准确性,说明基于单胞孔隙结构获取界面对流换热系数的方法是有效的,同时也验证了局部热非平衡模型能够更加精确地描述多孔泡沫的流动传热过程。

关键词：多孔泡沫单胞孔隙结构局部热非平衡界面对流换热系数

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坚守文化本色拥抱科技发展——2023首届中国民族改良乐器精品展论坛综述

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人民音乐 2024年第2期 69-71页

作者：李文浩兰州文理学院音乐舞蹈学院

2023第三十届中国国际乐器展览会(以下简称“中国国际乐器展”)于6月29日—7月2日在北京举行,其间举办的“首届中国民族改良乐器精品展”活动,成为本次展会的“点睛之笔”。这是中国国际乐器展成立三十年来,首次将目光聚焦在“民族改良... 详细信息

2023第三十届中国国际乐器展览会(以下简称“中国国际乐器展”)于6月29日—7月2日在北京举行,其间举办的“首届中国民族改良乐器精品展”活动,成为本次展会的“点睛之笔”。这是中国国际乐器展成立三十年来,首次将目光聚焦在“民族改良乐器”领域,为沉寂许久的“乐改”工作重拾焦点,活动由“成果评选”“精品展”和“论坛”三个部分组成。

关键词：论坛综述点睛之笔首届

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考虑不对称转速边界约束的变速抽蓄机组综合惯量调频控制

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电力系统自动化 2024年第16期48卷 88-98页

作者：成昕雨王丹李文浩毛承雄强电磁技术全国重点实验室(华中科技大学) 湖北省武汉市430074 华中科技大学电气与电子工程学院湖北省武汉市430074

当系统出现频率跌落时,变速抽蓄机组可大幅降低转速、迅速释放转子动能,从而为系统提供惯量支撑,但目前已有的调频方案未能有效发挥变速抽蓄机组的这一优势。为充分利用转子动能,提出一种考虑不对称转速边界约束的变速抽蓄机组综合惯量... 详细信息

当系统出现频率跌落时,变速抽蓄机组可大幅降低转速、迅速释放转子动能,从而为系统提供惯量支撑,但目前已有的调频方案未能有效发挥变速抽蓄机组的这一优势。为充分利用转子动能,提出一种考虑不对称转速边界约束的变速抽蓄机组综合惯量调频控制策略。首先,从变速抽蓄机组的有功支撑特性和不对称转速约束条件出发,得出适用于变速抽蓄机组的最优频率控制结构,该结构中包含两个时间常数不同的虚拟惯量控制环节。然后,分析各惯量控制环节的作用并整定相关参数。在此基础上,计及变速抽蓄机组运行特性与电力系统调频需求,设计了变速抽蓄机组不对称综合惯量控制策略,使得机组转速降低时可以为系统提供更大的惯量支撑。仿真结果表明,所提调频策略能够充分发挥变速抽蓄机组的优势,维持系统频率稳定。

关键词：变速抽蓄机组综合惯量控制频率调节惯量支撑转子动能

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