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Experimental reconstructions of 3D atomic structures from electron microscopy images using a Bayesian genetic algorithm

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npj Computational Materials 2022年第1期8卷 2076-2083页

作者： Annick De Backer Sandra Van Aert Christel Faes Ece Arslan Irmak Peter DNellist lewys jones EMAT University of AntwerpGroenenborgerlaan 1712020AntwerpBelgium NANOlab Center of Excellence University of AntwerpGroenenborgerlaan 1712020AntwerpBelgium I-BioStat Data Science InstituteHasselt UniversityHasseltBelgium Department of Materials University of OxfordParks RoadOX13PHOxfordUK Advanced Microscopy Laboratory Centre for Research on Adaptive Nanostructures and Nanodevices(CRANN)Dublin 2Ireland School of Physics Trinity College DublinThe University of DublinDublin 2Ireland

We introduce a Bayesian genetic algorithm for reconstructing atomic models of monotype crystalline nanoparticles from a single projection using Z-contrast *** number of atoms in a projected atomic column obtained from annular dark field scanning transmission electron microscopy images serves as an input for the initial three-dimensional *** algorithm minimizes the energy of the structure while utilizing a priori information about the finite precision of the atom-counting results and neighbor-mass *** results show promising prospects for obtaining reliable reconstructions of beam-sensitive nanoparticles during dynamical processes from images acquired with sufficiently low incident electron doses.

关键词： algorithm atomic utilizing

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Synthesis of tungsten ditelluride thin films and highly crystalline nanobelts from pre-deposited reactants

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Tungsten 2020年第3期2卷 321-334页

作者： John B.Mc Manus Cansu Ilhan Bastien Balsamo Clive Downing Conor P.Cullen Tanja Stimpel‑Lindner Graeme Cunningham Lisanne Peters lewys jones Daragh Mullarkey Igor V.Shvets Georg S.Duesberg Niall McEvoy School of Chemistry Trinity College DublinDublin 2 D02 PN40Ireland AMBER Centre CRANN InstituteTrinity College DublinDublin 2 D02 PN40Ireland SIGMA Clermont UniversitéClermont Auvergne63000 Clermont–FerrandFrance Institute of Physics EIT 2Faculty of Electrical Engineering and Information TechnologyUniversität der Bundeswehr München85579 NeubibergGermany School of Physics Trinity College DublinDublin 2 D02 PN40Ireland

Tungsten ditelluride(WTe_(2))is a layered transition metal dichalcogenide(TMD)that has attracted increasing research inter-est in recent ***_(2) has demonstrated large non-saturating magnetoresistance,potential for spintronic applications and promise as a type-II Weyl *** majority of works on WTe_(2) have relied on mechanically exfoliated flakes from chemical vapour transport(CVT)-grown crystals for their *** producing high-quality samples,this method is hindered by several disadvantages including long synthesis time,high-temperature annealing and an inherent lack of *** this work,a synthesis method is demonstrated that allows the production of large-area polycrystalline films of WTe_(2).This is achieved by the reaction of pre-deposited films of W and Te at a relatively low temperature of 550℃.Sputter X-ray photoelectron spectroscopy reveals the rapid but self-limiting nature of the oxidation of these WTe_(2) films in ambient *** WTe_(2) films are composed of areas of micrometre-sized nanobelts that can be isolated and offer potential as an alternative to CVT-grown *** nanobelts are highly crystalline with low defect densities indicated by transmission electron microscopy and show promising initial electrical results.

关键词： Two-dimensional materials Tungsten ditelluride Film conversion Electrodeposition Nanoelectronics

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