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Effect of the Preparation Method on Co/Al<sub>2</sub>O<sub>3</sub>Catalyst Applied to Ethanol Steam Reforming Reaction Production of Hydrogen

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Modern Research in Catalysis 2012年第3期1卷 52-57页

作者： Silmara Rodrigues Garcia josé mansur assaf Laboratory of Catalysis-Chemical Engineering Department-Federal University of Sao Carlos

Alumina supported cobalt catalysts were prepared, characterized and applied in ethanol steam reforming for hydrogen production. The support and the supported catalysts were prepared, respectively, by the solvothermal and precipitation, impregnation and deposition-precipitation methods. The cobalt was added by impregnation and deposition-precipitation in the Al2O3 supports using a Co(NO3)2·6H2O solution. The solids were characterized, Temperature-Programmed Re-duction with H2 (RTP-H2), X-Ray Diffraction (DRX), BET Nitrogen Adsorption and Temperature Programmed Oxida-tion (TPO). The results indicated that the preparation method and the treatment conditions of samples were appropriate for obtaining the wanted compounds. Co3O4 phase was verified for all catalysts through analyses of DRX and RTP-H2 results. Catalytic tests were performed by varying the temperature from 450?C to 600?C, with water: ethanol molar ratio of 3:1. The ethanol conversion was superior of 99%, with greater hydrogen yield at 600℃. The lower carbon deposition was observed in catalysts prepared with solvothermal/deposition-precipitation methods at 450℃.

关键词： Hydrogen Ethanol Reform Cobalt Alumina

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Assessment of Genetic Stability Among In Vitro Plants of Arachis retusa Using RAPD and AFLP Markers for Germplasm Preservation

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Journal of Integrative Plant Biology 2007年第3期49卷 307-312页

作者： Rachel Fatima Gagliardi Luiz Ricardo Hanai Georgia Pacheco Carlos Alberto Oliveira Leonardo Alves Carneiro josé Francisco Montenegro Valls Elisabeth mansur Maria Lucia Carneiro Vieira Laboratório de Micropropagacao e Transformacao de Plantas Universidade do Estado do Rio de Janeiro postal code 20550-013 Maracana Rio de Janeiro Brazil Departamento de Genética - Escola Superior de Agricultura Luiz de Queiroz Universidade de Sao Paulo postal code 13418-900 Piracicaba Brazil Embrapa Recursos Genéticos e Biotecnologia postal code 70770-901 Brasilia Brazil

Arachis retusa Krapov. et W. C. Gregory et Valls is endemic in the West-central region of Brazil, occurring In areas endangered by human actions. The establishment of in vitro preservation methods for wild species of Arachis is an alternative to seed banks for germplasm storage, multiplication and distribution. The risk of genetic changes Induced by tissue culture and the monitoring of the genetic stability of the biological material before, during and after storage must be considered In the context of conservation. Random amplified polymorphlc ONA （RAPO） and amplified fragment length polymorphism （AFLP） fingerprinting were used to evaluate the genetic stability of in vitro plants originated from cotyledons and embryo axes of A. retusa. Cotyledons originated shoots through direct organogenesls and embryo axes displayed muItishoot formation Induced by 110 mmol/L and 8.8 mmol/L BAP, respectively. Ninety genomlc regions （loci） generated from RAPO and 372 from AFLP analyses were evaluated. All amplified fragments detected by both techniques in plants derived from the two explant types were monomorphic. The results Indicate that the recovered shoots are genetically stable at the assessed genomic regions.

关键词： amplified fragment length polymorphism Arachis retusa in vitro preservation micropropagation random amplifiedpolymorphic DNA somaclonal variation

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COMPETITIVE LIQUID-LIQUID EXTRACTION OF NICKEL AND COBALT WITH D2EHPA

COMPETITIVE LIQUID-LIQUID EXTRACTION OF NICKEL AND COBALT WI...

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International Solvent Extraction Conference 2005

作者： josé dos Prazeres Ferreira Filho Adriane Salum Marcelo Borges mansur Departamento de Engenharia Química Universidade Federal de Minas Gerais R. Espírito Santo 35 6° andar Belo Horizonte MG Brazil Departamento de Engenharia Química Universidade Federal de Minas Gerais R. Espírito Santo 35 6° andar Belo Horizonte MG Brazil Departamento de Engenharia Química Universidade Federal de Minas Gerais R. Espírito Santo 35 6° andar Belo Horizonte MG Brazil

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