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Multifunctional Nacre‑Like Nanocomposite Papers for Electromagnetic Interference Shielding via Heterocyclic Aramid/MXene Template‑Assisted In‑Situ Polypyrrole Assembly

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Nano-Micro Letters 2025年第3期17卷 37-54页

作者： jinhua Xiong Xu Zhao Zonglin Liu He chen Qian Yan Huanxin Lian Yunxiang chen Qingyu Peng Xiaodong He National Key Laboratory of Science and Technology On Advanced Composites in Special Environments Center for Composite Materials and StructuresHarbin Institute of TechnologyHarbin 150080People’s Republic of China

Robust, ultra-flexible, and multifunctional MXene-basedelectromagnetic interference (EMI) shielding nanocomposite filmsexhibit enormous potential for applications in artificial intelligence,wireless telecommunication, and portable/wearable electronic *** this work, a nacre-inspired multifunctional heterocyclic aramid(HA)/MXene@polypyrrole (PPy) (HMP) nanocomposite paper withlarge-scale, high strength, super toughness, and excellent tolerance tocomplex conditions is fabricated through the strategy of HA/MXenehydrogel template-assisted in-situ assembly of PPy. Benefiting from the"brick-and-mortar" layered structure and the strong hydrogen-bondinginteractions among MXene, HA, and PPy, the paper exhibits remarkable mechanical performances, including high tensile strength (309.7 MPa),outstanding toughness (57.6 MJ m−3), exceptional foldability, and structural stability against ultrasonication. By using the template effect ofHA/MXene to guide the assembly of conductive polymers, the synthesized paper obtains excellent electronic conductivity. More importantly,the highly continuous conductive path enables the nanocomposite paper to achieve a splendid EMI shielding effectiveness (EMI SE) of 54.1 dBat an ultra-thin thickness (25.4 μm) and a high specific EMI SE of 17,204.7 dB cm2g−1. In addition, the papers also have excellent applicationsin electromagnetic protection, electro-/photothermal de-icing, thermal therapy, and fire safety. These findings broaden the ideas for developinghigh-performance and multifunctional MXene-based films with enormous application potential in EMI shielding and thermal management.

关键词： MXene Remarkable mechanical properties Heterocyclic aramid Electromagnetic interference shielding Polypyrrole Multifunctionality

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Kangfuxin solution alleviates esophageal stenosis after endoscopic submucosal dissection:A natural ingredient strategy

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World Journal of Gastroenterology 2025年第1期31卷 110-125页

作者： Xin Zhou Dan Ma Yi-Xiang He jing jin Hong-Lian Wang Yun-Feng Wang Fan Yang Jian-Qin Liu Jie chen Zhi Li Department of Spleen and Stomach Diseases the Affiliated Traditional Chinese Medicine HospitalSouthwest Medical UniversityLuzhou 646000Sichuan ProvinceChina The Key Laboratory of Integrated Traditional Chinese and Western Medicine for Prevention and Treatment of Digestive System Diseases of Luzhou City The Affiliated Traditional Medicine HospitalSouthwest Medical UniversityLuzhou 646000Sichuan ProvinceChina Department of Gastroenterology Changhai HospitalNaval Medical UniversityShanghai 20082China Research Center of Integrated Chinese and Western Medicine The Affiliated Traditional Chinese Medicine HospitalSouthwest Medical UniversityLuzhou 646000Sichuan ProvinceChina School of Integrated Traditional Chinese and Western Clinical Medicine North Sichuan Medical CollegeNanchong637100Sichuan ProvinceChina

BACKGROUND Esophageal stricture ranks among the most significant complications following endoscopic submucosal dissection(ESD).Excessive fibrotic repair is a typical pathological feature leading to stenosis after *** To examine the effectiveness and underlying mechanism of Kangfuxin solution(KFX)in mitigating excessive fibrotic repair of the esophagus *** Pigs received KFX at 0.74 mL/kg/d for 21 days after esophageal full circumferential *** examinations occurred on days 7 and 21 *** vitro,recombinant transforming growth factor(TGF)-β1(5 ng/mL)induced a fibrotic microenvironment in primary esophageal fibroblasts(pEsF).After 24 hours of KFX treatment(at 1.5%,1%,and 0.5%),expression ofα-smooth muscle actin-2(ACTA2),fibronectin(FN),and type collagen I was *** signaling was analyzed,including TGF-β1,Smad2/3,and phosphor-smad2/3(p-Smad2/3).RESULTS Compared to the Control group,the groups treated with KFX and prednisolone exhibited reduced esophageal stenosis,lower weight loss rates,and improved food tolerance 21 d after *** treatment,Masson staining revealed thinner and less dense collagen fibers in the submucosal ***,the expression of fibrotic effector molecules was notably ***,KFX downregulated the transduction levels of fibrotic functional molecules such as TGF-β1,Smad2/3,and p-Smad2/*** vitro,pEsF exposed to TGF-β1-induced fibrotic microenvironment displayed increased fibrotic activity,which was reversed by KFX treatment,leading to reduced activation of ACTA2,FN,and collagen *** 1.5%KFX treatment group showed decreased expression of p-Smad 2/3 in TGF-β1-activated *** KFX showed promise as a therapeutic option for post-full circumferential esophageal ESD strictures,potentially by suppressing fibroblast fibrotic activity through modulation of the TGF-β1/Smads signaling pathway.

关键词： Kangfuxin solution Natural component Endoscopic submucosal dissection Esophagus stricture Fibrosis

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Construction of 3D porous Cu_(1.81)S/nitrogen-doped carbon frameworks for ultrafast and long-cycle life sodium-ion storage

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International Journal of Minerals,Metallurgy and Materials 2025年第1期32卷 191-200页

作者： chen chen Hongyu Xue Qilin Hu Mengfan Wang Pan Shang Ziyan Liu Tao Peng Deyang Zhang Yongsong Luo Key Laboratory of Microelectronics and Energy of Henan Province Henan Joint International Research Laboratory of New Energy Storage TechnologyCollege of Physics and Electronic EngineeringXinyang Normal UniversityXinyang 464000China School of Physics and Electronic Engineering Nanyang Normal UniversityNanyang 473061China

Transition metal sulfides have great potential as anode mterials for sodium-ion batteries(SIBs)due to their high theoretical specific ***,the inferior intrinsic conductivity and large volume variation during sodiation-desodiation processes seriously affect its high-rate and long-cyde performance,unbeneficial for the application as fast-charging and long-cycling SIBs ***,the three-dimensional porous Cu_(1.81)S/nitrogen-doped carbon frameworks(Cu_(1.81)S/NC)are synthesized by the simple and facile sol-gel and annealing processes,which can accommodate the volumetric expansion of Cu_(1.81)S nanoparticles and accelerate the transmission of ions and electrons during Na^(+)insertion/extraction processes,exhibiting the excellent rate capability(250.6 mA·g^(-1)at 20.0 A·g^(-1))and outstanding cycling stability(70% capacity retention for 6000 cycles at 10.0 A·g^(-1))for ***,the Na-ion full cells coupled with Na_(3)V_(2)(PO_(4))_(3)/C cathode also demonstrate the satisfactory reversible specific capacity of 330.5 mAh·g^(-1)at 5.0 A·g^(-1)and long-cycle performance with the 86.9% capacity retention at 2.0 A·g^(-1)after 750 *** work proposes a promising way for the conversionbased metal sulfides for the applications as fast-charging sodium-ion battery anode.

关键词： copper sulfide nanoparticles porous carbon framework fast charging long-cycle performance sodium-ion full batteries

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On the ionospheric response in the Taiwan region to Typhoon Meranti in September 2016

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Geodesy and Geodynamics 2025年第1期16卷 29-41页

作者： Peng chen Mingzhu Xiong Yibin Yao Hao chen Fucai Tang Liangcai Qiu Yuchen Zhang College of Geomatics Xi'an University of Science and Technology State Key Laboratory of Geodesy and Earth's Dynamics Innovation Academy for Precision Measurement Science and Technology Chinese Academy of Science School of Geodesy and Geomatics Wuhan University Key Laboratory of Geospace Environment and Geodesy Ministry of Education Wuhan University

Previous studies have revealed that typhoons can affect the ionosphere. This paper uses GNSS observations provided by GNSS tracking stations of Taiwan region, ERA5 gravity wave dissipation products,and Himawari-8 band 07 brightness temperature observation data to analyze the impact of Typhoon Meranti on Taiwan region's ionosphere from September 13 to 15, 2016. In addition to the daily effects of traveling ionospheric disturbances(TIDs), TIDs of various intensities caused by Meranti-induced gravity waves were observed during this period, which is inseparable from the state of the typhoon and the topographic features during its progress. The ionospheric disturbance caused by the edge of a typhoon is usually larger than that at the typhoon eye. When the typhoon approached Taiwan region with high intensity on September 14, it was observed that the gravity waves caused by the typhoon had a wavelength of about 174-293 km, a period of 13.5-23.5 min, and a propagation speed of 142-302 m/s. When the vortex structure of a typhoon interacts with complex surfaces such as mountains, it is easier to excite more medium-scale gravity waves. The origin that excites gravity waves and causes ionospheric anomalies is different from the location of the typhoon eye and changes over time. The gravity waves caused by the typhoon lasted for three days in the central mountains of Taiwan region. Still, background wind conditions restricted the propagation of gravity waves from the mesosphere to the thermosphere and led to TID predominantly concentrated between 06:00 and 13:00 UT each day.

关键词： Typhoon GNSS TEC TID Gravity waves

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Detection and interpretation of the time-varying seasonal signals in China with multi-geodetic measurements

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Geodesy and Geodynamics 2025年第1期16卷 42-54页

作者： Liansheng Deng Yugang Xiao Qusen chen Wei Peng Zhao Li Hua chen Zhiwen Wu School of Electrical and Electronic Information Engineering Hubei Polytechnic University Hubei Luojia Laboratory GNSS Research Center Wuhan University Changjiang Spatial Information Technology Engineering Co. Ltd. Key Laboratory of Spatial Data Mining & Information Sharing of the Ministry of Education Fuzhou University School of Geodesy and Geomatics Wuhan University The First Surveying and Mapping Institute of Hunan Province

The time-varying periodic variations in Global Navigation Satellite System(GNSS) stations affect the reliable time series analysis and appropriate geophysical interpretation. In this study, we apply the singular spectrum analysis(SSA) method to characterize and interpret the periodic patterns of GNSS deformations in China using multiple geodetic datasets. These include 23-year observations from the Crustal Movement Observation Network of China(CMONOC), displacements inferred from the Gravity Recovery and Climate Experiment(GRACE), and loadings derived from Geophysical models(GM). The results reveal that all CMONOC time series exhibit seasonal signals characterized by amplitude and phase modulations, and the SSA method outperforms the traditional least squares fitting(LSF) method in extracting and interpreting the time-varying seasonal signals from the original time series. The decrease in the root mean square(RMS) correlates well with the annual cycle variance estimated by the SSA method, and the average reduction in noise amplitudes is nearly twice as much for SSA filtered results compared with those from the LSF method. With SSA analysis,the time-varying seasonal signals for all the selected stations can be identified in the reconstructed components corresponding to the first ten eigenvalues. Moreover, both RMS reduction and correlation analysis imply the advantages of GRACE solutions in explaining the GNSS periodic variations,and the geophysical effects can account for 71% of the GNSS annual amplitudes, and the average RMS reduction is 15%. The SSA method has proved to be useful for investigating the GNSS timevarying seasonal signals. It could be applicable as an auxiliary tool in the improvement of nonlinear variations investigations.

关键词： GNSS coordinate time series Singular spectrum analysis Time-varying seasonal signals Loading effects GRACE

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Vinyl flanked amorphous conjugated polymer by Knoevenagel condensation of diketopyrrolopyrrole and indacenodithiophene for flexible transistor

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Science China Materials 2025年第1期68卷 110-116页

作者： Yanlin chen Pinyu chen Shihong Zhou Zhiwei Yang Haijun long Xianfeng Liang Tianwen chen jing Li Luxi Tan Haoli Zhang Lichun Dong Zitong Liu School of Chemistry and Chemical Engineering Chongqing UniversityChongqing 401331China State Key Laboratory of Applied Organic Chemistry(SKLAOC) Key Laboratory of Special Function Materials and Structure Design(MOE)College of Chemistry and Chemical EngineeringLanzhou UniversityLanzhou 730000China Chongqing Institute of Green and Intelligent Technology Chinese Academy of SciencesChongqing 400714China

Conjugated polymers exhibit exceptional adaptability in flexible thin-film transistors,owing to their inherent flexibility and high charge ***,achieving conjugated polymers that demonstrate both high mobility and stability under mechanical stress,such as bending or stretching,remains a significant *** this study,we synthesized an ethylene-bridged conjugated polymer,PDPPVIDT,derived from methyl-side diketopyrrolopyrrole(DPP)and indacenodithiophene(IDT)aldehydes,using an environmentally friendly Knoevenagel condensation reaction under mild conditions,resulting in a moderate yield with promising *** characterization techniques revealed enhanced backbone planarity with stableπ-πstacking,while thin films of PDPPVIDT displayed a nearamorphous nature due to the conformational isomerism of the ethylene *** structure enables simultaneous charge transport and ***,flexible organic thinfilm transistor(OTFT)devices based on PDPPVIDT demonstrated excellent hole mobility(μh)reaching up to 1.70 cm^(2) V^(−1) s^(−1),along with high mechanical bending *** work underscores the potential of vinyl-bridged donor-acceptor conjugated polymers,highlighting the industrial adaptability of their production process and offering new insights for the design and synthesis of future flexible electronic materials.

关键词： D-A conjugated polymers diketopyrrolopyrrole flexible thin-film transistors indacenodithiophene Knoevenagel condensation

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Beyond Performance of Learning Control Subject to Uncertainties and Noise: A Frequency-Domain Approach Applied to Wafer Stages

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IEEE/CAA Journal of Automatica Sinica 2025年第1期12卷 198-214页

作者： Fazhi Song Ning Cui Shuaiqi chen Kai Zhang Yang Liu Xinkai chen Jiubin Tan IEEE the Center of Ultra-precision Optoelectronic Instrument Engineering Harbin Institute of Technology the Key Laboratory of Ultra-Precision Intelligent Instrumentation Ministry of Industry and Information Technology the State Key Laboratory of Precision Electronic Manufacturing Technology and Equipment Guangdong University of Technology the Center of Ultraprecision Optoelectronic Instrument Engineering Harbin Institute of Technology the Key Laboratory of UltraPrecision Intelligent Instrumentation Ministry of Industry and Information Technology the Department of Electronic and Information Systems Shibaura Institute of Technology

The increasingly stringent performance requirement in integrated circuit manufacturing, characterized by smaller feature sizes and higher productivity, necessitates the wafer stage executing a extreme motion with the accuracy in terms of nanometers. This demanding requirement witnesses a widespread application of iterative learning control(ILC), given the repetitive nature of wafer scanning. ILC enables substantial performance improvement by using past measurement data in combination with the system model knowledge. However, challenges arise in cases where the data is contaminated by the stochastic noise, or when the system model exhibits significant uncertainties, constraining the achievable performance. In response to this issue, an extended state observer(ESO) based adaptive ILC approach is proposed in the frequency *** being model-based, it utilizes only a rough system model and then compensates for the resulting model uncertainties using an ESO, thereby achieving high robustness against uncertainties with minimal modeling effort. Additionally, an adaptive learning law is developed to mitigate the limited performance in the presence of stochastic noise, yielding high convergence accuracy yet without compromising convergence speed. Simulation and experimental comparisons with existing model-based and data-driven inversion-based ILC validate the effectiveness as well as the superiority of the proposed method.

关键词： Extended state observer learning control model uncertainties motion control stochastic noise

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Accurate visualization colorectal cancer by monitoring viscosity variations with a novel mitochondria-targeted fluorescent probe

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Chinese Chemical Letters 2025年第2期36卷 319-322页

作者： Fan Zheng Runsha Xiao Shuai Huang Zhikang chen chen Lai Anyao Bi Heying Yao Xueping Feng Zihua chen Wenbin Zeng Xiangya School of Pharmaceutical Sciences Central South University Hunan Key Laboratory of Diagnostic and Therapeutic Drug Research for Chronic Diseases Central South University Department of General Surgery Xiangya Hospital Central South University Hunan Key Laboratory of Precise Diagnosis and Treatment of Gastrointestinal Tumor Xiangya Hospital Central South University National Clinical Research Center for Geriatric Disorders Xiangya Hospital Central South University Department of Oncology Xiangya Hospital Central South University Department of Otolaryngology-head and Neck Surgery and Institute of Medical Sciences Xiangya Hospital Central South University

Colorectal cancer(CRC) is one of the most prevalent malignant tumors worldwide, exhibiting high morbidity and mortality. Lack of efficient tools for early diagnosis and surgical resection guidance of CRC have been a serious threat to the long-term survival rate of the CRC patients. Recent studies have shown that relative higher viscosity was presented in tumor cells compared to that in normal cells, leading to viscosity as a potential biomarker for CRC. Herein, we reported the development of a series of novel viscosity-sensitive and mitochondria-specific fluorescent probes(HTB, HTI, and HTP) for CRC *** them, HTB showed high sensitivity, minimal background interference, low cytotoxicity, and significant viscous response capability, making it an ideal tool for distinguishing colorectal tumor cells from normal cells. Importantly, we have successfully utilized HTB to visualize in a CRC-cells-derived xenograft(CDX) model, enriching its medical imaging capacity, which laid a foundation for further clinical translational application.

关键词： Bioimaging Cancer diagnosis Colorectal cancer Fluorescent probe Mitochondrial-targeted Viscosity

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Miyaoka-type inequalities for terminal threefolds with nef anti-canonical divisors

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Science China Mathematics 2025年第1期68卷 1-18页

作者： Masataka Iwai chen Jiang Haidong Liu Department of Mathematics Graduate School of ScienceOsaka UniversityOsaka 560-0043Japan Shanghai Center for Mathematical Sciences&School of Mathematical Sciences Fudan UniversityShanghai 200438China Department of mathematics Sun Yat-sen UniversityGuangzhou 510275China

In this paper,we study Miyaoka-type inequalities on Chern classes of terminal projective 3-folds with nef anti-canonical *** X be a terminal projective 3-fold such that-KX is *** show that if c_(1)(X)·c_(2)(X)≠0,then c_(1)(X)·c_(2)(X)≥1/252;if further X is not rationally connected,then c_(1)(X)·c_(2)(X)≥4/5 and this inequality is *** order to prove this,we give a partial classification of such varieties along with many *** also study the nonvanishing of c_(1)(X)^(dim X-2)·c_(2)(X)for terminal weak Fano varieties and prove a Miyaoka-Kawamata-type inequality.

关键词： terminal threefolds Miyaoka-type inequality boundedness

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Computational Insights into the Interactions of Farnesoid X Receptor with Fargesone A,a Natural Product from Magnolia fargesii

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Chemical Research in Chinese Universities 2025年第1期41卷 146-154页

作者： ZHANG Li chen Yaqiong LI Weihua School of Pharmacy Shanghai Key Laboratory of Molecular ImagingShanghai University of Medicine and Health SciencesShanghai201318P.R.China School of Pharmacy East China University of Science and TechnologyShanghai200237P.R.China

Farnesoid X receptor(FXR)is a ligand-activated nuclear receptor and plays important roles in the regulation of metabolism and homeostasis of several important physiological substances,such as bile acids,glucose,and *** such,FXR has become a promising therapeutic target for the treatment of several metabolic diseases and liver ***,fargesone A(FA),a natural product from Magnolia fargesii was identified to be a novel,potent FXR agonist that demonstrated good in vitro and in vivo ***,the detailed interaction mechanism of FA with FXR remains *** this study,we employed multiple computational approaches including molecular docking,molecular dynamics simulation,and binding free energy calculation to address the *** comparisons of the structural dynamics and binding free energies,an optimal binding mode was identified,in which FA interacts with FXR via a direct hydrogen bond with His447 and hydrophobic interactions with multiple residues,such as Leu287,Met290,Met328,Ile352,and *** mutants,namely,H447F and L287N,were further constructed to validate the importance of the identified *** anticipate that these findings could be helpful for future rational design of new FA analogues targeting FXR.

关键词： Farnesoid X receptor(FXR) Binding mode Molecular docking Molecular dynamics Fargesone A

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