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Toward an understanding of dwell fatigue damage mechanism of bimodal Ti-6Al-4V alloys

Journal of Materials Science & Technology 2022年第13期108卷 244-255页

作者： l.R.Zeng l.M.lei x.M.luo G.P.Zhang Shenyang National laboratory for Materials Science Institute of Metal ResearchChinese Academy of SciencesShenyang 110016China School of Mechanical Engineering Chengdu UniversityChengdu 610106China AECC Shanghai Commercial Aircraft Engine Manufacturing Co. Ltd.Shanghai 201306China

Dwell fatigue effect is a long-standing problem threatening the long-term service reliability for fan blades and fan disks of an aircraft *** understand the basic mechanism of dwell fatigue damage,pure fatigue and 60 s dwell fatigue properties of bimodal Ti-6Al-4V alloys with different volume fractions of the primaryα(α_(p))phase were examined *** results showed that both pure fatigue and dwell fatigue life decreased with increasing the volume fraction of theα_(p)phase and the dwell fatigue life was lower than the pure fatigue *** quasi-in-situ test results and the quantitative characterization of damage behaviors of the local microstructure units defined by theα_(p)-secondaryα(α_(s))combination reveal that theα_(s)phase close to theα_(p)phase with extensively slip activities was gradually damaged under dwell fatigue loading,while that under pure fatigue loading was undamaged,demonstrating that the dwell loading induced the damage of theα_(s)phase,and further reduced the fatigue life.A stress relaxation-based model is proposed to describe the physical mechanism on dwell fatigue damage of the bimodal Ti-6Al-4V alloy,*** elastic deformation of theα_(s)phase caused by the strain incompatibility would be gradually transformed into plastic deformation during the dwell stage,and thus promotes fatigue *** model provides new insights into the microscopic process of stress/strain transfer between the soft and hard microstructure units under dwell fatigue loading.

关键词： Dwell effect Fatigue damage Stress relaxation Volume fraction of primaryαphase Quasi-in-situ testing

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PRIMARY STUDY FOR THE TECHNOlOGY OF ElECTROlESS PlATING Fe-Al-P AllOYS

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Acta Metallurgica Sinica(English letters) 1999年第5期12卷 733-735页

作者： l.l.Wang,l.H.Zhao,W.Y.Hu, x.l.Shu, x.J.Yuan, B.W.Zhang and x.Sheng Department of Applied Physics, Hunan University, Changsha 410082, China Hunan Univ Changsha China

Manuscript received 24 June 1999 The Fe Al P alloy deposits were plated on copper sheets by electroless plating. The change law of the deposition rate, composition, surface appearance and structure for the deposits was studied by changing the metallic salt ratios (AlCl 3/AlCl 3+FeSO 4), the concentration of metallic salt AlCl 3 and reductant NaH 2PO 2. The optimum plating bath was obtained. It was found that the choices of ligand and reductant were the key of increasing Al content for the deposits.

关键词： electroless Fe Al P plating Fe Al P alloys technology structure

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Achieving Reliable CoSb_(3) based thermoelectric joints with low contact resistivity using a high-entropy alloy diffusion barrier layer

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Journal of Materiomics 2022年第4期8卷 882-892页

作者： Z.Sun x.Chen Juncheng Zhang Huiyuan Geng l.x.Zhang State Key laboratory of Advanced Welding and Joining Harbin Institute of TechnologyHarbin150001China

Skutterudite(SKD)thermoelectric materials have high conversion efficiency,great mechanical proper-ties,and economical practicability in the medium temperature range(500e550C).They need to bejoined with metal electrodes to form a thermoelectric power generation device during ***,high contact resistivity,severe element diffusion,and large coefficient of thermal expansionmismatch are main obstacles for their *** address these issues,a FeCoNiCrMo high-entropyalloy diffusion barrier layer was designed and prepared using an arc smelting method in this *** heating temperatures on the microstructure and properties of the bonded joints were *** maximum shear strength was 21.6 Mpa and the corresponding reaction layer thickness,contactresistivity were 3.77 mm,1.8 mUcm2 respectively at 600C,40 MPa,10 *** strength dropped downto 18.8 MPa and the contact resistivity increased to 4.2 mU cm2 after aging for 640 *** modelwas established and it predicted that the contact resistivity would keep lower than 6.5 mU cm2(300 h,100 days)and 11 mU cm2(8760 h,1 year)and the reaction layer thickness would not exceed 25 mm(2400 h,100 days)and 45 mm(8760 h,1 year).

关键词： High-entropy diffusion barrier layer Skutterudite Diffusion bonding Microstructure Shear strength Contact resistivity

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Eutectic-reaction brazing of Al_(0.3)CoCrFeNi high-entropy alloys using Ni/Nb/Ni interlayers

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Journal of Materials Science & Technology 2022年第26期121卷 245-255页

作者： Y.lei J.Sun x.G.Song M.x.Yang T.l.Yang J.Yin State Key laboratory of Advanced Welding and Joining Harbin Institute of TechnologyHarbin 150001China Beijing Power Machinery Institute Beijing 100074China Sichuan Aerospace Changzheng Equipment Manufacturing Co. Ltd.Chengdu 610100China

In this study,a novel eutectic-reaction brazing of Al_(0.3)CoCrFeNi high-entropy alloys(HEAs)^(1)was investigated with a design of laminated Ni/Nb/Ni *** typical Al_(0.3)CoCrFeNi brazing seam consisted of proeutecticγ,the lamellar eutectic structure composed of face-centered cubic(FCC)phase(eutecticγ)and C14 laves,as well as a few amounts of Nb based solid solution.A high density of nanoscale ordered l1_(2)(γ)phase was precipitated withinγphase *** the brazing temperature raised from 1200 to 1320℃,the dissolution volume of Al_(0.3)CoCrFeNi alloy into Ni-Nb liquid was *** microstructure of the brazing seam changed from hypereutectic(blocky laves+γphase)to eutectic(laves+eutecticγ)to hypoeutectic structures(proeutecticγ+laves/γeutectic structure).The shear strength of joints was increased gradually due to the formation of eutectic lamellae and the cellular growth of proeutecticγ*** maximum shear strength of the joint brazed at 1320℃for 10 min was up to 592 MPa,reaching 95%of the base *** joint mainly ruptured in the soft proeutecticγphase in a ductile fracture mode.

关键词： High-entropy alloys Brazing Eutectic structure Shear strength

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Effect of Mo Addition on Microstructural Characteristics in a Re-containing Single Crystal Superalloy

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Journal of Materials Science & Technology 2015年第2期31卷 143-147页

作者： x.G.liu l.Wang l.H.lou J.Zhang Superalloys Division Institute of Metal ResearchChinese Academy of Sciences Shenyang National laboratory for Materials Science Institute of Metal ResearchChinese Academy of Sciences

The effect of Mo addition on microstructural characteristics of a nickel-base single crystal superalloy containing 4 wt% Re was investigated. The γ/γ’ partitioning ratios determined by energy dispersive spectrometer attached to a transmission electron microscope showed that the addition of Mo enhanced the partitioning of Re,W and Cr in the g matrix while decreased the concentration of Ta in the matrix. Synchrotron radiation diffraction was adopted to measure the γ/γ’ lattice misfit at room temperature. The results indicated that Mo addition changed the γ/γ’ lattice misfit towards larger negative as well as increased the tetragonal distortion of the γ lattice. Additionally,Mo addition led to microstructural instability and altered the precipitation behavior of topologically close-packed phases during 1100 C exposure. Instead of precipitating directly from the matrix,the μ phase was observed to be converted from the α phase which precipitated preferentially as a metastable intermediate in the alloy with high Mo content.

关键词： Superalloy Molybdenum Microstructure Partitioning

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Gelation capability of cysteine-modified cyclo(l-lys-l-lys)s dominated by Fmoc and Trt protecting groups

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Science China Chemistry 2016年第3期59卷 293-302页

作者： Huimin Geng Qianying Zong Jie you lin Ye Aiying Zhang Ziqiang Shao Zengguo Feng School of Materials Science and Engineering Beijing Institute of Technology

A series of symmetrical peptidomimetics （3-8） based on cysteine-modified cyclo（l-lys-l-lys）s were synthesized, and their gelation capability in organic solvents was dominated by fluorenylmethyloxycarbonyl （Fmoc） and triphenylmethyl （Trt） protecting groups and the exchange of thiol-to-disulfide as well. The peptidomimetics holding Trt （3 and 4） showed no gel performance, while the Fmoc groups promoted 5 and 6 to give rise to thermo-reversible organogels in a number of organic solvents. The self-assembled fibrillar networks were distinctly evidenced in the organogels by transmission electron micros- copy （TEM） and scanning electron microscopy （SEM） observations. Fourier transform infrared spectroscopy （FT-IR） and fluorescence analyses revealed that the hydrogen bonding and ^-rt stacking play as major driving forces for the self-assembly of these organogelators. A 13-turn secondary structure was deduced for the organogel of 6 by virtue of x-ray diffraction, FT-IR and circular dichroism （CD） measurements, and an interdigitated bilayer structure was also presented.

关键词： organogel cyclic dipeptide self-assembly cysteine β-turn

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Force and impulse multi-sensor based on flexible gate dielectric field effect transistor

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International Journal of Minerals,Metallurgy and Materials 2025年第1期32卷 214-220页

作者： Chao Tan Junling lü Chunchi Zhang Dong liang lei Yang Zegao Wang College of Materials Science and Engineering Sichuan UniversityChengdu 610065China The 54th Research Institute of China Electronics Technology Group Corporation Shijiazhuang 050081China

Nowadays,force sensors play an important role in industrial production,electronic information,medical health,and many other ***-dimensional material-based filed effect transistor(2D-FET)sensors are competitive with nano-level size,lower power consumption,and accurate ***,few of them has the capability of impulse detection which is a path function,expressing the cumulative effect of the force on the particle over a period of *** we fabricated the flexible polymethyl methacrylate(PMMA)gate dielectric MoS_(2)-FET for force and impulse sensor *** systematically investigated the responses of the sensor to constant force and varying forces,and achieved the conversion factors of the drain current signals(I_(ds))to the detected impulse(I).The applied force was detected and recorded by I_(ds)with a low power consumption of~30 *** sensitivity of the device can reach~8000%and the 4×1 sensor array is able to detect and locate the normal force applied on ***,there was almost no performance loss for the device as left in the air for two months.

关键词： flexible gate dielectric transistor force sensor impulse sensor force sensor array

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CRYSTAllOGRAPHIC ANAlYSIS OF THE lATH MARTENSITE TRANSFORMATION IN Fe-Ni-Mn AllOY

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Acta Metallurgica Sinica(English letters) 2004年第6期17卷 862-869页

作者： x.P.lin Y.Dong x.M.Cao Y.Zhang N.J.Gu x.l.Ma DepartmentofMaterialsScienceandTechnology HebeiUniversityofTechnologyTianjin300130ChinaManuscriptreceived18November2003 inrevisedform1June2004

Habit plane rotation of lath martensite transformation in Fe-Ni-Mn alloy was predicted by means of Displacement Vector Theory. Its surface relief effect was observed and a math model for the quantitative analysis of habit plane rotation of lath martensite transformation was established by means of atomic force microscopy (AFM). The experiment showed that the largest rotation of habit plane of lath martensite transformation predicted by means of Displacement Vector Theory is 13.50°, and it's incompatible with the concept of invariant plane strain (IPS); surface relief of lath martensite revealed no character of IPS, i.e. it exhibited irregular 'N'-shaped 'surface relief packet', and 'surface relief packet' was composed of layers of several small surface reliefs, the AFM quantitative analysis of habit plane rotation of lath martensite transformation was 11.11°, which was in agreement with the prediction of Displacement Vector Theory (13.50°) and it firmly confirmed the habit plane rotation of lath martensite transformation and the correctness of Displacement Vector Theory.

关键词： atomic force microscope (AFM) surface relief invariant plane strain (IPS) relief angle shear angle

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Viscosity and structure relationship with equimolar substitution of CaO with MgO in the CaO–MgO–Al_(2)O_(3)–SiO_(2)slag melts

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International Journal of Minerals,Metallurgy and Materials 2025年第1期32卷 70-79页

作者： Yong Hou Shuo Zhang Jie Dang Jia Guo Hanghang Zhou xuewei lü College of Materials Science and Engineering Chongqing UniversityChongqing 400044China Chongqing Key laboratory of Vanadium-Titanium Metallurgy and New Materials Chongqing UniversityChongqing 400044China

Currently,the Al_(2)O_(3)content in the high-alumina slag systems within blast furnaces is generally limited to 16wt%–18.5wt%,making it challenging to overcome this *** most studies that concentrated on managing the MgO/Al_(2)O_(3)ratio or basicity,this paper explored the effect of equimolar substitution of MgO for CaO on the viscosity and structure of a high-alumina CaO-MgO-Al_(2)O_(3)-SiO_(2)slag system,providing theoretical guidance and data to facilitate the application of high-alumina *** results revealed that the viscosity first decreased and then increased with higher MgO substitution,reaching a minimum at 15mol%MgO *** transform infrared spectroscopy(FTIR)results found that the depths of the troughs representing[SiO_(4)]tetrahedra,[AlO_(4)]tetrahedra,and Si-O-Al bending became progressively deeper with increased MgO *** of the Raman spectra showed that the average number of bridging oxygens per Si atom and the x_(Q^(3))/x_(Q^(2))(x_(Q^(i))is the molar fraction of Q^(i) unit,and i is the number of bridging oxygens in a[SiO_(4)]tetrahedral unit)ratio increased from 2.30 and 1.02 to 2.52 and 2.14,respectively,indicating a progressive polymerization of the silicate structure.x-ray photoelectron spectroscopy(xPS)results highlighted that non-bridging oxygen content decreased from 77.97mol% to 63.41mol% with increasing MgO concentration,whereas bridging oxygen and free oxygen contents *** analysis demonstrated a gradual increase in the polymerization degree of the tetrahedral structure with the increase in MgO ***,bond strength is another important factor affecting the slag *** occurrence of a viscosity minimum can be attributed to the complex evolution of bond strengths of non-bridging oxygens generated during depolymerization of the[SiO_(4)]and[AlO_(4)]tetrahedral structures by CaO and MgO.

关键词： aluminosilicate viscosity structure spectroscopy

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The evolution of Epstein-Barr virus detection in nasopharyngeal carcinoma

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Cancer Biology & Medicine 2018年第1期15卷 1-5页

作者： you Quan li Ni Sann Khin Melvin l.K.Chua Division of Radiation Oncology National Cancer Center Oncology Academic Clinical Program Duke-NUS Medical School

The detection of Epstein-Barr virus(EBV)in nasopharyngeal carcinoma(NPC)has evolved over the last40 years,transitioning from simple serological tests of latent viral infection to extremely sensitive measurements of

关键词：乳头状瘤病毒癌症临床症状进化鼻 EBV 实用程序 DNA

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