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Thickening progression mechanism of silica fume-oil well cement composite system at high temperatures

Petroleum Science 2024年第4期21卷 2793-2805页

作者： Hang Zhang Miao-Miao Hu Peng-Peng Li guo-Qing Liu Qing-Lu Chang Jie Cao Ming Liu Wen-Hua Xu Xiu-Jian Xia jin-tang guo School of Chemical Engineering and Technology Tianjin UniversityTianjin300350China Zhejiang Institute of Tianjin University Shaoxing312300ZhejiangChina Haihe Laboratory of Sustainable Chemical Transformations Tianjin300192China CNPC Engineering Technology R&D Company Limited Beijing102206China

This work studied the thickening progression mechanism of the silica fume-oil well cement composite system at high temperatures(110-180.C)in order to provide a theoretical guidance for the rational application of silica fume in the cementing *** showed that silica fume seldom affected the thickening progression of oil well cement slurry at 110-120.C,but when temperature reached above130.C,it would aggravate the bulging degree of thickening curves and significantly extend the thickening time,meanwhile causing the abnormal“temperature-based thickening time reversal”and“dosage-based thickening time reversal”phenomena in the range of 130-160.C and 170-180.C *** 130-160.C,the thickening time of oil well cement slurry was mainly associated with the generation rate of calcium hydroxide(CH)*** introduced silica fume would be attracted to the cement minerals'surface that were hydrating to produce CH and agglomerate together to form an“adsorptive barrier”to hinder further hydration of the inner cement ***“adsorptive barrier”effect strengthened with the rising temperature which extended the thickening time and caused the occurrence of the“temperature-based thickening time reversal”*** 170-180.C,the pozzolanic activity of silica fume significantly enhanced and considerable amount of C-S-H was generated,thus the“temperature-based thickening time reversal”vanished and the“dosage-based thickening time reversal”was presented.

关键词： Silica fume Oil well cement Thickening time reversal Pozzolanic reaction Adsorptive barrier CH and C-S-H

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Storage Stability of Alpha-Lipoic Acid-loaded Lipid Nanoparticles

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过程工程学报 2010年第2期10卷 332-338页

作者：唐金国夏强刘光煜 State Key Laboratory of Bioelectronics Southeast UniversityNanjingJiangsu 210096China Suzhou Key Laboratory of Biomedical Materials and Technology SuzhouJiangsu 215123China 3.Suzhou Nanohealth Biotech Co.Ltd. SuzhouJiangsu 215123China Suzhou Nanohealth Biotech Co.Ltd. SuzhouJiangsu 215123China

Alpha-lipoic acid-loaded lipid nanoparticles(ALA-LNs) were prepared by high pressure homogenization *** influences of storage conditions such as time and temperature on the physical and chemical storage stability of ALA-LNs were studied in *** stability was evaluated by particle size and polydispersity index,morphology of ALA-LNs,and capacity of ALA *** dilution and pH stability of ALA-LNs suspensions were also *** three months storage,the mean size of ALA-LNs at 4 and 40 ℃ was increased by 2.68% and 3.62% compared with the original size,***-LNs stored at 40 ℃ had ellipsoid shape and the mean size was about 152 nm(SD=23.6).The loading capacity of ALA at 40 ℃ was much higher than those stored at other two *** good dilution and pH stability were also *** sample had good fluidity even at 4 ℃.

关键词： alpha-lipoic acid lipid nanoparticles storage stability particle size particle morphology

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Synergistic effect of bonding heterogeneity and phonon localization in introducing excellent thermoelectric properties in layered heteroanionic NdZnSbO material

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Journal of Energy Chemistry 2025年第1期100卷 259-272页

作者： Da Wan Shuwei tang Shulin Bai Xiaodong Li Peng Ai Wanrong guo Tuo Zheng College of Materials Science and Engineering Liaoning Technical University Faculty of Chemistry Northeast Normal University

Layered rare-earth metal oxides, harnessing the dual properties of oxides and two-dimensional layered materials, exhibit remarkable thermal stability and quantum confinement effects. Therefore, this work adopts the first-principles calculation combined with the Boltzmann transport theory to predict the thermoelectric properties of NdZnSbO compound. The coexistence of weak interlayer van der Waals interactions, robust intralayer ionic bonding, and partial covalent bonding leads to remarkable bonding heterogeneity, which engenders pronounced phonon scattering and imposes constraints on thermal transport along the out-of-plane direction. The weakened chemical bonds induced by the antibonding states, together with the rattling-like behavior of the Zn atom, culminate in the profound anharmonicity in the layered NdZnSbO compound. The weakening bond and heavy element contribute to the softness of phonon modes, which significantly diminishes the phonon group velocity. The redistribution-dominated four-phonon scattering process spans a large optical gap, which effectively reduces the lattice thermal conductivity. The NdZnSbO compound exhibits direct semiconductor characteristic with a bandgap of 0.73 e V by adopting the Heyd-Scuseria-Ernzerhof(HSE06) functional in combination with spin–orbit coupling(SOC) effect. The multi-valley feature of NdZnSbO compound augur favorably for band degeneracy, thus amplifying the power factor. Consequently, an optimal figure-of-merit(ZT) of 3.40 at 900 K is achieved for the n-type NdZnSbO compound. The present study delves deeply insights into the origins for the low thermal conductivity of NdZnSbO compound and proposes an optimization scheme to enhance overall thermoelectric performance.

关键词： Bond strength (chemical)

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CaH2-promoted activity of Ni-carbonate interface for CO2 methanation

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Journal of Energy Chemistry 2025年第1期100卷 522-532页

作者： jin-Peng Wang guo-Cui Mao Hui-Lin Jiang Bao-Xia Dong Yun-Lei Teng School of Chemistry and Chemical Engineering Yangzhou University

Transition metal-carbonate interfaces often act as active sites in heterogeneous catalytic *** interface between transition metal and metal carbonate exhibits a dynamic equilibrium during the CO2hydrogenation reaction,involving surface carbonate hydrogenation and ***,there have been few reports on engineering the activity of the interface between transition metal and alkaline earth metal carbonate for catalytic *** work demonstrated that the incorporation of CaH2in Ni/CaCO3enhances the CO2methanation activity of the *** CO2conversion for Ni/CaH2-CaCO3reached 68.5%at 400°C,which was much higher than that of the Ni/CaCO3（31.6%） and Ni/CaH2-CaO （42.4%） ***,the Ni/CaH2-CaCO3catalysts remained stable during the stability test for 24 h at 400°C and 8 *** research revealed that CaH2played a crucial role in promoting the activity of the Ni-carbonate interface for ***2could modify the electronic structure of Ni and tune the structural properties of CaCO3to generate medium basic sites （OH groups）,which are favorable for the activation of H2and ***-situ Fourier transform infrared spectroscopy （FTIR） analysis combined with density functional theory calculations demonstrated that CO2activation occurs at the hydroxyl group （OH） on the CaH2-modified Ni-carbonate surface,leading to the formation of CO3H****,our study has confirmed that CO2methanation over the Ni/CaH2-CaCO3catalysts proceeds via the formate pathway.

关键词： Metal hydride Ni catalysts Carbonate Metal-carbonate interface

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Amino acid assisted aqueous synthesis of highly stable CsPbBr_(3)nanocrystals for cell imaging

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Nano Research 2025年第1期18卷 675-683页

作者： Xue Li Yanan guo guoying Tan Qingyi Liu Nan Song Yu tang State Key Laboratory of Applied Organic Chemistry Key Laboratory of Nonferrous Metal Chemistry and Resources Utilization of Gansu ProvinceCollege of Chemistry and Chemical EngineeringLanzhou UniversityLanzhou 730000China State Key Laboratory of Baiyunobo Rare Earth Resource Researches and Comprehensive Utilization Baotou Research Institute of Rare EarthsBaotou 014030China

Lead halide perovskite nanocrystals(NCs)exhibit excellent optoelectronic performance and have drawn great interests in the fields of biological imaging and ***,the poor stability of CsPbX_(3)(X=Cl,Br,I)in water is still a challenge to hinder their practical *** this work,a facile strategy has been developed for aqueous synthesis of CsPbX_(3) nanocrystals,in which L-glutamic acid(LGlu)has been used to replace oleic acid in the synthetic *** from the synergic effects of L-Glu and oleylamine(OAm),CsPbBr_(3)nanocrystals(L-Glu/OAm-CsPbBr_(3)NCs)with high water stability have been directly prepared under a mild condition at room temperature in water,facilitated by the process of crystal phase transformation from Cs_(4)PbBr_(6) to CsPbBr_(3).L-Glu/OAm-CsPbBr_(3)NCs exhibit a high quantum yield of 85%and a narrow full width at half maximum of 16 nm,demonstrating their efficient luminescence in ***,L-Glu on the surface have contributed greatly to an acidic environment and passivation of surface defects,improving the water stability and dispersibility of CsPbBr_(3)***,L-Glu/OAm-CsPbBr_(3)NCs exhibit great biocompatibility due to the presence of L-Glu,resulting in their good performance for HeLa cell ***,we propose a facile and effective method to prepare CsPbBr_(3)nanocrystals with excellent water stability by using L-Glu and OAm as cooperated ligands and expand their application in cell imaging.

关键词： aqueous synthesis cell imaging lead halide perovskite nanocrystals L-glutamic acid phase transformation

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C^3I/M&S互操作性研究

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指挥控制与仿真 2010年第2期32卷 1-5,10页

作者：唐金国海军航空工程学院科研部山东烟台264001

结合C^3I/M&S互操作性的主要问题,总结了互操作性技术参考模型,在此基础上对C^3I/M&S互操作性的数据模型及标准、接口标准进行了详细论述,介绍了北约C3I/SIM互操作性试验情况,并指出了未来C^3I/M&S互操作性研究的发展趋势,对军队C3I系... 详细信息

结合C^3I/M&S互操作性的主要问题,总结了互操作性技术参考模型,在此基础上对C^3I/M&S互操作性的数据模型及标准、接口标准进行了详细论述,介绍了北约C3I/SIM互操作性试验情况,并指出了未来C^3I/M&S互操作性研究的发展趋势,对军队C3I系统和仿真系统的建设有一定的指导意义。

关键词： C3I 建模与仿真互操作性技术参考模型接口标准数据模型

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Sky location of massive black hole binaries in the foreground of Galactic white dwarf binaries

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Science China(Physics,Mechanics & Astronomy) 2025年第1期Mechanics & Astronomy) .卷 97-108页

作者： Pan guo Hong-Bo jin Cong-Feng Qiao Yue-Liang Wu The International Centre for Theoretical Physics Asia-Pacific University of Chinese Academy of Sciences The School of Physical Sciences University of Chinese Academy of Sciences Institute for Frontiers in Astronomy and Astrophysics Beijing Normal University National Astronomical Observatories Chinese Academy of Sciences Institute of Theoretical Physics Chinese Academy of Sciences

For space-based gravitational wave （GW） detection,the main noise source for massive black hole binaries （MBHBs） is attributed to approximately 10～7double white dwarf binaries in the *** a GW source,the amplitude of the detector response,recorded by a space-based gravitational wave detector,exhibits a modulation effect with a year period when observing the source from various orbital *** the adverse conditions mentioned above,where there is a strong foreground noise and annual modulation in the signals,we employed the wavelet transform and the strong-amplitude relevant orbital position search methods,which allows the weak MBHB sources to achieve higher locating *** detail,for two MBHB sources of lower intensity,the precision of luminosity distance,represented by the ratio ?DL/DLat the 95%confidence level,is enhanced by factors of ～*** angular resolutions,denoted by??s,are enhanced by a factor of ～*** improvements increase the number of detectable GW sources,facilitate multi-messenger follow-up observations and provide constraints on the cosmological constant.

关键词： space-based gravitational wave detection gravitational waves massive black hole binaries

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作战管理语言及其发展现状

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指挥控制与仿真 2008年第5期30卷 9-12页

作者：唐金国海军航空工程学院山东烟台264001

介绍了国外作战管理语言研究领域的发展现状,详细阐述了作战管理语言的定义、构想及其服务体系结构的验证。探讨作战管理语言的体系、信息内容和结构规范、信息交换机制规范及技术验证。最后强调该研究对我军的重要借鉴作用。

关键词：作战管理语言 C2信息交换数据模型 C2和模拟系统互用性

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心房纤颤心室率对心力衰竭患者血清NT-proBNP浓度的影响

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检验医学与临床 2012年第2期9卷 179-180,182页

作者：唐金国重庆市渝北区人民医院心血管内科 401120

目的探讨心房纤颤(简称房颤)心室率对心力衰竭患者血清N-端脑利钠肽前体(NT-proBNP)浓度的影响。方法入选101例心力衰竭患者,按心电图诊断分为快速型房颤组(心室率大于100次/分,n=33)、普通型房颤组(心室率60～100次/分,n=32)和窦性心律... 详细信息

目的探讨心房纤颤(简称房颤)心室率对心力衰竭患者血清N-端脑利钠肽前体(NT-proBNP)浓度的影响。方法入选101例心力衰竭患者,按心电图诊断分为快速型房颤组(心室率大于100次/分,n=33)、普通型房颤组(心室率60～100次/分,n=32)和窦性心律组(n=36),再按纽约心脏病协会(NYHA)心功能分级标准分为心功能Ⅱ、Ⅲ和Ⅳ级3个亚组。采用胶体金法检测受试者血清NT-proBNP浓度并进行统计学分析。结果快速型房颤组、普通型房颤组及窦性心律组患者血清NT-proBNP浓度随NYHA心功能分级增加呈增高趋势,每组各亚组间比较差异有统计学意义(P0.05)。在相同心功能分级亚组,快速型房颤组患者血清NT-proBNP浓度显著高于窦性心律组和普通型房颤组(P0.05)。结论血清NT-proBNP浓度与心力衰竭严重程度相关;房颤对心力衰竭患者血清NT-proBNP浓度有一定影响,房颤心室率增快(超过100次/分)对血清NT-proBNP浓度影响越明显。

关键词：心力衰竭心房纤颤 N-端脑利钠肽前体

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基于属性的舰载机航材备件品种确定方法

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火力与指挥控制 2015年第7期40卷 87-91页

作者：张帅唐金国俞金松张昀申海军航空工程学院解放军92941部队

航材备件品种确定是舰载机供应保障工作的重要内容。基于属性对舰载机航材备件品种确定进行研究。基于粗糙集理论对属性集进行属性约简,确定航材备件品种确定的主要影响属性,然后基于属性约简进行航材备件品种确定。给出了单属性、顺次... 详细信息

航材备件品种确定是舰载机供应保障工作的重要内容。基于属性对舰载机航材备件品种确定进行研究。基于粗糙集理论对属性集进行属性约简,确定航材备件品种确定的主要影响属性,然后基于属性约简进行航材备件品种确定。给出了单属性、顺次属性和多属性的品种决策方法。最后结合实例进行了应用分析。

关键词：航材备件品种属性粗糙集模糊层次分析法模糊综合评判

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