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Preparation and Performance of Ternary Early Strength Agent and Quercetin Composite Cement Sealing Material

Journal of Wuhan University of Technology(Materials Science) 2025年第1期40卷 130-140页

作者： LIU jian ChEN Meiting JI Xiaoli XU Chao Wang Chunmei Department of Safety Science and Engineering Anhui University of Science and TechnologyHuainan 232001China Key Laboratory of Mine Safety and high Efficient Mining Jointly Built by Province and Education Ministry Anhui University of Science and TechnologyHuainan 232001China Department of Chemical Engineering and Explosives Anhui University of Science and TechnologyHuainan 232001China

A ternary early-strengthening agent consisting of calcium formate+triethanolamine+lithium sulfate was compounded with quercetin to shorten the setting time of cementitious materials while ensuring their early *** optimum ratio of the three early-strengthening agents was determined as 0.5%calcium formate+0.04%triethanolamine+0.4%lithium sulfate by response surface *** effects of the ternary early-strengthening agent composed of calcium formate+triethanolamine(TEA)+lithium sulfate on cementitious pore sealing materials under the synergistic effect of quercetin were studied by means of the performance tests of compressive strength,fluidity,and setting time,and the microstructural characterizations of X-ray powder diffractometer(XRD),thermogravimetry(TG-DSC)and scanning electron microscopy(SEM).The study shows that the synergistic effect of ternary early-strengthening agent and quercetin forms a multi-performance composite admixture for cementitious *** best performance was obtained with the compounding scheme of 0.5%calcium formate+0.04%triethanolamine+0.4%lithium sulfate ternary early-strengthening agent and 0.05%*** compressive strength of 1,3,7,and 28 d are 94.8%,39.8%,42%,and 28%higher than those of the blank group,*** initial time and final setting time are 41 and 57 minutes,*** to the microscopic analysis,the network and fibrous C-S-h gels generated by ternary early-strengthening agents are attached to the surface promoted by quercetin,which forms skeleton support while thickening and solidifying the cement slurry,which enhances the early compressive strength of the cement-based materials.

关键词： sealing material ternary early-strengthening agent quercetin synergetic effect response surface methodology

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The Mechanism of heating Rate on the Secondary Recrystallization Evolution in Grain Oriented Silicon Steel

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Journal of Wuhan University of Technology(Materials Science) 2025年第1期40卷 275-282页

作者： GAO Qian LI Jun Wang Xianhui CAO Laifu GONG jian LI Bo Central Iron and Steel Research Institute Group Beijing 100081China Shougang Zhixin Electromagnetic Material R&D(Beijing)Co. Ltd.Beijing 101300China Beijing Shougang Co. Ltd.Qian’an 064404China

Grain-oriented silicon steels were prepared at different heating rates during high temperature annealing,in which the evolution of magnetic properties,grain orientations and precipitates were *** illustrate the Zener factor,the diameter and number density of precipitates of interrupted testing samples were statistically *** effect of precipitate ripening on the Goss texture and magnetic property was *** indicated that the trend of Zener factor was similar under different heating rates,first increasing and then decreasing,and that the precipitate maturing was greatly inhibited as the heating rate *** recrystallization was developed at the temperature of 1010℃when a heating rate of 5℃/h was used,resulting in Goss,Brass and{110}oriented grains growing abnormally and a magnetic induction intensity of ***,increasing the heating rate to 20℃/h would inhibit the development of undesirable oriented grains and obtain a sharp Goss ***,when the heating rate was extremely fast,such as 40℃/h,poor secondary recrystallization was developed with many island grains,corresponding to a decrease in magnetic induction intensity to 1.87 *** a suitable heating rate of 20℃/h,the sharpest Goss texture and the highest magnetic induction of 1.94 T with an onset secondary recrystallization temperature of 1020℃were found among the experimental variables in this *** heating rate affected the initial temperature of secondary recrystallization by controlling the maturation of precipitates,leading to the deviation and dispersion of Goss texture,thereby reducing the magnetic properties.

关键词： high temperature annealing heating rate secondary recrystallization grain oriented silicon steel

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Separate Control of high Frequency Electro-hydraulic Vibration Exciter

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Chinese Journal of Mechanical Engineering 2011年第2期24卷 293-302页

作者： JIA Wen＇ang RUAN jian REN Yan The Key Laboratory of Mechanical Manufacture and Automation of Ministry of Education Zhejiang University of Technology Hangzhou 310032 China

The working frequency of the conventional electro-hydraulic vibration exciters,which consist of a servo valve and a hydraulic cylinder,is generally restricted within a narrow range due to limited frequency response capability of the servo valve *** counteract such restriction,a novel scheme for an electro-hydraulic vibrator,controlled by a two-dimensional valve（2D valve） and a bias valve in parallel,is therefore *** frequency,amplitude and offset are independently controlled by rotary speed,axial sliding of the spool of the 2D valve and axial sliding of the spool of the bias *** principle of separate control was presented and the regulation approach of frequency,amplitude and offset was discussed.A mathematical model of the hydraulic power mechanism for the proposed vibration exciter was established to investigate the relationship between the amplitude and the axial sliding of the 2D valve＇ spool,as well as that between the offset and the axial sliding of the bias valve＇s spool at various *** experimental system was built to validate the theoretical *** is verified that the 2D exciter is capable of working smoothly in a frequency range of 5- 200 *** its frequency,amplitude and offset can be controlled respectively by either closed loop or open loop *** is a linear relationship between the output amplitude and the spool axial opening of the 2D valve until a point when the flow rate becomes saturate and the amplitude remains *** offset displacement of the cylinder＇s piston is linearly proportional to the axial displacement of the spool of the bias valve,when the valve opening is less than 25%.Thereafter,the slop of the offset curve decreases and tends to *** proposed electro-hydraulic vibration controlled by the 2D valve not only facilitates the realization of high-frequency electro-hydraulic vibration,the high-accuracy of vibration can also be achieved by means of independent controls to the freque

关键词： control valves electro-hydraulic system vibration exciter dynamics characteristics

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Output Waveform Analysis of an Electro-hydraulic Vibrator Controlled by the Multiple Valves

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Chinese Journal of Mechanical Engineering 2014年第1期27卷 186-197页

作者： REN Yan RUAN jian JIA Wen'ang College of Mechanical & Electrical Engineering Wenzhou University Key Laboratory of Special Purpose Equipment and Advanced Machining Technology Ministry of Education & Zhejiang Province Zhejiang University of Technology

The existing research of the electro-hydraulic vibrator mainly focuses on system stability, working frequency width and output waveform distortion. however, this high frequency performance of the electro-hydraulic vibrator is difficult to be improved greatly due to fast insufficiently frequency response of the servo valve itself and limited compensation capability of the control structure in the vibrator system. In this paper, to realize high frequency vibration, an improved two-dimensional valve （here within defined as a 2D valve） as a main control component is adopted to the parallel connection with a servo valve to control the electro-hydraulic vibrator, Because the output waveforms of this electro-hydraulic vibrator are incapable to be verified through timely feedback as in the conventional electro-hydraulic servo system, the analysis to the output waveform becomes crucial to the design and control of the electro-hydraulic vibrator. The mathematical models of hydraulic actuation mechanism and the orifice area of the parallel valves connection are established first. And then the vibration process is divided into two sections in terms of the direction of the flow, the analytical expression of the excited waveform is solved. Based on relationships exist between working states and the control parameters the analytical results, the vibration boundary positions and the are derived. Finally an experimental system was built to validate the theoretical analysis. It is verified that this electro-hydraulic vibration system could achieve high working frequency, up to 2 000 hz. The excited waveform is similar to the sinnsoidal waveform. And the ascent and decent slopes of the waveforms are somewhat asymmetrical. This asymmetry is not only caused by the change of the direction of the elastic force but also dependent on the bias position of the vibration. Consequentky the distortion of effective working waveform is less tha~ 10%. This electro-hydraulic vibrator controlled by t

关键词： 2D valves hydraulic multiple-valve system electro-hydraulic vibrator excited waveform

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Inversion of Evaporation and Water Vapor Transport Using hY-2 Multi-Sensor Data

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Journal of Ocean University of China 2020年第1期19卷 13-22页

作者： LIU Dong’ang SUN jian GUAN Changlong Physical Oceanography Laboratory/CIMST Ocean University of China and Qingdao National Laboratory for Marine Science and Technology

hY-2 satellite is the first marine dynamic environment satellite of *** this study,global evaporation and water vapor transport of the global sea surface are calculated on the basis of hY-2 multi-sensor data from April 1 to 30,*** algorithm of evaporation and water vapor transport is discussed in detail,and results are compared with other reanalysis *** sea surface temperature of hY-2 is in good agreement with the ARGO buoy *** clusters are shown in the scatter plot of hY-2 and OAFlux evaporation due to the uneven global distribution of *** improve the calculation accuracy,we compared the different parameterization schemes and adopted the method of calibrating hY-2 precipitation data by SSM/I and Global Precipitation Climatology Project(GPCP)*** calculating the water vapor transport,the adjustment scheme is proposed to match the balance of the water cycle for data in the low latitudes.

关键词： hY-2 multi-sensor data inversion evaporation water vapor transport data calibration

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Effect of Meridional Characteristic angle on Aerodynamic Performance of Ram-Rotor

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Journal of Thermal Science 2020年第3期29卷 753-762页

作者： hAN Ji'ang GUAN jian ZhONG Jingjun ChEN Luting Naval Architecture and Ocean Engineering College Dalian Maritime UniversityDalian 116026China Merchant Marine College Shanghai Maritime UniversityShanghai 201306China

A kind of meridional concept which has a shape of contraction-expansion(Con-Exp)was applied to the ram-rotor in the paper,and detailed numerical simulation to understand the impact of meridional shape and geometric characteristic angle on the aerodynamic behavior of ram-rotors has been *** to baseline,there was a positive effect in intensifying shock train and suppressing low momentum fluid in Con-Exp scheme,and the pressure ratio and efficiency of Con-Exp scheme increased by 2.075%and 3.160%,*** the contracting angle was increasing,supersonic flow at and after throat region accelerated remarkably,and the static pressure rise was decreased *** terminating shock train was transformed to terminating shock,and the efficiency of ram-rotor was unfavorable to improve due to low throttle *** expanding angle rose,the terminating shock moved forward and turned to shock train *** pressure rise capacity and throttling ability of ram-rotor were *** low momentum fluid was accumulated near the middle and upper flow-path,yielding greater flow loss at large expanding angle.

关键词： ram-rotor meridional shape contracting angle expanding angle numerical simulation

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highly Efficient and Stable hydrogen Production in All ph Range by Two-Dimensional Structured Metal-Doped Tungsten Semicarbides

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Research 2019年第1期2019卷 991-1004页

作者： Edison h.ang Khang N.Dinh Xiaoli Sun Ying h.ang Jun Yang Zhili Dong Xiaochen Dong Wei h.ang Zhiguo Wang hua Zhang Qingyu Yan Energy Research Institute Interdisciplinary Graduate SchoolNanyang Technological University637553Singapore Centre for Programmable Materials School of Materials Science and EngineeringNanyang Technological University639798Singapore Institute of Advanced Materials Nanjing Tech UniversityNanjing 210000China School of Physical Electronics University of Electronic Science and Technology of ChinaChengdu 610054China Department of Chemistry City University of Hong KongKowloonHong Kong

Transition-metal-doped tungsten semicarbide nanosheets(M-doped W_(2)C NSs,M=Fe,Co,and Ni)have been synthesized through carburization of the mixture of tungsten trioxide,polyvinylpyrrolidone,and metal *** nanosheets grow directly on the W mesh and have the lateral dimension of several hundreds of nm to a few�m with a thickness of few tens *** is demonstrated that the M-doped W_(2)C NSs exhibit superior electrocatalytic activity for hydrogen evolution reaction(hER).Impressively,the Nidoped W_(2)C NSs(2 at%Ni)with the optimized hER activity show extremely low onset overpotentials of 4,9,and 19 mV and modest Tafel slopes of 39,51,and 87 mV dec−1 in acidic(ph=0),neutral(ph=7.2),and basic(ph=14)solutions,respectively,which is close to the commercial Pt/C *** functional theory(DFT)calculations also demonstrate that the Gibbs free energy for h adsorption of Ni-W_(2)C is much closer to the optimal valueG_(h∗)=-0.073 eV as compared to-0.16 eV of W_(2)***,nearly 100%Faradaic efciency and long-term stability are obtained in those *** realization of highly tolerant metal semicarbide catalyst performing on par with commercial Pt/C in all range of ph ofers a key step towards industrially electrochemical water splitting.

关键词： highly closer realization

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Effect of Vane Opening on Aerodynamic Performance of the Ram-rotor Test System

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Journal of Thermal Science 2016年第3期25卷 207-215页

作者： hAN Ji-ang GUAN jian ZhONG Jingjun YUAN Chenguang Marine Engineering College Dalian Maritime University

In order to research the influence of adjustable vane on the aerodynamic performance of the ram-rotor test system, FLUENT soft-ware has been adopted to simulate the flow passage of the ram-rotor test system numerically. The vane opening is controlled by changing the stagger angle of the vane blades. Results show that flow uniformity of vane outlet is influenced by the vane openings, which has an impact on the aerodynamic loss to some extent. Total pressure ratio, adiabatic efficiency and mass flow rate can be regulated by different openings of the vane. Compared with -8° vane opening, top efficiency of the ram-rotor increases by about 13.8% at ＋6° opening. And total pressure ratio drops by 5.87%. The rising opening increases the relative Mach number at inlet of the ram-rotor and weakens the intensity of the tip clearance leakage, which comes to a decreasing aerodynamic loss.

关键词： adjustable vane ram-rotor test system aerodynamic performance numerical simulation

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Breaking the structural symmetry of active sites in zeolite imidazolate framework for enhanced CO2 photoreduction

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Science China Chemistry 2025年

作者： Yupeng han Yayu Yan Qiaohong Li Xin Wu Fei Wang jian Zhang State Key Laboratory of Structural Chemistry Fujian Institute of Research on the Structure of Matter Chinese Academy of Sciences University of Chinese Academy of Sciences College of Chemistry Fuzhou University

Adjusting the structure and composition of active sites is a highly effective method for activating linear ***, precise control of interfacial chemistry within molecular-scale environments presents a significant challenge in heterogeneous catalysis. In our study, we present symmetry-broken Mo-O-Co triple-atom active sites within the hybrid zeolite imidazole framework hZIF-CoMo. These sites disrupt the electronic balance and create a weak built-in electric field, thus promoting photocatalytic CO2reduction. The CO yield over hZIF-CoMo is improved to 3.1 mmol g-1h-1, which is over four times higher than the parent cobalt-imidazole framework MAF-6-Co. Both experimental and theoretical studies indicate that electronic modulation through the symmetry-breaking Mo-O-Co moiety acts as an organizing knob to accelerate charge separation and result in more carriers participating in the catalytic reaction. This work provides important insights into optimizing site-related electronic structures for targeted photocatalytic reactions.

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Dual-ligand chiral MOFs exhibiting circularly polarized room temperature phosphorescence for anti-counterfeiting

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Science China Chemistry 2025年

作者： hongrui Zheng Qingqing Wang Xinchao Wang Fei Wang Shangda Li jian Zhang State Key Laboratory of Structural Chemistry Fujian Institute of Research on the Structure of Matter Chinese Academy of Sciences Fujian Key Laboratory of Polymer Materials College of Chemistry and Materials Science Fujian Normal University

Advanced chiral optical materials exhibiting circularly polarized room-temperature phosphorescence（CPRTP） possess significant research value. This study facilitates the synthesis of chiral metal-organic frameworks（CMOFs） with good CPRTP performance by implementing a dual-ligand strategy. By self-assembling the luminescent ligand h2BIIM with the chiral ligands L-or D-h2IDPA in the presence of Zn（II） ions, two robust three-dimensional（3D） CMOFs were successfully constructed. These complexes demonstrated intense fluorescence and exhibited prolonged yellow room-temperature phosphorescence（RTP） with a duration of up to 6 s. Notably, they exhibited both circularly polarized fluorescence(glum= ±7.57 × 10-3) and CPRTP(glum=±2.68 × 10-3). These unique properties were effectively utilized in the creation of multi-color anti-counterfeiting patterns,underscoring their promising potential for a wide range of applications.

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