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Development of metal organic fromwork-199 immobilized zeolite foam for adsorption of common indoor VOCs

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Journal of Environmental Sciences 2017年第5期29卷 321-330页

作者： Vipin K.Saini joao Pires School of Environment and Natural Resources Doon UniversityDehradun 248001India Department of Chemistry and Biochemistry Faculty of SciencesUniversity of LisbonLisbon 1749-016Portugal

Reticulated foam shaped adsorbents are more efficient for the removal of volatile organic compounds（VOCs）,particularly from low VOC-concentration indoor air streams. In this study composite structure of zeolite and metal organic frameworks（MOFs）,referred as ZMF,has been fabricated by immobilization of fine MOF-199 powder on foam shaped Zeolite Socony Mobil-5（ZSM-5）Zeolitic structure,referred as ZF. The ZMF possess a uniform and well-dispersed coating of MOF-199 on the porous framework of ZF. It shows higher surface area,pore volume,and VOCs adsorption capacity,as compared to ***-fabrication changes in selective adsorption properties of ZMF were studied with three common indoor VOCs（benzene,n-hexane,and cyclohexane）,using gravimetric adsorption technique. The adsorption capacity of ZMF with different VOCs follow the order of benzene 〉 n-hexane 〉 cyclohexane. In comparison with MOF-199 and ZF,the composite structure ZMF shows improvement in selectivity for benzene from other two VOCs. Further,improvement in efficiency and stability of prepared ZMF was found to be associated with its high MOF loading capacity and unique morphological and structural properties. The developed composite structure with improved VOCs removal and recyclability could be a promising material for small to limited scale air pollution treatment units.

关键词： VOCs Adsorption Composite materials Selectivity Zeolite foam MOFs HKUST-1

PHASE-FIELD MODELING OF ELASTIC EFFECTS IN EUTECTIC GROWTH WITH MISFIT STRESSES

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International Journal of Modeling, Simulation, and Scientific Computing 2013年第1期4卷 34-50页

作者： ZOHREH EBRAHIMI joao REZENDEH AICES Graduate School RWTH Aachen University D-52056 AachenGermany Institute of Minerals Engineering(GHI)RWTH Aachen University D-52056 AachenGermany

Elastic interactions,arising from a difference of lattice spacing between two coherent phases in eutectic alloys with misfit stresses,can have an influence on microstructural pattern formation of eutectic colonies during solidification *** a thermodynamic point of view the elastic energy contributes to the free energy of the phases and modifies their mutual ***,the elastic stresses will have an effect on stability of lamellae,lamellae spacing and growth *** this paper,a phase-field model is employed to investigate the influence of elastic misfits in eutectic *** model reduces to the traditional sharp-interface model in a thin-interface limit,where the microscopic interface width is small but *** elastic model is designed,based on linear microelasticity theory,to incorporate the elastic energy in the phase-field *** and numerical approaches,required to model elastic effects,are formulated and the stress distributions in eutectic solidification structures are *** twodimensional simulations are performed for directed eutectic growth and the simulation results for different values of the misfit stresses are illustrated.

关键词： Elastic energy misfit stress eutectic growth.

Imbalance in T-cell differentiation as a biomarker of chronic diabetic foot ulceration

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Cellular & Molecular Immunology 2019年第10期16卷 833-834页

作者： joao Moura joao Rodrigues Marta Gonçalves Claudia Amaral Margarida Lima Eugenia Carvalho Center for Neuroscience and Cell Biology(CNC) University of CoimbraCoimbraPortugal INEB-Instituto Nacional de Engenharia Biomedica University of PortoPortoPortugal I3S-Instituto de Investigaçao e Inovaçao em Saude University of PortoPortoPortugal Department of Hematology Hospital de Santo Antonio(HSA)Centro Hospitalar Universitario do Porto(CHUP)PortoPortugal Unidade Multidisciplinar de Investigaçao Biomedica(UMIB/ICBAS/UP) PortoPortugal Department of Endocrinology Hospital de Santo Antonio(HSA)Centro Hospitalar Universitário do Porto(CHUP)PortoPortugal Department of Geriatrics University of Arkansas for Medical Sciences(UAMS)and Arkansas Children’s Hospital Research Institute(ACHRI)Little RockArkansas 72202USA

Diabetes is a growing epidemic due to the systematic increase in overweight and obesity,and chronic diabetic foot ulcers(DFUs)are the most debilitating and costly complication of *** is still essential for DFU care,but early detection is limited because we do not have a good DFU ***,we report the preliminary results of a large longitudinal study to test the effectiveness of the use of T-cell phenotype and TCR repertoire diversity as DFU *** results show that the ratio of effector/naïve T-cells and the number of TCR expansions are valuable biomarkers of DFU prognosis.

关键词： diabetic chronic obesity

Intelligent negotiation model for ubiquitous group decision scenarios

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Frontiers of Information Technology & Electronic Engineering 2016年第4期17卷 296-308页

作者： joao CARNeirO Diogo MARTINHO Goreti MARReirOS Paulo NOVAIS GECAD-Knowledge Engineering and Decision Support Group Institute of EngineeringPolytechnic of PortoPorto 4200-072Portugal ALGORITMI Centre University of MinhoGuimaraes 4800-058Portugal

Supporting group decision-making in ubiquitous contexts is a complex task that must deal with a large amount of factors to succeed. Here we propose an approach for an intelligent negotiation model to support the group decision-making process specifically designed for ubiquitous contexts. Our approach can be used by researchers that intend to include arguments, complex algorithms, and agents' modeling in a negotiation model. It uses a social networking logic due to the type of communication employed by the agents and it intends to support the ubiquitous group decision-making process in a similar way to the real process, which simultaneously preserves the amount and quality of intelligence generated in face-to-face meetings. We propose a new look into this problem by considering and defining strategies to deal with important points such as the type of attributes in the multicriterion problems, agents' reasoning, and intelligent dialogues.

关键词： Group decision support systems Ubiquitous computing Automatic negotiation Social networks Multi-agent systems

Influence of climate fluctuations on Pinus palustris growth and drought resilience

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Forest Ecosystems 2023年第6期10卷 681-689页

作者： joao Campoa Joshua Puhlick CENSE–Center for Environmental and Sustainability Research CHANGE-Global Change and Sustainability InstituteDepartment of Environmental Sciences and EngineeringNOVA School of Science and TechnologyNOVA University LisbonCampus de Caparica2829-516 CaparicaPortugal The Jones Center at Ichauway 3988 Jones Center Drive39870NewtonGAUSA

The longleaf pine(Pinus palustris Mill.)ecosystem is an endangered ecosystem in the southeastern USA,and efforts to restore the species are ***,in recent decades,the region has experienced drastic fluctuations between wet and dry growing season conditions from year to year,and it is not fully understood how these fluctuations have influenced the growth of *** address this topic,we cored *** trees in woodlands of southwest Georgia and used dendrochronology techniques to determine how climate fluctuations have influenced the growth and drought resilience of *** also cored slash pine(Pinus elliottii Engelm.)trees in the same woodlands to compare growth between *** *** growth was less impacted by adverse climate conditions compared to ***,the strength of correlations between *** growth and temperature,precipitation,and Palmer Drought Severity Index(PDSI)changed over *** recent decades,climate conditions during the growing season became more influential on *** growth than the previous year's *** is concerning given that drought severity during the growing season has been *** results also indicate that *** was less resilient to droughts during the 2000s and 2010s than to those of the *** this new climate paradigm,our results suggest that *** might be more susceptible to growth reductions and less resistant to droughts than once *** work highlights the importance of understanding the impact of novel climate conditions on *** and has implications for restoration efforts,such as using silvicultural treatments that reduce tree vulnerability to drought(e.g.,thinning)and promote other climate-adapted species in mixture with ***.

关键词： Longleaf pine Slash pine Pinus elliottii Climate change Dendrochronology Dendroclimatology Forest disturbances

TLBO with variable weights applied to shop scheduling problems

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CAAI Transactions on Intelligence Technology 2019年第3期4卷 148-158页

作者： Leonardo Ramos Rodrigues joao Paulo Pordeus Gomes Electronics Division Institute of Aeronautics and SpacePraca Marechal Eduardo Gomes50Sao Josedos Campos 12228-904Brazil Computer Science Department Federal University of CearaRua Campus do PiciSnFortaleza 60440-554Brazil

The teaching–learning-based optimisation (TLBO) algorithm is a population-based metaheuristic inspired on the teaching–learning process observed in a classroom. It has been successfully used in a wide range of applications. In this study, the authors present a variant version of TLBO. In the proposed version, different weights are assigned to students during the student phase, with higher weights being assigned to students with better solutions. Three different approaches to assign weights are investigated. Numerical experiments with benchmark instances of the flow-shop and the job-shop scheduling problems are carried out to investigate the performance of the proposed approaches. They compare the proposed approaches with the original TLBO algorithm and with two variants of TLBOs proposed in the literature in terms of solution quality, convergence speed and simulation time. The results obtained by the application of a Friedman statistical test showed that the proposed approaches outperformed the original version of TLBO in terms of convergence, with no significant losses in the average makespan. The additional simulation time required by the proposed approaches is small. The best performance was achieved with the approach of assigning a fixed weight to half the students with the best solutions and assigning zero to other students.

关键词： TLBO variable weights shop scheduling problems

3D Progressive Damage Based Macro-Mechanical FE Simulation of Machining Unidirectional FRP Composite

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Chinese Journal of Mechanical Engineering 2018年第3期31卷 128-143页

作者： Yan-Li He joao-Paulo Davim Hong-Qian Xue Key Laboratory of Contemporary Design and Integrated Manufacturing Technology of Ministry of Education School of Mechanical EngineeringNorthwestern Polytechnical University Department of Mechanical Engineering University of AveiroCampus Santiago

Finite element(FE) simulation is a powerful tool for investigating the mechanism of machining fiber?reinforced polymer composite(FRP). However in existing FE machining simulation works,the two?dimensional(2 D) progressive damage models only describe material behavior in plane stress,while the three?dimensional(3 D) damage models always assume an instantaneous sti ness reduction pattern. So the chip formation mechanism of FRP under machin?ing is not fully analyzed in general stress state. A 3 D macro?mechanical based FE simulation model was developed for the machining of unidirectional glass fiber reinforced plastic. An energy based 3 D progressive damage model was proposed for damage evolution and continuous sti ness degradation. The damage model was implemented for the Hashin?type criterion and Maximum stress criterion. The influences of the failure criterion and fracture energy dissipa?tion on the simulation results were studied. The simulated chip shapes,cutting forces and sub?surface damages were verified by those obtained in the reference experiment. The simulation results also show consistency with previous 2 D FE models in the reference. The proposed research provides a model for simulating FRP material behavior and the machining process in 3 D stress state.

关键词： FRP Macro mechanical Machining Finite element Progressive damage

Zircon U-Pb and Lu-Hf isotope constraints on Archean crustal evolution in Southeastern Guyana Shield

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Geoscience Frontiers 2019年第4期10卷 1477-1506页

作者： joao Marinho Milhomem Neto Jean-Michel Lafon Programa de Pos-graduacao em Geologia e Geoquimica-PPGG Instituto de Geociencias-IGUniversidade Federal do Para-UFPA66075-110BelemParaBrazil Laboratório de Geologia Isotópica-Pará-Iso IG-UFPA66075-110BelémParáBrazil

The southeastern Guyana Shield,northeast Amazonian Craton,in the north of Brazil,is part of a widespread orogenic belt developed during the Transamazonian orogenic cycle(2.26-1.95 Ga)that includes a large Archean continental landmass strongly reworked during the Transamazonian orogeny,named Amapa *** consists mainly of a high-grade metamorphic granulitic-migmatitic-gneiss complex,of Meso-to Neoarchean age and Rhyacian granitoids and supracrustal *** the first time,coupled U-Pb and Lu-Hf isotope data were obtained on zircon by LA-ICP-MS from five tectono-stratigraphic units of the Archean basement and one Paleoproterozoic intrusive rock,in order to investigate the main episodes of crustal growth and ***-rock Sm-Nd isotope data were compared to the zircon Lu-Hf *** main magmatic episodes were defined by U-Pb zircon dating,two in the Mesoarchean(~3.19 Ga and 2.85 Ga)and one in the Neoarchean(~2.69-2.65 Ga).SubchondriticεHf(t)values obtained for almost all investigated units indicate that crustal reworking processes were predominant during the formation of rocks that today make up the Amapa ***-TDMC model ages,ranging from2.99 Ga to 3.97 Ga,indicate that at least two important periods of mantle extraction and continental crust formation occurred during the Archean in southeastern Guyana Shield,an older one in the Eoarchean(~4.0 Ga)and a younger one in the Mesoarchean(~3.0-3.1 Ga).The latter is recognized as an important period of crustal accretion *** recognition of an Eoarchean episode to the southeastern most part of the Guyana Shield is unprecedented and was not recorded by whole-rock Sm-Nd data,which were restricted to the Meso-Paleoarchean(2.83 Ga to 3.51 Ga).This finding reveals t hat continental crust generation in the Amazonian Craton began at least 500 Ma earlier than previously suggested by the SmNd systematics.

关键词： U-Pb-Lu-Hf isotopes Zircon Archean crustal evolution Southeastern Guyana Shield Amazonian Craton

Quantification of theophylline or paracetamol in milk matrices by high-performance liquid chromatography

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Journal of Pharmaceutical Analysis 2017年第6期7卷 401-405页

作者： Tania A.P.fernandes joao P.Aguiara Ana I.fernandes joao F.Pinto CiiEM-Centro de Investigacao Interdisciplinar Egas Moniz Instituto Superior de Cinncias da Saude Egas MonizCampus Universitario-Quinta da GranjaMonte de Caparica2829-511 CaparicaPortugal iMed.UL-Dep.Tecnologia Farmaceutica Faeuldade de FarmdciaUniversidade de LisboaAv.Prof.Gama Pinto1649-003 LisboaPortugal

A simple, accurate and sensitive high-performance liquid chromatography （HPLC） method was developed, validated and applied to the determination of either theophylline or paracetamol in milk-based samples. The method allowed drug quantification in fresh and powdered milk with a relatively short run time of analysis and it was also successfully applied to the quantification of the drugs in solid dosage forms intended for pediatric use. Moreover, the main significant advantages over other published works are the simplicity of the sample preparation, reduced assay time and sample loss. The method meets the International Conference on Harmonization guideline for analytical methods validation regarding specificity, linearity, accuracy, precision, specificity and robustness as required by health authorities and applied by industry while designing and marketing new drug products. The technique encompasses the separation of the analytes with a reverse phase C18 column under isocrafic conditions and UV detection at 272 nm and 243 nm, respectively, for theophylline and paraeetamol. The lower limit of quantification for both drugs was determined as 0.2 μg/mL and the between-batch accuracy was 99.7%. This HPLC method allows quantification of theophylline and paracetamol in milk matrices and it can be applied in the design, development and production of milk-based pediatric dosage forms.

关键词： Liquid chromatography Fresh milk Powdered milk Paracetamol Theophylline