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Microstructural evolution and deformation behavior of friction stir welded twin-induced plasticity steel

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Journal of Materials Science & Technology 2024年第2期169卷 68-81页

作者： Ke Qiao kuaishe wang Jia wang Zhengyang Hao Yating Xiang Peng Han Jun Cai Qi Yang Wen wang School of Metallurgical Engineering National and Local Joint Engineering Research Center for Functional Materials ProcessingXi’an University of Architecture and TechnologyXi’an 710055China Shanghai Research Institute of Materials Shanghai 200437China

The weldability of twin-induced plasticity(TWIP)steel with ultra-high strength via friction stir welding(FSW)technique was investigated,and microstructural evolution and deformation behavior of whole and micro-zones of FSW TWIP joint were studied for the first *** results showed that the content of recrystallized grains in the stir zone(SZ)increased from 10.5%of basal material(BM)to 14.2%,and that of heat affected zone(HAZ)increased to 78.6%.The percentage of annealing twins decreased from 26.8%in BM to 11%in SZ,while increased to 35%in *** with the BM,the ultimate tensile strength and yield strength of the FSW joint increased to 1036 and 550 MPa,respectively,reaching 106.7%and 110.9%of BM,*** elongation of the entire joint was 50.5%,which was lower than that of BM due to the nonuniform deformation during the tensile *** engineering strain was mainly concentrated in BM and SZ and transferred to each other during the tensile test,while the engineering strain in HAZ was always the ***,the tensile fracture occurred in the *** order of ultimate tensile strength of micro-zones in the FSW joint was as follows:HAZ>BM≈*** order of yield strength was as follows:HAZ>BM>SZ.

关键词： Twin-induced plasticity steel Friction stir welding Microstructure Mechanical property Deformation behavior

A new insight into LPSO phase transformation and mechanical properties uniformity of large-scale Mg-Gd-Y-Zn-Zr alloy prepared by multi-pass friction stir processing

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Journal of Magnesium and Alloys 2024年第5期12卷 2041-2056页

作者： Xiaohu Guan Wen wang Ting Zhang Pai Peng Qiang Liu Peng Han Ke Qiao Jun Cai Liqiang wang kuaishe wang School of Metallurgical Engineering National and Local Joint Engineering Research Center for Functional Materials Processing Xi'an University of Architecture and Technology Xi'an Rare Metal Materials Institute Co.Ltd State Key Laboratory of Metal Matrix Composites School of Material Science and Engineering Shanghai Jiao Tong University

A large-scale fine-grained Mg-Gd-Y-Zn-Zr alloy plate with high strength and ductility was successfully prepared by multi-pass friction stir processing(MFSP) technology in this work. The structure of grains and long period stacking ordered(LPSO) phase were characterized,and the mechanical properties uniformity was investigated. Moreover, a quantitative relationship between the microstructure and tensile yield strength was established. The results showed that the grains in the processed zone(PZ) and interfacial zone(IZ) were refined from 50 μm to 3 μm and 4 μm, respectively, and numerous original LPSO phases were broken. In IZ, some block-shaped 18R LPSO phases were transformed into needle-like 14H LPSO phases due to stacking faults and the short-range diffusion of solute atoms. The severe shear deformation in the form of kinetic energy caused profuse stacking fault to be generated and move rapidly, greatly increasing the transformation rate of LPSO phase. After MFSP, the ultimate tensile strength, yield strength and elongation to failure of the large-scale plate were 367 MPa, 305 MPa and 18.0% respectively. Grain refinement and LPSO phase strengthening were the major strengthening mechanisms for the MFSP *** particularly, the strength of IZ was comparable to that of PZ because the strength contribution of the 14H LPSO phase offsets the lack of grain refinement strengthening in IZ. This result opposes the widely accepted notion that IZ is a weak region in MFSP-prepared large-scale fine-grained plate.

关键词： Friction stir processing Multi-pass Mg-Gd-Y-Zn-Zr alloy LPSO phase transformation Mechanical properties

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离心干燥制备含镧钼酸铵的焙解机制

稀有金属材料与工程 2024年第5期53卷 1349-1354页

作者：张晓王快社牛帅任宝江刘旭洋西安建筑科技大学冶金工程学院陕西西安710055 西安建筑科技大学功能材料加工国家与地方联合工程研究中心陕西西安710055 金堆城钼业股份有限公司陕西西安710077 陕西省“四主体一联合”先进钼化合物功能材料校企联合研究中心陕西西安710077

本实验采用离心干燥法,含镧钼酸铵为原料,将其焙解为含镧三氧化钼。通过XRD和TG-MS对含镧钼酸铵在空气中的热分解过程进行了分析,并研究了不同焙解温度制备含镧三氧化钼的形貌及理化性能。结果表明,含镧钼酸铵为非晶态、中空近球形颗粒... 详细信息

本实验采用离心干燥法,含镧钼酸铵为原料,将其焙解为含镧三氧化钼。通过XRD和TG-MS对含镧钼酸铵在空气中的热分解过程进行了分析,并研究了不同焙解温度制备含镧三氧化钼的形貌及理化性能。结果表明,含镧钼酸铵为非晶态、中空近球形颗粒,在热分解过程中经历了3个阶段:室温至196.5℃,离心干燥粉发生从非晶态到晶态的转变;196.5~337.8℃,铵根离子完全分解,有亚稳态h-MoO_(3)生成;337.8~410.1℃,h-MoO_(3)发生相变生成α-MoO_(3)。含镧三氧化钼“遗传”了离心干燥粉形貌,为近球形,随着焙解温度升高,颗粒表面越粗糙,破碎颗粒增多,内部小颗粒由不规则的粘结颗粒向规则的片状转变。焙解温度对含镧三氧化钼杂质元素含量影响不大,但随着温度升高,含镧三氧化钼的粒度和松装密度稍有减小。

关键词：含镧钼酸铵焙解离心干燥

C70600白铜空心锭立式连铸工艺参数对凝固过程的影响

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机械科学与技术 2024年第1期43卷 64-72页

作者：蔡军杨清相乔柯王文王快社西安建筑科技大学冶金工程学院西安710055 国家联合地方功能材料加工中心西安710055

为了获得Ф260×Ф80 C70600白铜空心锭立式连铸合理的工艺参数,通过数值模拟定量分析了各种工艺参数对温度场和应力场的影响。结果表明:浇铸温度每提高20℃,液穴深度增加10 mm;拉坯速度每提高10 mm/min,液穴深度增加20 mm;液穴深度随... 详细信息

为了获得Ф260×Ф80 C70600白铜空心锭立式连铸合理的工艺参数,通过数值模拟定量分析了各种工艺参数对温度场和应力场的影响。结果表明:浇铸温度每提高20℃,液穴深度增加10 mm;拉坯速度每提高10 mm/min,液穴深度增加20 mm;液穴深度随着石墨芯管冷却强度的增大而减小。基于正交试验和方差分析发现,F_(A)>F_(0.01)(3,3),F_(B)>F_(D)>F_(0.1)(3,3),F_(C)

关键词：立式连铸工艺参数空心锭液穴深度应力场数值模拟

黑磷烯量子点作为水基润滑添加剂的摩擦学性能研究

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机械工程学报 2024年第3期60卷 226-237页

作者：王伟魏春艳屈怡珅董少文吕凡凡金杰王快社西安建筑科技大学冶金工程学院西安710055 北京交通大学经济管理学院北京100040 北京交通大学机械与电子控制工程学院北京100040

为了提高钛合金加工的表面质量,降低其加工成本。利用具有高承载、低摩擦等特性的黑磷烯量子点作为钛合金加工液的高效润滑介质。采用MS-T3001摩擦磨损试验机,以GCr15轴承钢/TC4钛合金盘为摩擦副研究黑磷烯量子点作为水基润滑添加剂的... 详细信息

为了提高钛合金加工的表面质量,降低其加工成本。利用具有高承载、低摩擦等特性的黑磷烯量子点作为钛合金加工液的高效润滑介质。采用MS-T3001摩擦磨损试验机,以GCr15轴承钢/TC4钛合金盘为摩擦副研究黑磷烯量子点作为水基润滑添加剂的摩擦学性能。试验结果表明,黑磷烯量子点的平均横向尺寸为4.44 nm±0.86 nm,厚度约小于4 nm,在超纯水中表现出良好的分散性。随着接触压力增加,摩擦因数和磨损率先快速减小后缓慢增加。在1273 MPa接触压力、119.3 mg/L浓度下,和超纯水相比,黑磷烯量子点水基润滑添加剂的平均摩擦因数和磨损率分别降低27.6%和28.29%。磨痕表面分析表明,黑磷烯量子点水基润滑添加剂的抗磨减摩机理为钛合金磨损表面生成的Fe_(2)O_(3)、TiO_(2)、Al_(2)O_(3)氧化物组成的摩擦化学反应膜及黑磷烯量子点层间剪切和滚珠效应的协同作用。此研究为黑磷烯水基润滑添加剂在钛合金切削润滑领域的应用提供理论依据。

关键词：黑磷烯量子点润滑添加剂摩擦学性能润滑机理

水下搅拌摩擦加工Ti-15-3合金的组织及超塑性变形

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兵器材料科学与工程 2024年第4期47卷 59-63页

作者：倪立锦王文韩鹏乔柯强凤鸣王快社西安建筑科技大学冶金工程学院陕西西安710055

采用水下搅拌摩擦加工技术制备细晶Ti-15V-3Al-3Cr-3Sn(Ti-15-3)合金。通过电子背散射衍射对搅拌区(stirring zone,SZ)晶粒细化机制进行分析。用电子万能试验机对SZ试样进行超塑性拉伸。结果表明:SZ高角度晶界比例为74.5%,平均晶粒尺寸... 详细信息

采用水下搅拌摩擦加工技术制备细晶Ti-15V-3Al-3Cr-3Sn(Ti-15-3)合金。通过电子背散射衍射对搅拌区(stirring zone,SZ)晶粒细化机制进行分析。用电子万能试验机对SZ试样进行超塑性拉伸。结果表明:SZ高角度晶界比例为74.5%,平均晶粒尺寸为1.8μm,主要的晶粒细化机制为连续动态再结晶;在变形温度为675℃,应变率为3×10^(-4)s^(-1)时,SZ试样的伸长率达到了465%,为超塑性,主要变形机制为晶界滑移,同时伴随连续动态再结晶和β→α相变。

关键词：水下搅拌摩擦加工 Ti-15-3合金显微组织超塑性晶界滑移

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Tribological behavior of black phosphorus nanosheets as water-based lubrication additives

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Friction 2022年第3期10卷 374-387页

作者： Qingjuan wang Tingli HOU Wei wang Guoliang ZHANG Yuan GAO kuaishe wang School of Metallurgy Engineering Xi’an University of Architecture and TechnologyXi’an 710055China School of Mechanical Engineering Tianjin University of Technology and EducationTianjin 300222China

Black phosphorus(BP)with a layered structure has been used gradually as a lubrication additive in the tribological *** this study,BP powders are produced via an easy method of high-energy ball milling using red phosphorus as a raw ***,BP nanosheets are prepared via liquid exfoliation in N-methyl pyrolidone *** tribological behavior of BP nanosheets as water-based lubrication additives(BP-WL)is evaluated under Ti6Al4V(TC4)/GCr15 *** results suggest that the 70 mg/L BP-WL sample exhibits excellent lubrication performance,whose coefficient of friction(COF)and ball wear rate reduced by 32.4%and 61.1%,respectively,compared with those of pure ***,as the load increased,the tribological properties of BP-WL reduced gradually because of the agglomeration of BP *** on tribological experiments and worn surface analysis,boundary lubrication mechanisms are *** friction reduced,which is primarily attributed to the low interlaminar shear and adsorption of BP *** addition,a tribochemical reaction film comprising TiO_(2),Al_(2)O_(3),and Fe_(2)O_(3)effectively protects the surface of titanium alloy/steel from *** new water-based lubrication additive can be used to process titanium alloys.

关键词： black phosphorus(BP) tribological behavior lubrication additives titanium alloy/steel friction

Mo-14Re钼铼合金高温压缩耦合内变量的本构模型建立

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稀有金属材料与工程 2024年第5期53卷 1343-1348页

作者：杨俊宙王世臣王先俊王智轩王力邢海瑞胡卜亮高选乔张文胡平王快社西安建筑科技大学冶金工程学院陕西西安710055 功能材料加工国家地方联合工程研究中心陕西西安710055 西安建筑科技大学机电工程学院陕西西安710055 西北有色金属研究院陕西西安710016

为研究Mo-14Re钼铼合金高温流变行为及其跨尺度表征,采用Gleeble热模拟试验机对钼铼合金棒材进行了高温压缩试验,选取的温度为1400、1500、1600℃,应变速率为0.01、0.1、1、10 s^(-1)。结果表明,高温和低应变率变形时,应变率敏感因子逐... 详细信息

为研究Mo-14Re钼铼合金高温流变行为及其跨尺度表征,采用Gleeble热模拟试验机对钼铼合金棒材进行了高温压缩试验,选取的温度为1400、1500、1600℃,应变速率为0.01、0.1、1、10 s^(-1)。结果表明,高温和低应变率变形时,应变率敏感因子逐渐增大,材料塑性流动性能也就越好,且变形过程中应力硬化和软化2种现象同时存在。在此基础上,建立了跨尺度本构模型,流变应力表征考虑了与不动位错的阻力、热激活、晶界效应的微观剪切应力,微观组织演变考虑了晶粒尺寸、位错密度、动态再结晶率以及裂纹体积分数等微观组织演变。随后基于遗传算法确定了模型中的材料参数,屈服应力、晶粒尺寸和流变应力的模型计算值与试验结果吻合,可知该模型可以描述Mo-14Re钼铼合金在高温变形时流变行为及其微观组织演变。

关键词： Mo-14Re合金压缩变形本构方程跨尺度

Microstructure evolution and deformation mechanism ofα+βdual-phase Ti-xNb-yTa-2Zr alloys with high performance

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Journal of Materials Science & Technology 2022年第36期131卷 68-81页

作者： Ting Zhang Daixiu Wei Eryi Lu Wen wang kuaishe wang Xiaoqing Li Lai-Chang Zhang Hidemi Kato Weijie Lu Liqiang wang State Key Laboratory of Metal Matrix Composites School of Material Science and EngineeringShanghai Jiao Tong UniversityShanghai200240China School of Metallurgical Engineering Xi’an University of Architecture and TechnologyXi’an710055China Institute for Materials Research Tohoku University2-1-1 KatahiraSendaiMiyagi980-8577Japan Department of Stomatology Renji HospitalSchool of MedicineShanghai Jiao Tong UniversityShanghai200127China Department of Materials Science and Engineering KTH-Royal Institute of Technology10044StockholmSweden School of Engineering Edith Cowan University270 Joondalup DriveJoondalupPerthWA 6027Australia

Biomedicalβ-phase Ti-Nb-Ta-Zr alloys usually exhibit low elastic modulus with inadequate *** the present work,a series of newly developed dual-phase Ti-xNb-yTa-2Zr(wt.%)alloys with high performance were investigated in which the stability ofβ-phase was reduced under the guidelines of ab initio calculations and d-electronic *** effects of Nb and Ta contents on the microstructure,compressive and tensile properties were *** demonstrate that the designed Ti-xNb-yTa-2Zr alloys exhibit typical characteristics ofα+βdual-phase *** microstructure of the alloys is more sensitive to Nb rather than *** as-cast alloys exhibit needle-likeα′martensite at a lower Nb content of 3 wt.%and lamellarα′martensite at an Nb content of 5 wt.%.Among the alloys,the Ti-3Nb-13Ta-2Zr alloy shows the highest compressive strength(2270±10 MPa)and compressive strain(74.3%±0.4%).This superior performance is due to the combination ofα+βdual-phase microstructure and stressinducedα"***,lattice distortion caused by Ta element also contributes to the compressive *** and Ta contents of the alloys strongly affect Young's modulus and tensile properties after *** as-rolled Ti-3Nb-13Ta-2Zr alloy exhibits much lower modulus due to lower Nb content as well as moreα"martensite andβphase with a good combination of low modulus and high strength among all the designed *** probe tomography analysis reveals the element partitioning between theαandβphases in which Ta concentration is higher than Nb in theα***,the concentration of Ta is lower than that of Nb in theβphase,indicating that theβ-stability of Nb is higher than that of *** work proposes modernα+βdual-phase Ti-xNb-yTa-2Zr alloys as a new concept to design novel biomedical Ti alloys with high performance.

关键词： Titanium alloy Phase stability Martensite Phase transformation Mechanical behavior