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Wuhan University Journal of Natural Sciences 2008年第1期13卷 98-102页

作者： BIN Xiaobei WANG Kaipeng CAO Hong KUANG Shenglu yuan jizu School of Resource and Environment Engineering Wuhan University of Technology Wuhan 430070 Hubei China School of Material Science and Engineering Wuhan Institute of Technology Wuhan 430074 Hubei China

Several kinds of Tungstophosphates of Heteropoly Compounds （TPHC） with different compositions and the same structure were synthesized using the method of solid-phase reaction to change the tool ratio of Na4P2O7·10H2O, WO3 and Na2WO4 · 2H2O. TPHC, as a catalyst, was used in oxidative desulfurization of diesel. The results show that TPHC has catalytic activity. With THPC existing, the highest desulfurization rate reaches 51.85%, 32.6% higher than that yield without TPHC. And the desulfiarization rate increases with decreasing WO3. FT-IR spectra of TPHC shows that the catalytic activity is related to the activity of end oxygen（Od）.The more active Od is, the stronger the capability of obtaining or losing electron is. It means that TPHC has a good catalytic activity. FT-IR spectra of TPHC indicates that desulfurization rate is in linear correlation with Iw-Od/Ip-Od/ Iw-Od is intensity of W-Od vibration band, Ip-Od is intensity of P-Od vibration band） and correlation coefficient reaches 0.965.

关键词： diesel oxidative desulfurization heteropoly compound catalyst

SYNTHESES OF 4A ZEOLITE IN DETERGENTS WITH KAOLIN

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Journal of Wuhan University of Technology(Materials Science) 1997年第Z1期12卷 58-62页

作者：曹明礼 Wuhan University of Technology

The main technical conditions for synthesizing 4A zeolite with kaolin were determined. The whiteness and calcium ion exchange capacity (CIEC) of the product were increased by calcining and screening the colouring ions, and the high quality 4A zeolite was synthesized successfully. Moreover, the formation mechanism of zeolite also discussed.

关键词： kaolin calcine 4A zeolite

STUDY ON ENHANCING THE WHITENESS OF CALCINED KAOLIN BY USING ADDITIVE

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Journal of Wuhan University of Technology(Materials Science) 1997年第Z1期12卷 42-46页

作者：曹明礼 Wuhan University of Technology The First Architectural Eng. Corporation of Guangzhou

To meet some special requirements such as paper filler,ceramic titanium white and synthetic 4A zeolite, the raising whiteness of calcined kaolin has become more and more important. The calcined experiments were carried out with and without additive to increase the whiteness of calcined kaolin. Results show that additive of chloride (A) or oxides can obviously increase the whiteness of calcined kaolin. Meantime,the mechanisms of enhancing the whiteness of calcined kaolin were discussed.

关键词： kaolin calcining enhancing whiteness additive

Study on the Treatment of Cellulosic Ethanol

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Journal of Environmental Science and Engineering 2010年第1期4卷 20-24页

作者： Zhihui Shi jizu yuan Zonghua Wang Wuhan University of Technology Wuhan 430070 China Nanyang Normal Colloge Nanyang 473000 China

Wastewater from the production of cellulosic ethanol was treated by the processes of internal micro-electrolysis method ＋ABR＋UASB ＋MBR. The results of running indicated that, when COD is 12000 mg/L and HRT of UASB is 48 h, the COD removal rate reaches 72% and HRT of MBR is 20 h, COD removal rate is between 80.8% and 87.5%. The effluent COD concentration stabilized at 301- 537 mg/L, it indicates that the MBR system has a strong ability to resist impact load.

关键词： Cellulosic ethanol micro-electrolysis UASB MBR.

ANALOG STUDY ON THE DEPRESSING MECHANISM OF TANNIN TO DIOPSIDE

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Journal of Wuhan University of Technology(Materials Science) 1996年第1期11卷 36-41页

作者：曹明礼袁继祖袁楚雄 Wuhan Univ of Technology Wuhan China

The depression mechanisms of tannin on the diopside surface have been studied by the rise of Infrared spectroscopy (IR), simulated pulp and mixed solution tests, It is found that the first order hydroxy completes of calcium are able to interact with tannin, and to form chemical complexes. es. The functional groups in tannin molecules participating in the chemical complexation are the hydroxyl groups, and carboxyl groups derived from the hydrolysis of hydroxyl groups.

关键词： tannin diopside depression mechanisms

FLOTATION SEPARATION OF WOLLASTONITE FROM DIOPSIDE

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Journal of Wuhan University of Technology(Materials Science) 1994年第1期9卷 59-64页

作者：袁继祖曹明礼袁楚雄 Wuhan Univ of Tech. China

The floatabilities of single mineral samples of Tvollas-tonite and diopside have been studied with addition of a cationic collector , dodecylamine hydrochloride (DDA ?HC1) , and modifiers. A mixture of two minerals was successfully separated , when DDA ?HC1 and tannic acid (as depressant)were used together . The interaction between tannic acid and wollastonite and diopside in the pulp and the adsorption of tannic acid on the surface of the two minerals was sttidide with the help of ultra-violet (UV) spectroscopy and X-ray photoelectron spectroscopy (XPS) , re-spectively.

关键词： wollastontte diopside flotation

Mechanism of Surface Modification for Sericite

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Journal of Wuhan University of Technology(Materials Science) 2007年第3期22卷 470-472页

作者：高惠民 School of Resources and Environmental Engineering Wuhan University of Technology

Surface modification of sericite by wet method was conducted with the addition of 1.0 % （w/w） silane. The resulting wetting contact angle and activity ratio of sericite were 130° and 98% respectively. Good pre-evaluation indexes of oil value （40.8%） and dispersivity （14.0 mL） were obtained. When 30 % of sericite was filled into acrylonitrile butadiene styrene（ABS） plastic, the bending strength and tensile strength of the composite material were reduced by 7% and 14.3% in comparison to those of pure ABS plastic, while the rigidity was increased by 3 times, and the impact strength and breaking elongation were reduced significantly. The mechanism of surface modification was investigated and the configuration of silane coupling agent on the surface of sericite was given. Infrared （IR） spectroscopic analysis indicates that the adsorption of silane on the surface of sericite belongs to chemical adsorption.

关键词： sericite surface modification ABS plastic

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溶胶-凝胶法制备高岭土基复合颜料

非金属矿 2008年第4期31卷 26-28,56页

作者：晏全香袁继祖武汉理工大学资环学院湖北武汉430070

以软质高岭土为基材,采用溶胶-凝胶法制备高岭土-二氧化钛复合颜料,对比不同条件下制备的复合颜料的性能指标,研究出较合理的工艺流程和工艺条件,实现以低成本制备性能优良(高白度、低吸油量)的新型复合颜料,以代替价格昂贵的钛白粉。

关键词：高岭土溶胶-凝胶法钛白粉复合颜料

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一种新型环保型污泥脱水絮凝剂的研制与应用

工业水处理 2007年第1期27卷 17-20页

作者：曾德芳袁继祖武汉理工大学资源与环境工程学院湖北武汉430070

以虾蟹壳和累托石为主要原料,制备出一种新型环保型污泥脱水絮凝剂,该絮凝剂的最佳配比为m(天然有机高分子)∶m(改性累托石)=16∶,它与传统絮凝剂聚丙烯酰胺相比,污泥脱水率提高了5.47%,污泥沉降时间缩短了33.33%,吨污泥单耗絮凝剂成本... 详细信息

以虾蟹壳和累托石为主要原料,制备出一种新型环保型污泥脱水絮凝剂,该絮凝剂的最佳配比为m(天然有机高分子)∶m(改性累托石)=16∶,它与传统絮凝剂聚丙烯酰胺相比,污泥脱水率提高了5.47%,污泥沉降时间缩短了33.33%,吨污泥单耗絮凝剂成本下降了4%,且处理过程中的二次污染大大减少。还对该絮凝剂的制备过程及絮凝机理等进行了阐述。

关键词：污泥脱水絮凝剂累托石水处理

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高新技术产业集群创新体系框架模型实证分析

科技进步与对策 2006年第7期23卷 124-126页

作者：王春梅袁继祖武汉理工大学资源与环境工程学院湖北武汉430070

对高新技术产业集群创新体系的构成进行了分析,指出了目前该体系具有的局限性。提出了创新高新技术产业集群创新体系框架模型,并给出了模型结构的系统解释,最后以美国硅谷地区的高新技术产业集群为例说明了该模型的应用。

关键词：高新技术产业集群区域产业集群创新体系模型