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Geochemical characteristics of Carboniferous volcanic rocks from the Wulungu-Luliang area, Junggar basin: constraints on magma source and tectonic setting

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Chinese Journal Of Geochemistry 2015年第4期34卷 515-524页

作者： Wei Liu kuihua zhang Guanlong zhang Peiming Zhou Qizhi Wang School of Resources and Geosciences China University of Mining and Technology The West Research Center Company of Sinopec Shengli Oilfield

The Carboniferous volcanic rocks in the Wulungu-Luliang area are mainly andesites of medium- to high-K calc-alkalic series. Volcanic rock samples have relatively high alkali(Na2O + K2 O = 4.7 % to 6.8 %) and low Ti O2contents(0.7 % to 0.9 %), relatively high Mg O(2.5 % to 3.4 %) and Mg#(49.9 % to 67.1 %), high rare earth element(REE) contents, and relatively high K2 O contents(1.7 % to 3.1 %). Chondrite-normalized REE patterns show light REE enrichment((La/Yb)N= 4.15 to 5.19)with weak Eu anomalies(d Eu = 0.75 to 0.92). These samples are enriched in large-ion lithophile elements but relatively depleted in high field strength elements. The trace elements and REE patterns are similar to those of Setouchi and central Ryukyu high-Mg andesites, indicating a highMg andesite source. Relatively high Y contents(16.7 to24.4 ppm), and relatively low Sr/Y ratios(17.2 to 38.8) and Ti O2contents(0.7 % to 0.9 %) exclude the possibility of slab melting. Low Sr/Nd(16.6 to 42.8), Ba/Th(66.4 to266.8), and U/Th(0.2 to 0.3) indicate that the influence of slab-derived fluids is low. The ratios of Ce/Th(4.9–7.3), Ce/Pb(1.8–4.2), Ba/Rb(7.99–22.03), Ba/Th(66.4–266.8), and La/Sm(3.6–4.3) are similar to ratios found in subducting sediment melts. Relatively high ratios of K/Nb(1357–3258),Th/La(0.28–0.42), Zr/Nb(8.8–27.1), and especially Th/Nb(0.48–1.25) suggest that the magma was assimilated and contaminated by upper continental crust. These characteristics, along with the ratios of La/Yb, Sc/Ni, Th/Yb, Ta/Yb,Ce/P2O5, and Zr/Ti O2, demonstrate that the earlier Carboniferous volcanic rocks in the Wulungu-Luliang area were generated in a continental island-arc setting.

关键词：火山岩地球化学特征石炭系岩浆源准噶尔盆地构造背景古陆高钾钙碱性系列

Multi-porous electroactive poly(L-lactic acid)/ polypyrrole composite micro/nano fibrous scaffolds promote neurite outgrowth in PC12 cells

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Neural Regeneration Research 2013年第1期8卷 31-38页

作者： Qiaozhen Yu Shuiling Xu kuihua zhang Yongming Shan College of Materials and Textile Engineering Jiaxing Key Laboratory of Modern Textile and Garment Jiaxing University College of Medicine Jiaxing University College of Mathematics Physics and Information Engineering Jiaxing University

In this study, poly（L-lactic acid）/ammonium persulfate doped-polypyrrole composite fibrous scaffolds with moderate conductivity were produced by combining electrospinning with in situ polymerization. PC12 cells were cultured on these fibrous scaffolds and their growth following electrical stimulation （0-20.0 μA stimulus intensity, for 1-4 days） was observed using inverted light microscopy, and scanning electron microscopy coupled with the MTT cell viability test. The results demonstrated that the poly（L-lactic acid）/ammonium persulfate doped-polypyrrole fibrous scaffold was a dual multi-porous micro/nano fibrous scaffold. An electrical stimulation with a current intensity 5.0- 10.0 μAfor about 2 days enhanced neuronal growth and neurite outgrowth, while a high current intensity （over 15.0 μA） suppressed them. These results indicate that electrical stimulation with a moderate current intensity for an optimum time frame can promote neuronal growth and neurite outgrowth in an intensity- and time-dependent manner.

关键词： neural regeneration tissue engineering poly(L-lactic acid)/polypyrrole composite multi-porousfibrous scaffold electrical stimulation PC12 cell lines axon electric spinning grants-supportedpaper photographs-containing paper neuroregeneration

准噶尔盆地哈山地区石炭系二叠系火山岩储层发育机制研究

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地学前缘 2024年第2期31卷 327-342页

作者：周健林承焰刘惠民张奎华张关龙王千军于洪洲倪胜利牛花朋焦小芹刘姗中国石油化工股份有限公司胜利油田分公司勘探开发研究院山东东营257000 中国石油化工股份有限公司胜利油田分公司山东东营257000 中国石油大学(华东)地球科学与技术学院山东青岛266580 中国石油大学(北京)地球科学学院北京102249

哈山地区位于准噶尔盆地西北缘,形成于陆缘岛弧背景之下,其石炭系二叠系火山岩储层是油气藏勘探的重点领域。为进一步明确哈山地区石炭系二叠系火山岩储层的勘探前景,在岩心、薄片鉴定基础上,综合扫描电镜、微米CT、流体包裹体等技术方... 详细信息

哈山地区位于准噶尔盆地西北缘,形成于陆缘岛弧背景之下,其石炭系二叠系火山岩储层是油气藏勘探的重点领域。为进一步明确哈山地区石炭系二叠系火山岩储层的勘探前景,在岩心、薄片鉴定基础上,综合扫描电镜、微米CT、流体包裹体等技术方法,结合储层物性参数、主微量元素分析结果,对该区石炭系二叠系火山岩储层发育机制展开系统研究。结果表明:(1)哈山地区火山岩储集空间类型主要为溶蚀孔、粒间孔和溶蚀缝,孔隙直径大且连通性较好,但非均质性较强;(2)火山岩岩相、裂缝、风化淋滤和深部热液流体是影响火山岩储层物性的关键因素——溢流相和爆发相是有利储层发育相带,构造抬升和逆冲推覆使推覆体前翼、断层交汇处储层物性更优质,风化淋滤又进一步改善了储层;(3)基于物性岩相储集空间联合分析,将哈山地区火山岩储层划分为3类,其中优质储层主要位于逆冲推覆带的“三角”地带。结论认为,哈山地区石炭系二叠系火山山岩具备发育大规模优质储层的条件,展现出巨大的油气勘探开发潜力。

关键词：火山岩储集空间储集物性形成机制哈山地区

中国东西部陆相页岩油地质特征差异性分析及其对富集规律影响——以胜利探区为例

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油气地质与采收率 2024年第4期31卷 42-59页

作者：张奎华王越于洪洲周健汪誉新宋梅远倪胜利中国石化胜利油田分公司山东东营257000 中国石化胜利油田分公司勘探开发研究院山东东营257015

以胜利探区为例,系统对比研究了中国东西部陆相湖盆页岩油地质特征差异性及其对富集规律的影响。济阳坳陷沙四段上亚段—沙三段下亚段在古地貌、古气候、古水体介质等因素共同控制下,富有机质纹层状碳酸盐页岩大规模分布,富有机质黏土... 详细信息

以胜利探区为例,系统对比研究了中国东西部陆相湖盆页岩油地质特征差异性及其对富集规律的影响。济阳坳陷沙四段上亚段—沙三段下亚段在古地貌、古气候、古水体介质等因素共同控制下,富有机质纹层状碳酸盐页岩大规模分布,富有机质黏土纹层成烃与富碳酸盐纹层成储协同演化为游离烃规模富集提供了有利条件。准噶尔盆地西北缘哈山地区风城组强裂陷作用导致强烈火山活动,在火山喷发物质与古气候共同影响下,富有机质纹层状含碱长英页岩相大规模分布,且成烃成储演化过程中形成较多的长英质矿物,并伴生大量的基质溶蚀孔和晶间孔,为页岩油富集奠定了重要基础。哈山地区在多期逆冲推覆过程中,准原地系统持续生烃、油多气少和相对较好的保存条件以及构造覆压、生烃增压作用产生的异常高压为页岩油高产提供了必要条件。准噶尔盆地东南缘(准东南)芦草沟组在海迹湖咸水环境下,受火山凝灰质与微生物作用影响,形成了富有机质纹层状页岩相夹贫有机质层状白云岩相的主要岩相组合类型。博格达山周缘山前构造带芦草沟组富有机质页岩均进入成熟演化阶段,胜利探区构造相对稳定区具备页岩油勘探前景。

关键词：陆相页岩油页岩岩相富集规律济阳坳陷哈山地区准东南地区

Petroleum in the Jurassic Reservoirs within the Eastern Fukang Sub-depression,Junggar Basin,NW China:Correlation and Source Rock

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Acta Geologica Sinica(English Edition) 2023年第3期97卷 777-795页

作者： CHENG Bin LIU Hua zhang kuihua REN Xincheng MENG Xiangyu LIU Dezhi Shandong Provincial Key Laboratory of Deep Oil and Gas China University of Petroleum(East China)QingdaoShandong 266580China Shandong Provincial Key Laboratory of Reservoir Geology China University of Petroleum(East China)QingdaoShandong 266580China Laboratory for Marine Mineral Resources Qingdao National Laboratory for Marine Science and TechnologyQingdaoShandong 266071China Sinopec Shengli Oilfield Company DongyingShandong 257000China

The origin and source of the petroleum in the Jurassic reservoirs within the eastern Fukang sub-depression were geochemically *** show thermal maturities matching the peak generation stage,while the condensates are at the early stage of intense *** and condensates may have experienced mild evaporative fractionation,while mixing of severely biodegraded with non-biodegraded oils has *** biomarkers and isotopes,petroleums were classified into GroupⅠ,ⅡandⅢgenetic groups,with GroupⅢfurther divided intoⅢa andⅢb ***Ⅰpetroleum displays heavy carbon isotopes,a strong predominance of pristine over phytane,high C_(19)and C_(20)tricyclic and C_(24)tetracyclic terpanes,low gammacerane,and dominant C_(29)steranes,while GroupⅡshows light carbon isotopes,a predominance of phytane over pristine,high C_(21)and C_(23)tricyclic with low C_(24)tetracyclic terpanes,high gammacerane and dominant C_(27)***Ⅲa petroleum shows mixing compositions of GroupⅠandⅡ,while GroupⅢb displays similar compositions to Group I,but with significantly higher Ts,C_(29)Ts and C_(30)diahopane ***-source rock correlation suggests GroupⅠandⅡpetroleums originate from Jurassic and Permian source rocks,respectively,while GroupⅢa are mixtures sourced from these rocks andⅢb are mixtures from Jurassic and Triassic source rocks.

关键词： biomarkers oil-source rock correlation Jurassic reservoirs Fukang sub-depression Junggar Basin

后道拉伸对聚丁二酸丁二醇酯/丝胶蛋白共混纤维结构与性能的影响

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蚕业科学 2024年第1期50卷 23-33页

作者：夏榆姚勇波姚菊明生俊露张葵花蒋毅张军峰浙江理工大学材料科学与工程学院杭州310018 嘉兴大学浙江省纱线材料成形与复合加工技术研究重点实验室浙江嘉兴314001 嘉兴市第一医院浙江嘉兴314001 禾欣可乐丽超纤皮(嘉兴)有限公司浙江嘉兴314003

为提高纤维的力学性能,采用后道拉伸处理聚丁二酸丁二醇酯(poly(butylene succinate),PBS)/丝胶蛋白(silk sericin,SS)共混纤维,研究拉伸倍数和拉伸温度对纤维形态结构、化学结构、热性能、力学性能与降解性能的影响。结果表明,随着拉... 详细信息

为提高纤维的力学性能,采用后道拉伸处理聚丁二酸丁二醇酯(poly(butylene succinate),PBS)/丝胶蛋白(silk sericin,SS)共混纤维,研究拉伸倍数和拉伸温度对纤维形态结构、化学结构、热性能、力学性能与降解性能的影响。结果表明,随着拉伸倍数增加,PBS与丝胶蛋白发生相对位移,纤维表面沿拉伸方向出现明显条纹;随着拉伸温度增加,纤维表面的条纹减少,表明温度的增加提高了PBS分子链的运动能力,使纤维保持致密结构。随着拉伸倍数和拉伸温度的提高,共混纤维的力学性能和结晶度呈现先增加后减小的趋势,在后道拉伸倍数为4倍,拉伸温度为75℃时,纤维的结晶度可达61.30%,此条件下的纤维断裂强度最大为2.0 cN/dtex,接近粘胶纤维的力学强度,可满足纺纱、非织造等纺织加工工艺的要求。

关键词：聚丁二酸丁二醇酯丝胶蛋白共混纤维拉伸倍数拉伸温度

准噶尔盆地西北缘哈山地区风城组碱湖页岩油地质特征与勘探展望

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古地理学报 2024年第5期26卷 1017-1036页

作者：刘惠民文华国张奎华郭佩张关龙于洪洲熊伟周健徐文礼宋梅远李长志中国石油化工股份有限公司胜利油田分公司山东东营257001 成都理工大学自然资源部深时地理环境重建与应用重点实验室四川成都610059 成都理工大学油气藏地质及开发工程全国重点实验室四川成都610059 中国石油化工股份有限公司胜利油田分公司勘探开发研究院山东东营257015

玛湖凹陷二叠系风城组是准噶尔盆地近年来页岩油勘探开发和增储上产的重点层位。哈拉阿拉特山地区(简称哈山地区)位于玛湖凹陷北缘,由于位于逆冲带附近且处于勘探早期,该区风城组的沉积背景、古地理位置及页岩油勘探潜力尚不明确。根据... 详细信息

玛湖凹陷二叠系风城组是准噶尔盆地近年来页岩油勘探开发和增储上产的重点层位。哈拉阿拉特山地区(简称哈山地区)位于玛湖凹陷北缘,由于位于逆冲带附近且处于勘探早期,该区风城组的沉积背景、古地理位置及页岩油勘探潜力尚不明确。根据哈山地区风城组页岩油近10年的勘探开发基础资料和成果,系统梳理了该区页岩的沉积环境、岩相划分、源岩品质、含油性和储集性,探讨了哈山地区页岩油的“甜点”发育规律和勘探前景。结果表明:玛湖主体洼陷之外,哈山地区中部风城组发育另一个碱湖沉积沉降中心,其火山喷发、沉积演化和成碱阶段与南部乌夏地区具有很好的可比性,为风城组另一富烃凹陷;提出了风城组碱湖页岩四端元对三角页岩划分方案,将风城组页岩划分为含盐和非含盐8种页岩岩相;整体上,哈山地区风城组黏土质页岩和钙质页岩有机质丰度最高,云质页岩和盐质页岩含油性相对较好,云质页岩和粉砂岩储集性最好,提出了云质页岩为I类甜点,粉砂岩为Ⅱ类甜点。哈山地区风城组页岩在源岩和储集层品质方面与乌夏地区风城组相当,具有较好的页岩油勘探前景。

关键词：碱湖逆冲带页岩岩相划分富烃凹陷页岩甜点风城组准噶尔盆地

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Fabrication of glycidyl methacrylate-modified silk fibroin/poly(L-lactic acid-co-ε-caprolactone)-polyethylene glycol diacrylate hybrid 3D nanofibrous scaffolds for tissue engineering

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Frontiers of Materials Science 2023年第2期17卷 79-91页

作者： Yongyong Fan Anlin Yin Yunhuan Li Qi Gu Yan Zhou Junlong Zhou Ruibo Zhao kuihua zhang Institute of Smart Biomaterials School of Materials Science and Engineering and Zhejiang-Mauritius Joint Research Center for Biomaterials and Tissue EngineeringZhejiang Sci-Tech UniversityHangzhou 310018China College of Materials and Textile Engineering Nanotechnology Research InstituteJiaxing UniversityJiaxing 314001China

In order to provide a biomimetic natural extracellular matrix microenvironment with excellent mechanical capacity for tissue regeneration,a novel porous hybrid glycidyl methacrylate-modified silk fibroin/poly(L-lactic acid-co-ε-caprolactone)–polyethylene glycol diacrylate(SFMA/P(LLA-CL)–PEGDA)hybrid three-dimensional(3D)nanofibrous scaffolds was successfully fabricated through the combination of 3D nanofibrous platforms and divinyl PEGDA based photocrosslinking,and then further improved water resistance by ethanol vapor *** electron microscopy and micro-computed tomography results demonstrated significant PEGDA hydrogel-like matrices bonded nanofibers,which formed a 3D structure similar to that of“steel bar(nanofibers)‒cement(PEGDA)”,with proper pore size,high porosity,and high pore connectivity ***,the hybrid 3D nanofibrous scaffolds showed outstanding swelling properties as well as improved compressive and tensile ***,these hybrid 3D nanofibrous scaffolds could provide a biocompatible microenvironment,capable of inducing the material‒cell hybrid and regulating human umbilical vein endothelial cells *** thus present significant potential in tissue regeneration.

关键词： hybrid 3D nanofibrous scaffold silk fibroin tissue engineering human umbilical vein endothelial cell

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济阳陆相断陷盆地页岩油研究进展

油气地质与采收率 2024年第4期31卷 60-72页

作者：李军亮刘惠民王勇张奎华周广清李政王伟庆方正伟张顺刘鑫金刘鹏张子麟魏晓亮中国石化胜利油田分公司勘探开发研究院山东东营257015 页岩油气富集机理与高效开发全国重点实验室山东东营257015 中国石化胜利油田分公司山东东营257000 中国石化胜利油田分公司油气勘探管理中心山东东营257000 中国石化胜利油田分公司石油工程技术研究院山东东营257200

济阳陆相断陷盆地页岩油是现实的资源接替新领域,具有巨大勘探潜力,是胜利油田可持续发展的重要资源基础。结合近年来济阳陆相断陷盆地页岩油地质研究与勘探成效,系统梳理了济阳陆相断陷盆地页岩沉积、成储、成烃及页岩油富集理论认识... 详细信息

济阳陆相断陷盆地页岩油是现实的资源接替新领域,具有巨大勘探潜力,是胜利油田可持续发展的重要资源基础。结合近年来济阳陆相断陷盆地页岩油地质研究与勘探成效,系统梳理了济阳陆相断陷盆地页岩沉积、成储、成烃及页岩油富集理论认识、配套增产压裂技术等方面的新进展。研究表明:①提出了基于矿物组成、沉积构造、结晶程度和有机质丰度的“四要素三端元”页岩岩相划分方案,揭示了“四古控相”机制,明确了页岩岩相呈“环带状”有序分布。②集成岩心微纳米CT扫描、氩离子抛光扫描电镜、FIB-FESEM、核磁共振冻融、X射线小角散射等页岩多尺度孔缝系统量化表征技术,明确了济阳陆相断陷盆地页岩储集空间孔缝兼顾,以无机孔缝为主,揭示了方解石重结晶、溶蚀作用和伊/蒙混层向伊利石转化作用是最为主要的成储机制,构建了页岩孔缝网络储集模型。③研发了富有机质页岩含油率评价方法,揭示了咸化湖盆富有机质页岩古生产力高、早生、早富特点,初步估算济阳陆相断陷盆地页岩油资源量超过1010t。④纹层/层状页岩岩相成烃、成储时空耦合控制了页岩油富集,表现为“咸化源岩早生、无机孔缝储集、微观源储一体、二元耦合富集”模式。⑤创建了陆相断陷盆地页岩油勘探“四性”“四定”综合评价体系及目标优选流程。⑥研发了适合济阳陆相断陷盆地页岩的“组合缝网压裂”“水平井多级分段”增产压裂技术。结合胜利油田实际情况,确立了“主力洼陷增储上产、富油小洼陷探索新阵地、外围小洼陷落实资源、兼顾优化矿权”的勘探思路,有序推进济阳陆相断陷盆地页岩油规模增储建产,相关成果认识与配套技术对同类油田的页岩油勘探开发具有一定的借鉴和参考意义。

关键词：断陷盆地页岩油岩相成储机制游离油综合评价体系组合缝网压裂