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Low Pressure DC Glow Discharge Air Plasma Surface Treatment of Polyethylene (PE) Film for Improvement of Adhesive Properties

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Plasma Science and Technology 2013年第1期15卷 56-63页

作者： krishnasamy navaneetha pandiyaraj Vengatasamy SELVARAJAN Rajendrasing R. DESHMUKH Coimbatore. Paramasivam YOGANAND Suresh BALASUBRAMANIAN Sundaram MARUTHAMUTHU Department of Physics Sri Shakthi Institute of Engineering and Technology Plasma Physics Laboratory Department of Physics Bharathiar University Department of Physics Institute of Chemical Technology Microbial-Corrosion Laboratory Central Electrochemical Research Institute

The present work deals with the change in surface properties of polyethylene （PE） film using DC low pressure glow discharge air plasma and makes it useful for technical applications. The change in hydrophilicity of the modified PE film surface was investigated by measuring contact angle and surface energy as a function of exposure time. Changes in the morphological and chemical composition of PE films were analyzed by atomic force microscopy （AFM） and X-ray photoelectron spectroscopy （XPS）. The improvement in adhesion was studied by measuring T-peel and lap-shear strength. The results show that the wettability and surface energy of the PE film has been improved due to the introduction of oxygen-containing polar groups and an increase in surface roughness. The XPS result clearly shows the increase in concentration of oxygen content and the formation of polar groups on the polymer surface. The AFM observation on PE film shows that the roughness of the surface increased due to plasma treatment. The above morphological and chemical changes enhanced the adhesive properties of the PE＇film surfaces, which was confirmed by T-peel and lap-shear tests.

关键词： glow discharge plasma PE hydrophilicity XPS and adhesion

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In vitro Cyto and Blood Compatibility of Titanium Containing Diamond-Like Carbon Prepared by Hybrid Sputtering Method

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Plasma Science and Technology 2012年第9期14卷 829-836页

作者： krishnasamy navaneetha pandiyaraj Jan HEEG Andreas LAMPKA Fabian JUNGE Torsten BARFELS Marion WIENECKE Young Ha RHEE Hyoung Woo KIM Department of Physics Sri Shakthi Institute of Engineering and Technology Institute of Surface and Thin Film Technology Hochschule WismarGermany Department of Microbiology College of Bioscience&BiotechnologyChungnam National University

In recent years, diamond-like carbon films （DLC） have been given more attention in research in the biomedical industry due to their potential application as surface coating on biomedical materials such as metals and polymer substrates. There are many ways to prepare metal containing DLC films deposited on polymeric film substrates, such as coatings from car- bonaceous precursors and some means that incorporate other elements. In this study, we in- vestigated both the surface and biocompatible properties of titanium containing DLC （Ti-DLC） films. The Ti-DLC films were prepared on the surface of poly （ethylene terephthalate）（PET） film as a function of the deposition power level using reactive sputtering technique. The films＇ hydrophilicity was studied by contact angle and surface energy tests. Their surface morphology was studied by scanning electron microscopy （SEM） and atomic force microscopy （AFM）. Their elemental chemical composition was analyzed using energy dispersive X-spectra （EDX） and X-ray photoelectron spectroscopy （XPS）. Their blood and cell compatibility was studied by in vitro tests, including tests on platelet adhesion, thrombus formation, whole blood clotting time and osteoblast cell compatibility. Significant changes in the morphological and chemical composition of the Ti-DLC films were observed and found to be a function of the deposition level. These morphological and chemical changes reduced the interfacial tension between Ti-DLC and blood proteins as well as resisted the adhesion and activation of platelets on the surface of the Ti-DLC films. The cell compatibility results exhibited significant growth of osteoblast cells on the surface of Ti incorporated DLC film compared with that of DLC film surface.

关键词： Ti-DLC hybrid reactive sputtering technique surface analysis cyto and blood compatibility

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Evaluation of influence of cold atmospheric pressure argon plasma operating parameters on degradation of aqueous solution of Reactive Blue 198(RB-198)

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Plasma Science and Technology 2020年第5期22卷 114-125页

作者： K navaneetha pandiyaraj D VASU P V A PADMANABHAN M PICHUMANI R R DESHMUKH V KANDAVELU Research Division of Plasma Processing(RDPP) Department of PhysicsSri Shakthi Institute of Engineering and TechnologyChinniyam Palayam(post)Coimbatore-641062India Department of Nanoscience and Technology Sri Ramakrishna Engineering CollegeCoimbatore-641022India Department of Physics Institute of Chemical TechnologyMatungaMumbai 400019India Department of Chemistry Sri Shakthi Institute of Engineering and TechnologyL&T bypassChinniyam Palayam(post)Coimbatore-641062India

The intention of this work is to remove Reactive Blue 198(RB-198)dye components from simulated water solution using cold atmospheric pressure argon plasma *** solutions of RB-198 dye were treated as a function of various operating parameters such as applied potential,reaction time and distance between the plasma jet and surface of the *** efficiency of the degradation of RB-198 molecules was explored by means of UV-Vis *** reactive species involved during the treatment process were examined by optical emission spectra(OES).The present hydroxyl radicals(OH·radical)and hydrogen peroxide(H2O2)in the plasma-treated aqueous dye solutions were investigated using various spectroscopic *** other parameters such as total organic carbon(TOC),conductivity and p H were also *** toxicity of plasma-treated RB-198 solution was finally studied by diffusion bacterial analysis and by tracking seed germination *** results show that a higher degradation percentage of99.27%was acquired for the RB-198 treated at higher reaction time and applied potential,and shorter distance between the plasma jet and water *** may be due to the formation of various reactive oxygen(OH·radical,atomic oxygen(O)and H2O2)and nitrogen species(nitric oxide(NO)radicals and N2 second positive system(N2 SPS))during the processes as confirmed by OES analysis and other spectroscopy ***(17.7%-81.8%)and pH(7.5-3.4)values of the plasma-treated RB-198 decreased significantly with respect to various operation parameters,which indicates the decomposition of RB-198 molecules in the aqueous ***,the conductivity of plasma-treated RB-198 aqueous solutions was found to have increased linearly during the plasma treatment due to the formation of various ionic species in aqueous *** toxicity analysis clearly exhibits the non-toxic behavior of plasma-treated RB-198 aqueous solution towards the bacterial growth and germination of see

关键词： RB-198 degradation non-toxicity cold atmospheric pressure plasma jet

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