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Bioleaching of vanadium from stone coal vanadium ore by Bacillus mucilaginosus:Influencing factors and mechanism

International Journal of Minerals,Metallurgy and Materials 2024年第8期31卷 1828-1838页

作者： Yingbo Dong jinyu Zan Hai Lin School of Energy and Environmental Engineering University of Science and Technology BeijingBeijing 100083China Beijing Key Laboratory on Resource-oriented Treatment of Industrial Pollutants Beijing 100083China

Vanadium and its derivatives are used in various industries,including steel,metallurgy,pharmaceuticals,and aerospace *** China has massive reserves of stone coal resources,these resources have low ***,the effective extraction and recovery of metallic vanadium from stone coal is an important way to realize the efficient resource utilization of stone coal vanadium ***,Bacillus mucilaginosus was selected as the leaching *** vanadium leaching rate reached 35.5%after 20 d of bioleaching under optimal operating *** cumulative vanadium leaching rate in the contact group reached 35.5%,which was higher than that in the noncontact group(9.3%).The metabolites of ***,such as oxalic,tartaric,citric,and malic acids,dominated in bioleaching,accounting for 73.8%of the vanadium leaching ***,during leaching,the presence of stone coal stimulated the expression of carbonic anhydrase in bacterial cells,and enzyme activity increased by 1.335-1.905 *** activity positively promoted the production of metabolite organic acids,and total organic acid content increased by 39.31 mg·L^(-1),resulting in a reduction of 2.51 in the pH of the leaching system with stone *** effect favored the leaching of vanadium from stone *** force microscopy illustrated that bacterial leaching exacerbated corrosion on the surface of stone coal beyond 10 *** study provides a clear and promising strategy for exploring the bioleaching mechanism from the perspective of microbial enzyme activity and metabolites.

关键词： Bacillus mucilaginosus stone coal vanadium ore bioleaching carbonic anhydrase organic acids

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A New Class of Strong Orthogonal Arrays of Strength Three

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Journal of Systems Science & Complexity 2024年第3期37卷 1233-1250页

作者： WANG Chunyan LIU Min-Qian YANG jinyu Center for Applied Statistics and School of Statistics Renmin University of ChinaBeijing 100872China School of Statistics and Data Science LPMC&KLMDASRNankai UniversityTianjin 300071China

Strong orthogonal arrays(SOAs) were recently introduced and studied as a class of spacefilling designs for computer experiments. To surely realize better space-filling properties, SOAs of strength three or higher are desirable. In addition, orthogonality is also an important property for designs of computer experiments, because it guarantees that the estimates of the main effects are uncorrelated. This paper first provides a systematic study on the construction of(nearly) orthogonal strength-three SOAs with better space-filling properties. The newly proposed strength-three SOAs enjoy almost the same space-filling properties of strength-four SOAs, and can accommodate much more columns than the latter. Moreover, they are(nearly) orthogonal and flexible in run sizes. The construction methods are straightforward to implement, and their theoretical supports are well established. In addition to the theoretical results, many designs are tabulated for practical needs.

关键词： Computer experiment orthogonality space-filling property strong orthogonal array

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Investigation on crystallization behavior between(Sc_(x)Yb_(1−x))O_(1.5)and CMAS:A new insight in the effect of Sc substitution

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Journal of Advanced Ceramics 2024年第6期13卷 789-799页

作者： Guangheng Zhang jinyu Shi Jie Zhang Jingyang Wang Shenyang National Laboratory for Materials Science Institute of Metal ResearchChinese Academy of SciencesShenyang 110016China School of Materials Science and Engineering University of Science and Technology of ChinaShenyang 110016China

Environmental barrier coatings(EBCs)with thermomechanical robustness against calcium–magnesium–aluminum–silicate(CMAS)deposits are in high *** aim of this work was to clarify the influence of Sc^(3+)on the crystallization behavior of Yb-based coatings against CMAS *** reaction products of solid solutions with compositions traversing the Sc_(2)O_(3)–Yb_(2)O_(3)system indicate that Sc^(3+)tends to form[BO_(6)]coordination polyhedra in the crystal structure to promote the formation of garnet and diopside,while Yb^(3+)occupies 7-,8-,and 9-coordinate sites to crystallize apatite and *** transformation of crystalline products from apatite/silicocarnotite to garnet/diopside greatly improves the efficiency of CMAS melt consumption and facilitates the prevention of its further penetration and *** on the commonality of cation occupancy in crystallography,an A(CaO+YbO_(1.5))–B(ScO_(1.5)+MgO+AlO_(1.5))–T(SiO_(2))pseudoternary phase diagram is established,which has great potential for describing phase equilibrium in coating-deposit systems and can provide guidance for the compositional design of corrosion-resistant coatings.

关键词： crystallization behavior cation partitioning scandium-ytterbium oxide(Sc_(x)Yb_(1−x))O_(1.5)solid solution calcium-magnesium-aluminum-silicate(CMAS)deposit pseudoternary phase diagram

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ASYMPTOTIC THEORY FOR THE CIRCUIT ENVELOPE ANALYSIS

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Journal of Computational Mathematics 2024年第4期42卷 955-978页

作者： Chunxiong Zheng Xianwei Wen jinyu Zhang Zhenya Zhou College of Mathematics and Systems Science Xinjiang UniversityUrumqi 830046China Department of Mathematical Sciences Tsinghua UniversityBeijing 100084China Empyrean Software Empyrean Technology Co.Ltd.Beijing 100102China

Asymptotic theory for the circuit envelope analysis is developed in this paper.A typical feature of circuit envelope analysis is the existence of two significantly distinct timescales:one is the fast timescale of carrier wave,and the other is the slow timescale of modulation *** first perform pro forma asymptotic analysis for both the driven and autonomous *** resorting to the Floquet theory of periodic operators,we make a rigorous justification for first-order asymptotic *** turns out that these asymptotic results are valid at least on the slow *** speed up the computation of asymptotic approximations,we propose a periodization technique,which renders the possibility of utilizing the NUFFT *** experiments are presented,and the results validate the theoretical findings.

关键词： Asymptotic analysis Circuit envelope analysis Floquet theory Singularly perturbed problem

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Heavier Group 14 Congeners of Metalla-isobenzenes:Access to Metalla-isosilabenzene and Metalla-isogermabenzene by One-Pot Reactions

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Chinese Journal of Chemistry 2024年第10期42卷 1121-1127页

作者： jinyu Zhao Yapeng Cai Xin Yang Hong Zhang Department of Chemistry Xiamen UniversityXiamenFujian 361005China

Metalla-isosilabenzenes and metalla-isogermabenzenes have been successfully synthesized by the formal[5+1]-cycloaddition of diethynylsilane or diethynylgermane with simple metal *** is the first example of a heavier Group 14 metalla-isobenzene isomer bearing a cumulative double bond motif within a *** novel complexes were fully characterized by NMR spectroscopy and single-crystal X-ray diffraction *** stabilization of the cyclic metal-vinylidene complexes has been analyzed using density functional theory(DFT)*** the metalla-isosilabenzenes bearing Si—H bond were treated with the trityl salt as a hydride scavenger,the formation of silylium cation was observed *** of metalla-isosilabenzenes and metalla-isogermabenzenes can readily undergo migratory insertion reactions to furnish siloles or germoles.

关键词： Metalla-isosilabenzene Metalla-isogermabenzene Density functional calculations Cycloaddition Metallacycles

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Distributed Stochastic Scheduling of Massive Backup Batteries in Cellular Networks for Operational Reserve and Frequency Support Ancillary Services

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Journal of Modern Power Systems and Clean Energy 2024年第2期12卷 393-404页

作者： Kun Li Jiakun Fang Xiaomeng Ai Shichang Cui Rongkang Zhao jinyu Wen State Key Laboratory of Advanced Electromagnetic Engineering and Technology School of Electrical and Electronic EngineeringHuazhong University of Science and TechnologyWuhan 430074China IEEE

Base station(BS)backup batteries(BSBBs),with their dispatchable capacity,are potential demand-side resources for future power *** enhance the power supply reliability and post-contingency frequency security of power systems,we propose a two-stage stochastic unit commitment(UC)model incorporating operational reserve and post-contingency frequency support provisions from massive BSBBs in cellular networks,in which the minimum backup energy demand is considered to ensure BS power supply *** energy,operational reserve,and frequency support ancillary services are co-optimized to handle the power balance and post-contingency frequency security in both forecasted and stochastic variable renewable energy(VRE)***,we propose a dedicated and scalable distributed optimization framework to enable autonomous optimizations for both dispatching center(DC)and *** BS model parameters are stored and processed locally,while only the values of BS decision variables are required to upload to DC under the proposed distributed optimization framework,which safeguards BS privacy *** studies on a modified IEEE 14-bus system demonstrate the effectiveness of the proposed method in promoting VRE accommodation,ensuring post-contingency frequency security,enhancing operational economics,and fully utilizing BSBBs'energy and power ***,the proposed distributed optimization framework has been validated to converge to a feasible solution with near-optimal performance within limited ***,numerical results on the Guangdong 500 kV provincial power system in China verify the scalability and practicality of the proposed distributed optimization framework.

关键词： Base station backup battery operational reserve frequency security distributed optimization privacy

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Designing ultrastrong and thermally stable FeCrAl alloys with the fine-grained structure

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Journal of Materials Science & Technology 2024年第4期171卷 198-208页

作者： Shuaiyang Liu jinyu Zhang Hui Wang Gang Liu Xiangdong Ding Jun Sun State Key Laboratory for Mechanical Behavior of Materials Xi’an Jiaotong UniversityXi’an 710049China Science and Technology on Reactor Fuel and Materials Laboratory Nuclear Power Institute of ChinaChengdu 610041China

Designing microstructurally stable FeCrAl alloys with excellent strength-ductility synergy is highly desir-able for their engineering ***,due to the preference nucleation of precipitates at grain boundaries(GBs),the improved precipitation strengthening of these alloys is usually accompanied by in-tergranular ***,we propose a novel thermomechanical processing route coupled with the Si alloying strategy via precipitation of coherent deformable Laves precipitates inside equiaxed fine-grains to achieve FeCrAl alloys with ultrahigh yield strength over∼992 MPa,excellent uniform elongation of∼7.6%at room temperature,and superior thermal stability at temperature∼1200℃.The Si alloying not only decreases the stacking fault energy of Laves precipitates favorable for their stacking-fault-mediated deformation but also hinders grain coarsening at 1200℃due to the Si-enrichment favorable for GB pin-ning *** results prove the possibility of achieving the collaborative enhancement of mutually exclusive properties in alloys,such as strength-ductility-thermal stability via nanoprecipitation engineer-ing,and offer a promising route to prepare dispersion-strengthened materials.

关键词： FeCrAl alloys Si alloying Mechanical properties Thermal stability Laves phase

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On Designs of Decentralized Reputation Management for Permissioned Blockchain Networks

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Computer Modeling in Engineering & Sciences 2024年第5期139卷 1755-1773页

作者： jinyu Chen Long Shi Qisheng Huang Taotao Wang Daojing He School of Electronic and Optical Engineering Nanjing University of Science and TechnologyNanjing210094China School of Mechanical Engineering and Automation Harbin Institute of TechnologyShenzhen518055China College of Electronics and Information Engineering Shenzhen UniversityShenzhen518060China School of Computer Science and Technology Harbin Institute of TechnologyShenzhen518055China

In permissioned blockchain networks,the Proof of Authority(PoA)consensus,which uses the election of authorized nodes to validate transactions and blocks,has beenwidely advocated thanks to its high transaction throughput and fault ***,PoA suffers from the drawback of centralization dominated by a limited number of authorized nodes and the lack of anonymity due to the round-robin block proposal *** a result,traditional PoA is vulnerable to a single point of failure that compromises the security of the blockchain *** address these issues,we propose a novel decentralized reputation management mechanism for permissioned blockchain networks to enhance security,promote liveness,and mitigate centralization while retaining the same throughput as traditional *** paper aims to design an off-chain reputation evaluation and an on-chain reputation-aided ***,we evaluate the nodes’reputation in the context of the blockchain networks and make the reputation globally verifiable through smart ***,building upon traditional PoA,we propose a reputation-aided PoA(rPoA)consensus to enhance securitywithout sacrificing *** particular,rPoA can incentivize nodes to autonomously form committees based on reputation authority,which prevents block generation from being tracked through the randomness of reputation ***,we develop a reputation-aided fork-choice rule for rPoA to promote the network’s ***,experimental results show that the proposed rPoA achieves higher security performance while retaining transaction throughput compared to traditional PoA.

关键词： Blockchain reputation management PoA throughput security decentralization

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A calibration and compensation method for an industrial robot with high accuracy harmonic reducers

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Science China(Technological Sciences) 2024年第3期67卷 725-739页

作者： ZHAO YiYang LIU Xun CAO JiaBin LIU jinyu XU Yan YAN WeiXin School of Mechanical Engineering Shanghai Jiao Tong UniversityShanghai 200240China College of Computer and Control Engineering Northeast Forestry UniversityHarbin 150040China

Industrial serial robots need high stiffness to keep absolute pose accuracy and meet the requirements in practical applications. However, the weak stiffness feature of robot joints and the payloads affected on robot end-effector, which will also increase the pose error of robot. Especially, the existing calibration methods often consider under no-payload condition without discussing the payload state. In this paper, we report a new industrial serial robot composed by a new harmonic reducer: Model-Y, based on high accuracy and high stiffness, and a kinematic parameter calibration algorithm which is based on a harmonic reducer forcedeformation model. To decrease the accuracy effects of payload, an iterative calibration method for kinematic parameters with payload situation was proposed. Simulation and experiments are conducted to verify the effectiveness of the proposed calibration method using the self-developed industrial serial robot. The results show a remarkably improved accuracy in absolute position and orientation with the robot's payload range. The position mean error has 70% decreased to 0.1 mm and the orientation mean error diminished to less than 0.01° after calibration with compensation. Additionally, online linear and circular tests are carried out to evaluate the position error of the robot during large-scale spatial and low-speed continuous movement. The accuracy is consistent with the previous calibration results, indicating the effectiveness and advantages of the proposed strategy in this article.

关键词： industrial serial robot Model-Y harmonic calibration stiffness model online compensation

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Combined effects of sea urchin-like structure and mixed Cu^(+)/Cu^(0)states on promoting C_(2)formation in electrocatalytic CO_(2)reduction

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Frontiers of Chemical Science and Engineering 2024年第3期18卷 63-73页

作者： Mengqing Shan Dongsheng Lu Jiatong Dong Shen Yan jinyu Han Hua Wang Collaborative Innovation Center of Chemical Science and Engineering Key Laboratory for Green Chemical Technology of the Ministry of EducationSchool of Chemical Engineering and TechnologyTianjin UniversityTianjin300354China

Surface engineering and Cu valence regulation are essential factors in improving the C_(2)selectivity during the electrochemical reduction of CO_(2).Herein,we present a sea urchin-like CuO/Cu_(2)O catalyst derived from rhombic dodecahedra Cu_(2)O through one-step oxidation/etching method where the mixed Cu^(+)/Cu^(0)states are formed via in situ reduction during *** combined effects of the morphology and the mixed Cu^(+)/Cu^(0)states on C–C coupling are evaluated by the Faradaic efficiency of C_(2)and the C_(2)/C1 ratio obtained in an H-cell.R-Cu^(O)/Cu_(2)O exhibited 49.5%Faradaic efficiency of C_(2)with a C_(2)/C1 ratio of 3.1 at−1.4 V *** hydrogen electrode,which are 1.5 and 3.2 times higher than those of R-Cu_(2)O,*** a flow-cell,68.0%Faradaic efficiency of C_(2)is achieved at a current density of 500 mA·cm^(−2).The formation of the mixed Cu^(+)/Cu^(0)states was confirmed by in situ Raman ***,the sea urchin-like structure provides more active sites and enables faster electron *** a result,the excellent C_(2)production on R-CuO/Cu_(2)O is primarily attributed to the synergistic effects of the sea urchin-like structure and the stable mixed Cu^(+)/Cu^(0)***,this work presents an integrated strategy for developing Cu-based electrocatalysts for C_(2)production through electrochemical CO_(2)reduction.

关键词： CO_(2)electrolysis sea urchin-like structure Cu^(+)/Cu^(0) C_(2)products

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