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Acta Metallurgica Sinica(English Letters) 2024年第1期37卷 78-88页

作者： Leilei Li kaikai song Qingwei Gao Changshan Zhou Xiaoming Liu Yaocen Wang Xiaojun Bai Chongde Cao School of Physical Science and Technology Northwestern Polytechnical UniversityXi’an710016China Weihai Research Institute of Industrial Technology Shandong UniversityWeihai264209China Research and Development Institute of Northwestern Polytechnical University in ShenzhenShenzhen518057China

The L1_(2)-strengthened Co_(34)Cr_(32)Ni_(27)Al_(4)Ti_(3)medium-entropy alloy(MEA)with precipitations of grain boundaries has been developed through selective laser melting(SLM)followed by cold rolling and annealing,exhibiting excellent strength-ductility *** as-printed alloy exhibits low yield strength(YS)of~384 MPa,ultimate tensile strength(UTS)of~453 MPa,and uniform elongation(UE)of 1.5%due to the existence of the SLM-induced *** cold rolling and annealing,the YS,UTS,and UE are significantly increased to~739 MPa,~1230 MPa,and~47%,*** enhancement primarily originates from the refined grain structure induced by cold rolling and *** presence of coherent sphericalγ'precipitates(L1_(2)phases)and Al/Ti-rich precipitates at the grain boundaries,coupled with increased lattice defects such as dislocations,stacking faults,and ultrafine deformation twins,further contribute to the property’s *** study highlights the potential of SLM in producing high-strength and ductile MEA with coherent L1_(2)nanoprecipitates,which can be further optimized through subsequent rolling and annealing *** findings offer valuable insights for the development of high-performance alloys for future engineering applications.

关键词： Medium-entropy alloy Selective laser melting Precipitation Strength Ductility

Ultrasonic vibration enabled under-liquid forming of metallic glasses

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Science Bulletin 2024年第2期69卷 163-166页

作者： Xin Li Luyao Li Sajad Sohrabi Jia'nan Fu Zhen Li Zhe Chen Rongce Sun Yu Zhang Jinbiao Huang Heting Zhang Jian Zhu Xiangyan Chen kaikai song Jiang Ma School of Mechanical Electrical&Information EngineeringShandong UniversityWeihai 264209China State Key Laboratory of Radio Frequency Heterogeneous Integration College of Mechatronics and Control EngineeringShenzhen UniversityShenzhen 518060China Department of Mechanics and Aerospace Engineering Southern University of Science and TechnologyShenzhen 518055China Shenzhen Research Institute of Shandong University Shenzhen 518057China

Advancements in forming technology offer significant advantages for the manufacturing industry,including enhanced efficiency,energy conservation,and improved material utilization[1].However,traditional additive manufacturing[2],thermoplastic forming[3],and laser cutting[4]encounter challenges when applied in under-liquid environments,mainly due to difficulties in temperature control and heat source provision.

关键词： glasses liquid metallic

Enhanced thermoelectric performance of n-type Bi_(2)Te_(2.7)Se_(0.3) via a simple liquid-assisted shear exfoliation

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Journal of Materials Science & Technology 2022年第22期117卷 251-258页

作者： Yifeng Wang Yilin song kaikai song Lin Pan Changchun Chen Kunihito Koumoto Qingfeng Liu College of Materials Science and Engineering Nanjing Tech UniversityNanjing 210009China Jiangsu Collaborative Innovation Center for Advanced Inorganic Function Composites Nanjing Tech UniversityNanjing 210009China Nagoya Industrial Science Research Institute Nagoya 464-0819Japan Center of Nanotechnology King Abdulaziz UniversityJeddah 21589Saudi Arabia State Key Laboratory of Materials-Oriented Chemical Engineering College of Chemical EngineeringNanjing Tech UniversityNanjing 210009China

A liquid-assisted shear exfoliation (LASE) as a new powder metallurgy method coupled with spark plasmasintering (SPS) was applied for n-type Bi_(2)Te_(2.7)Se_(0.3) and the effects on microstructure and anisotropictransport properties were investigated. Results revealed an effective reduction of average grain size dueto LASE and a high texturing in the bulks. Moreover, along the in-plane direction, electrical conductivitywas increased noticeably due to an enhanced carrier concentration, leading to a significantly improvedpower factor of 25 μW cm^(–1) K^(–2) at 303 K. Meanwhile, the total thermal conductivity was reduced effectively owing to reduction both in lattice component due to enhanced phonon scattering with the grainsize reduction, and in the bipolar component inhibited by the increased carrier concentration. Ultimately,a peak thermoelectric figure of merit (ZT) value of 0.83 was obtained at 448 K along the in-plane direction, increased by 95% compared with the pristine one. These results demonstrate the LASE process as auseful assistant method for enhancing the TE performance of layered materials.

关键词： Bi_(2)Te_(2.7)Se^(0.3) Liquid-assisted shear exfoliation Textured microstructure Thermoelectric

Phase formation,texture evolutions,and mechanical behaviors of Al0.5CoCr0.8FeNi2.5V0.2 high-entropy alloys upon cold rolling

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Progress in Natural Science:Materials International 2022年第2期32卷 196-205页

作者： Tongtong Sun Weidong song Feilong Shan kaikai song Kun Zhang Chuanxiao Peng Honggang Sun Lina Hu School of Mechanical Electrical & Information Engineering Shandong University State Key Laboratory of Explosion Science and Technology Beijing Institute of Technology CAS Key Laboratory of Microgravity (National Microgravity Laboratory) Institute of Mechanics Chinese Academy of Sciences Key Laboratory for Liquid-Solid Structural Evolution & Processing of Materials (Ministry of Education) Shandong University

The cold rolling(CR) reduction dependence of microstructure evolutions and mechanical properties for Al0.5CoCr0.8FeNi2.5V0.2high-entropy alloy(HEA) were *** HEA remains FCC structures consisting of nanoscale ordered L12phase,confirming the phase formation *** increasing CR reduction,the textures transform from random ones to FCC rolling ones accompanied by dense slip bands and deformation *** a 50% CR reduction,the deformation textures started to become evident and were governed by typical {111}F,{110}Goss and {112}Cu texture *** the CR reduction approached 90%,the deformation textures mainly contained the {110}A,{114}X,and {112}Cu texture *** a result,both Vickers hardness and ultimate strength increased,but the ductility decreased *** enhanced strength should be attributed to the anisotropy and work hardening behavior from *** plastic deformation for the samples under low CR reductions was dominated by deformation twins and slip ***,under high CR reductions,the textures severely impeded the further propagation of pre-existing slip bands,leading to the rapid decrease of ***,the CR reduction should be carefully designed before optimal heat treatments to enhance the strength and ductility synergy.

关键词： High-entropy alloys Cold rolling Texture Mechanical property Ductility

Additive manufacturing of a Co-Cr-W alloy by selective laser melting:In-situ oxidation,precipitation and the corresponding strengthening effects

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Journal of Materials Science & Technology 2022年第30期125卷 171-181页

作者： Kefeng Li Zhi Wang kaikai song Khashayar Khanlari Xu-Sheng Yang Qi Shi Xin Liu Xinhua Mao Institute of New Materials Guangdong Academy of SciencesGuangzhou 510650China National Engineering Research Center of Powder Metallurgy of Titanium and Rare Metals Guangzhou 510650China Guangdong Key Laboratory for Advanced Metallic Materials Processing South China University of TechnologyGuangzhou 510641China School of Mechanical Electrical and Information EngineeringShandong UniversityWeihai 264209China Advanced Manufacturing Technology Research Center Department of Industrial and Systems EngineeringThe Hong Kong Polytechnic UniversityHung HomKowloonHong KongChina Hong Kong Polytechnic University Shenzhen Research Institute Shenzhen 518000China

Additive manufacturing exhibits great potentials for the fabrication of novel materials due to its unique non-equilibrium solidification and heating *** this work,a novel nano-oxides dispersion strengthened Co28 Cr9 W1.5 Si(wt.%)alloy,fabricated by laser powder bed fusion(LPBF),was comprehensively *** the layer-by-layer featured process,in-situ formation of Si rich,amorphous,nano-oxide inclusions was observed,whose formation is ascribed to the high affinity of Si to ***,distinctive body-centered cubic(BCC)Co5 Cr3 Si2 nano-precipitates with an 8-fold symmetry were also confirmed to *** precipitates,rarely reported in previous studied Co-Cr alloys,were found to tightly bond with the in-situ ***,the morphologies,the size distributions as well as the microstructure of the interface between the matrix and the inclusions were investigated in detail and their influence on the tensile deformation was also *** existence of transition boundaries between these inclusions and the matrix strongly blocked the movement of dislocations,thereby increasing the strength of the *** was understood that when the plastic deformation proceeds,the fracture occurs in the vicinity of the oxide inclusions where dislocations accumulate.A quantitative analysis of the strengthening mechanism was also established,in which an additional important contribution to strength(~169 MPa)caused by the effects of in-situ formed oxide inclusions was calculated.

关键词： Co-Cr-W-Si alloy Selective laser melting Oxide inclusion Precipitation Strengthening mechanisms

Accelerating matrix/boundary precipitations to explore high-strength and high-ductile Co_(34)Cr_(32)Ni_(27)Al_(3.5)Ti_(3.5) multicomponent alloys through hot extrusion and annealing

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Journal of Materials Science & Technology 2023年第12期143卷 62-83页

作者： Xiaoming Liu Zongde Kou Ruitao Qu Weidong song Yijia Gu Changshan Zhou Qingwei Gao Jiyao Zhang Chongde Cao kaikai song Vladislav Zadorozhnyy Zequn Zhang Jürgen Eckert Shenzhen Research Institute of Shandong University Shenzhen 518057China State Key Laboratory of Explosion Science and Technology Beijing Institute of TechnologyBeijing 100081China School of Mechanical Electrical&Information EngineeringShandong UniversityWeihai 264209China School of Material Science and Engineering Nanjing University of Science and TechnologyNanjing 210094China School of Materials Science and Engineering Northwestern Polytechnical UniversityXi’an 710072China Department of Materials Science and Engineering Missouri University of Science and TechnologyRollaMO 65409USA Research and Development Institute of Northwestern Polytechnical University in Shenzhen Shenzhen 518057China National University of Science and Technology«MISIS» Moscow 119049Russia Erich Schmid Institute of Materials Science Austrian Academy of SciencesLeoben A-8700Austria Department of Materials Science Montanuniversität LeobenLeoben A-8700Austria

Annealing-regulated precipitation strengthening combined with cold-working is one of the most efficient strategies for resolving the conflict between strength and ductility in metals and ***,precipitation control and grain refinement are mutually contradictory due to the excellent phase stability of multicomponent *** work utilizes the high-temperature extrusion and annealing to optimize the microstructures and mechanical properties of the Co_(34)Cr_(32)Ni_(27)Al_(3.5)Ti_(3.5) multicomponent *** extrusion effectively reduces grain sizes and simultaneously accelerates the precipitation of coherent L12 nanoparticles inside the face-centered cubic(FCC)matrix and grain boundary precipitations(i.e.,submicron Cr-rich particles and L12-Ni 3(Ti,Al)precipitates),resulting in strongly reciprocal interaction between dislocation slip and hierarchical-scale *** annealing regulates grain sizes,dislocations,twins,and precipitates,further allowing to tailor mechanical *** high yield strength is attributed to the coupled precipitation strengthening effects from nanoscale coherent L12 particles inside grains and submicron grain boundary precipitates under the support of pre-existing *** excellent ductility results from the synergistic activation of dislocations,stacking faults,and twins during plastic *** present study provides a promising approach for regulat-ing microstructures,especially defects,and enhancing the mechanical properties of multicomponent alloys.

关键词： Multicomponent alloys Hot extrusion Microstructure Mechanical properties Precipitation strengthening

Thermal Stability and Transformation-mediated Deformability of Cu-Zr-Al-Ni Bulk Metallic Glass Composite

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Journal of Materials Science & Technology 2013年第9期29卷 868-872页

作者： Meiting Xie Pengna Zhang kaikai song School of Mechanical Engineering Binzhou Polytechnic College of Math and Physics Nanjing University of Information Science and Technology IFW Dresden Institut für Komplexe Materialien TU Dresden Institut für Werkstoffwissenschaft

The glass-forming ability and the thermal stability of Cu45Zr45AI5Ni5 metallic glass were systematically investigated by the differential scanning calorimetry. The activation energies for the glass transition and the onset crystallization and the crystallization peak were calculated to be 255.1, 308.7 and 311.5 kJ/mol, respectively, while the corresponding liquid fragility was determined to be 23.4. By controlling the casting process, Cu45Zr45AI5Ni5 bulk metallic glass composite with the presence of ductile B2 CuZr phase was fabricated. The composite shows a pronounced plastic strain of 6.8 ~ 0.05% with obvious work hardening, which results from the formation of multiple shear bands and the deformation-induced martensitic transformation.

关键词： Amorphous Activation energy Martensitic transformation Mechanical properties

High pressure floating-zone growth and property characterization of Cr-doped hexagonal YMnO_3 crystals

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Journal of Materials Science & Technology 2017年第9期33卷 1061-1066页

作者： Feng Wan Xiaojun Bai kaikai song Jianbang Zheng Xin Lin Chongde Cao Department of Applied Physics Northwestern Polytechnical University School of Mechanical Electrical & Information EngineeringShandong University (Weihai) State Key Laboratory of Solidification Processing School of Materials Science and EngineeringNorthwestern Polytechnical University

Large crystal growth of Cr-doped h-YMnO3has been investigated by using a high pressure optical floatingzone method. The size of the grown crystals is typically 60–70 mm in length and 4–5 mm in diameter. The structure of the grown crystals is analyzed by powder X-ray diffraction and scanning electron *** defects in the as-grown crystals, including low-angle grain boundary and inclusions are studied. An off-stoichiometric phenomenon is found with a slight Cr deficiency in different parts. The relationship between defects and growth conditions during crystal growth is also discussed. The magnetic properties show spin-glass phase features with weak ferromagnetic behavior below 30 K.

关键词： High pressure floating zone technique Crystal growth Cr-doped YMnO3 High vapor pressure compound

Glass-forming ability, phase formation and mechanical properties of glass-forming Cu-Hf-Zr alloys

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Progress in Natural Science:Materials International 2019年第5期29卷 576-581页

作者： K.Kosiba kaikai song U.Kühn Gang Wang S.Pauly Leibniz IFW Dresden Institute for Complex Materials School of Mechanical Electrical & Information Engineering Shandong University (Weihai) Laboratory for Microstructures Institute of Materials Shanghai University

The influence of Hf additions on the glass-forming ability（GFA）,phase formation and mechanical properties of Cu;Hf;Zr;（x=2,5,10,20 at.%）alloys has been systematically *** report on a distinct correlation between phase formation and GFA of Cu;Zr;-based *** additions of Hf reduce the thermal stability of the high-temperature B2Cu（Hf,Zr）phase,while the thermal stability of the corresponding undercooled melt is *** GFA of these alloy series gradually raises up to 10 at.%Hf,whereas at 20 at.%Hf,the GFA is drastically lowered,since the B2Cu（Hf,Zr）phase becomes unstable and the precipitation of the lowtemperature equilibrium phases is *** interrelation determines the microstructure and results in the formation of Cu-Hf-Zr-based bulk metallic glass *** composites not only show appreciable macroscopic plastic strain,but also high yield strength.

关键词： Metallic glasses Glass-forming ability Composites Continuous cooling transformation (CCT) diagram Mechanical properties

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基于增材制造技术的非晶合金研究进展

稀有金属材料与工程 2022年第4期51卷 1497-1513页

作者：雷杨王沛邓亮陈张伟马将刘志远宋凯凯深圳大学机电与控制工程学院广东深圳518060 中车工业研究院有限公司北京100161 山东大学(威海)机电与信息工程学院山东威海264209

近年来,为了满足具有大尺寸复杂结构的非晶合金构件的市场需求,具有高度柔性化成形、机加工量小和成形精度高等特点的增材制造技术被成功应用于制备块体非晶合金。本文基于各国块体非晶合金增材制造成形领域的最新研究成果及作者们多年... 详细信息

近年来,为了满足具有大尺寸复杂结构的非晶合金构件的市场需求,具有高度柔性化成形、机加工量小和成形精度高等特点的增材制造技术被成功应用于制备块体非晶合金。本文基于各国块体非晶合金增材制造成形领域的最新研究成果及作者们多年来在该领域的研究工作,系统介绍了现有非晶合金增材制造技术的研究现状,详细阐述了非晶合金在各类增材制造技术中的成形机理和性能方面的研究进展,深入探讨了现有非晶合金增材制造成形的技术难点,详细阐明了非晶合金增材制造成形工艺-组织结构-性能间的内在联系,指出制备高质量高性能非晶构件将是块体非晶合金增材制造成形领域未来研究的重要方向。

关键词：增材制造技术块体非晶合金力学性能