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Multi-spherical interactions and mechanisms of hydrocarbon enrichment in the Southeast Asian archipelagic tectonic system

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Science china Earth Sciences 2024年第2期67卷 566-583页

作者： Rixiang zhu Hongjun WANG Huajian WANG Xiaomei WANG Bo WAN Wang ZHANG Houqin zhu Yuke LIU Junlai LIU Qingren MENG Fang HAO {2. jin state key {2. of Lithospheric Evolution Institute of Geology and GeophysicsChinese Academy of SciencesBeijing100029China state key {2. of Enhanced Oil and Gas Recovery PetroChina Research Institute of Petroleum Exploration and DevelopmentBeijing100083China School of Earth Sciences and resources China University of GeosciencesBeijing100083China state key {2. of Deep Oil and Gas China University of Petroleum(East China)Qingdao266580China Institute of Energy Peking UniversityBeijing100871China

Global cooling began since 50 Ma,but a warm climate was maintained in the archipelagic tectonic system in Southeast Asia where a wealth of Cenozoic oil and gas resources was formed and *** the perspective of Earth system,this study analyzes Cenozoic tectonic activities,climatic and environmental evolution,and petroleum enrichment in Southeast Asia,and provides the following insights:(1)Subduction of oceanic plates and the extension of overlying continental lithosphere resulted in widespread volcanic eruptions as well as the formation of rift basins and shallow marine shelves,leading to complex interactions between deep tectonic processes and Earth’s surface including mountains,basins,and seas.(2.Microcontinental accretion and prolonged stay in equatorial low-latitude regions have changed trade winds into monsoons,altered ocean current pathways and flow rates,and profoundly affected rainfall and climate.(3)The archipelagic tectonic system,coupled with a hot and rainy climate,fostered tropical rainforests,mangroves,and phytoplankton,providing abundant organic matter and promoting the development of petroleum resources.(4)Combinations of rift basin development and marine transgression and regression led to an effective superposition of source-reservoir-seal combinations from multiplepetroleum *** deep burial of organic matter and high geothermal gradients facilitated the generation and large-scale accumulation of oil and gas.(5)Multi-spherical(such as atmosphere,biosphere,hydrosphere and lithosphere)interactions on the Earth,which resulted from the convergence of multiple tectonic plates,are believed as the primary driver for exceptional enrichments of Cenozoic oil and gas resources in Southeast *** understandings are significant for developing theories of oil and gas enrichment under the guidance of Earth System *** order to continue making significant oil and gas exploration discoveries in the deep-layers,deep-waters,and unconventio

关键词： Southeast Asia Archipelagic tectonic system Interactions of Earth’s spheres Oil and gas resources Cenozoic

Clay mineral transformation in medium–high maturity shale oil reservoir: a case study of the Qingshankou Formation， Songliao Basin， Northeast china

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Journal of Earth Science 2024年

作者： Xinping Liang Xueyu Yao Rukai zhu Xiaojun Wang zhijun {2. Changrong Li Institute of Energy， Peking University state key {2. of Shale Oil and Gas Enrichment Mechanisms and Effective Development College of Geosciences/National key laboratory of {2. resources and Engineering， china University of {2. (beijing) Research Institute of petroleum exploration & Development Petrochina petroleum Exploration and Production Research Institute SINOPEC

Currently， significant hurdles lie ahead in china’s lacustrine shale oil exploration and exploitation， particularly due to the high clay mineral content， which severely impacts pore development in organic-rich shales. In this study， we take the medium- to high-maturity shale of the Qingshankou Formation (K2.n) in the Gulong Sag， Songliao Basin， china， as an example and analyze the dynamic evolution of the clay minerals and their effects on pore development by core observations， scanning electron microscopy， X-ray diffraction， physical property and nitrogen adsorptions to provide a valuable reference for the effective evaluation of lacustrine clay-rich shale oil reservoirs. Our findings reveal that the dynamic transformation of clay minerals in the Qingshankou Formation is classified into three stages based on diagenesis， thermal maturity， and mineral characteristics: the initial stage (vitrinite reflectivity (Ro) 1.3%). Clay minerals play crucial roles in controlling shale reservoirs during the rapid transformation process， which is evidenced by the formation of shrinkage fractures， enhanced pore connectivity， increased porosity， and expanded space for shale oil adsorption and storage. In addition， authigenic quartz can form during the transformation of clay minerals， contributing to increased reservoir brittleness and improving the potential for reservoir fracturing.

关键词：

Effects of abnormally high heat stress on petroleum in reservoir——An example from the Tazhong 18 Well in the Tarim Basin

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Science china Earth Sciences 2008年第4期51卷 515-527页

作者： zhu DongYa1, jin {2.1, HU WenXuan2.& ZHANG XueFeng3 1 petroleum Exploration and Production Institute, china petroleum & Chemical Corporation, beijing 100083, china 2.Department of Earth Sciences, Nanjing University, Nanjing 2.0093, china 3 School of resource and Information, china University of petroleum, beijing 102.4., china petroleum Exploration and Production Institute China Petroleum & Chemical Corporation Beijing China Department of Earth Sciences Nanjing University Nanjing China School of resource and Information China University of Petroleum Beijing China

An igneous intrusion of 94m thick was discovered intruding into the Silurian sandstone from Tazhong 18 Well. The petroleum previously preserved in the Silurian sandstone reservoir was altered into black carbonaceous bitumen by abnormally high heat stress induced by the igneous intrusion. The reflec-tance of the carbonaceous bitumen reaches as high as 3.54%, indicating that the bitumen had evolved into a high thermal evolution level. Similar to the Silurian samples from the neighboring Tazhong 11, Tazhong 12. Tazhong 45 and Tazhong 47 wells, the distribution of C2., C2. and C2. steranes of the car-bonaceous bitumen is still "V" -shaped and can still be employed as an efficient parameter in oil source correlation. The "V" -shaped distribution indicates that the hydrocarbons from the Tazhong 18 and the neighboring wells were all generated from the Middle-Upper Ordovician hydrocarbon source rocks. However, the oil source correlation parameters associated with and terpanes had been changed greatly by the high heat stress and can no longer be used in oil source correlation. The δ 13C values of the pe-troleum from the neighboring wells are between -32.53‰ and -33.37‰, coincident with those of the Paleozoic marine petroleum in the Tarim Basin. However, the δ 13C values of the carbonaceous bitumen from the Tazhong 18 Well are between -2..18‰ and -2..2.‰, isotopically much heavier than the pe-troleum from the neighboring wells. The content of light hydrocarbons (nC14-nC2.) of the saturated hydrocarbon fraction in the carbonaceous bitumen is extremely higher than the content of heavy hy-drocarbons. The light/heavy hydrocarbon ratios (ΣnC2.-/ΣnC2.+) are between 4.56 and 39.17. In the saturated fraction, the even numbered hydrocarbons are predominant to the odd numbered, and the OEP (Odd to Even Predominance) values are between 0.2. and 0.49. However, the content of light hy-drocarbons in the petroleum from the neighboring wells is relatively low and the content of the even numb

关键词： Tarim Basin igneous intrusive abnormally high heat stress bitumen carbon isotope PAH

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沉积盆地波动过程分析:研究现状与展望

地学前缘 2024年第1期31卷 284-296页

作者：金之钧陈书平张瑞北京大学能源研究院北京100871 北京大学地球与空间科学学院造山带和地壳演化教育部重点实验室北京100871 页岩油气富集机理与高效开发全国重点实验室北京102206 中国石油大学(北京)地球科学学院油气资源与探测国家重点实验室北京102249

沉积盆地的波状运动是板块内部地壳运动的主要表现形式,沉积盆地的形成演化是地球系统中各种波动过程相互叠加的结果。盆地波动过程分析从沉积速率时间序列中分解出有周期规律的波动曲线,获得盆地演化历史的新认识,主要包括控制盆地演... 详细信息

沉积盆地的波状运动是板块内部地壳运动的主要表现形式,沉积盆地的形成演化是地球系统中各种波动过程相互叠加的结果。盆地波动过程分析从沉积速率时间序列中分解出有周期规律的波动曲线,获得盆地演化历史的新认识,主要包括控制盆地演化的波动周期与成藏旋回、盆地地壳升降运动与油气生成及热演化的关系、不整合面的时空分布与剥蚀量恢复、多尺度波动叠加控制下的地层格架时空分布与生储盖层配置关系、隆拗变迁规律与油气藏保存的关系等。盆地波动过程分析技术将成盆、成烃和成藏的研究思路与地壳的波动过程有机融合,可以定量描述油气成藏动态演化过程,对油气勘探实践具有指导作用。沉积盆地波动过程研究未来应着重开展超长天文周期与地球深部动力学旋回驱动的盆地波动机制研究,加强地质证据与数值模拟技术融合,完善盆地波动过程分析方法,推进盆地波动理论成果转化以全面理解圈层相互作用与资源环境效应。充分发挥盆地波动分析技术对油气藏分布规律的预测功能,为油气资源远景评价与勘探提供科学依据。

关键词：圈层相互作用地壳波状运动地球动力学天文周期油气成藏烃源岩

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天然氢气:一种潜在的零碳能源

科学通报 2024年第17期69卷 2344-2350页

作者：刘全有吴小奇孟庆强朱地黄晓伟朱东亚李朋朋金之钧北京大学能源研究院北京100871 中国石油化工股份有限公司石油勘探开发研究院北京102260 页岩油气富集机理与高效开发全国重点实验室北京102260 齐鲁工业大学(山东省科学院)能源研究所济南250014

2.2.年2.17日,Hand[1]在Science上发表了“Hidden hydrogen:Does Earth hold vast stores of a renewable,carbonfree fuel?”一文,对地球上是否存在巨量的天然氢(H_(2.)进行了探讨,引发了全球能源界和科技界对这一可再生零碳能源的热议,“寻找天然氢源的热潮”也入选了Science“2.2.年度十大科学突破”.H2.烧产物只有水,不释放CO_(2.,因而被认为是最环保的绿色能源.天然H2.为能源转型背景下不可忽视的新能源之一[2.,除了在未来一次能源需求中扮演重要角色外,甚至还可能成为气候问题的“解药”[1],同时其在原始有机质分子[3]和地球早期生命形成[4,5]中可能扮演了重要角色,因而得到了国际社会越来越多的关注.

关键词：绿色能源燃烧产物零碳新能源科学突破

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富有机质泥页岩孔隙结构研究进展及展望

沉积与特提斯地质 2024年第2期44卷 231-252页

作者：曹琰金之钧朱如凯刘扣其梁新平北京大学能源研究院北京100871 北京大学地球与空间科学学院北京100871 页岩油气富集机理与有效开发国家重点实验室北京100083 中国石化石油勘探开发研究院北京100083 中国石油勘探开发研究院北京100083

探究富有机质泥页岩孔隙结构的划分方案、前沿表征方法、演化及发育影响因素,对页岩油储量评价及商业开发具有指导意义。通过调研富有机质泥页岩孔隙结构研究进展,归纳孔隙的划分方案,对比不同现代测试手段在泥页岩孔隙结构表征过程中... 详细信息

探究富有机质泥页岩孔隙结构的划分方案、前沿表征方法、演化及发育影响因素,对页岩油储量评价及商业开发具有指导意义。通过调研富有机质泥页岩孔隙结构研究进展,归纳孔隙的划分方案,对比不同现代测试手段在泥页岩孔隙结构表征过程中的优劣性,探讨海、陆相泥页岩孔隙结构的演化模式和有机、无机孔隙发育的主控因素,展望富有机质泥页岩孔隙研究未来的发展趋势。结果表明:(1)泥页岩储层表征的手段主要可以划分为成像法、流体侵入法、吸附法、散射法四类。(2.红外连用的原子力显微镜(AFM-IR)能够揭示泥页岩中显微组分的化学和岩石力学非均质性,小角中子散射(SANS)、核磁共振(NMR)和纳米CT技术是揭示孔隙连通性的重要途径。(3)沉积环境控制着泥页岩岩相和有机质母质来源,成岩和生烃作用及其相互间影响是泥页岩孔隙演化的主控因素,海、陆相泥页岩孔隙演化随时间和深度总体上均有“减孔→增孔→减孔→增孔→减孔”的规律,但陆相泥页岩在未熟-成熟阶段孔隙变化得更频繁。(4)Ⅰ型干酪根的有机质孔发育潜力远高于Ⅲ型干酪根,强生烃能力的腐泥组显微组分可发育丰富的有机孔隙,液态烃运移之后经二次裂解形成的焦沥青能提供更有效的连续性渗透路径。(5)成岩过程中无机矿物间的相互转化,长石、碳酸盐岩等矿物差异性溶蚀,压实、压溶和胶结作用等均会复杂化无机孔隙网络,有机-无机相互作用及矿物自身的岩石力学性质也是无机孔隙发育的重要影响因素。岩心在地表和地下所处环境差异巨大,未来的研究需要建立一个页岩孔隙在地面与地层条件下的反馈机制和矫正机制,进一步还原页岩油气在地下孔隙结构中真实的赋存状态。

关键词：富有机质泥页岩孔隙结构成熟度孔隙演化

Hydrothermal recrystallization of the Lower Ordovician dolomite and its significance to reservoir in northern Tarim Basin

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Science china Earth Sciences 2010年第3期53卷 368-381页

作者： zhu DongYa jin {2. HU WenXuan petroleum Production and Exploration Institute of china petroleum and Chemical Corporation Beijing 100083China Department of Earth Sciences Nanjing UniversityNanjing 210093China

Discovered in S15 and some other wells, the Lower Ordovician in the northern Tarim Basin consists mainly of brown gray-dark gray very fine-fine crystalline dolomite, with a minor portion of locally light gray-white medium-coarse crystalline dolomite. Silicification can be observed in the medium-coarse dolomite, and some euhedral drusy quartz can also be found in pores and fractures of the dolomite. The homogenization temperature of the fluid inclusions in the medium-coarse dolomite is between 110 and 2.0°C with maximum between 140 and 190°C, and the salinity is between 10.7 and 18.5 wt.% NaCl Eq. The homogenization temperature and salinity of the fluid inclusions in the medium-coarse dolomite are similar to those in the drusy quartz. Compared with the very fine-fine dolomite, the medium-coarse phase contains relatively high Fe and Mn. The average concentration of FeO and MnO in the medium-coarse dolomite is 1.917% and 0.32.%, respectively. The medium-coarse dolomite has a remarkable negative Eu anomaly, consistent with the REE pattern of the intermediate-felsic igneous rocks in the Tarim Basin. The oxygen isotopic composition of the medium-coarse dolomite is relatively lighter than that of the very fine-fine dolomite. The δ18OPDB values of the medium-coarse dolomite are between -10.35‰ and -7.31‰. The δ18OSMOW values of the fluid associated with the medium-coarse dolomite can be calculated according to homogenization temperature and oxygen isotope fractionation factor between dolomite and fluid, and the calculated values are between +4‰ and +10‰, consistent with those of the hydrothermal fluid. The medium-coarse dolomite has relatively high 87Sr/86Sr ratios as well, indi- cating an origin associated with intermediate-felsic igneous rock. The homogenization temperature, element composition, REE pattern, oxygen and strontium isotopes demonstrate that the medium-coarse dolomite is the result of recrystallization of very fine-fine dolomite under hydrothermal environment

关键词： Tarim hydrothermal dolomite recrystallization reservoir

Detection and significance of higher thiadiamondoids and diamondoidthiols in oil from the Zhongshen 1C well of the Tarim Basin, NW china

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Science china Earth Sciences 2018年第10期61卷 1440-1450页

作者： Anlai MA zhijun jin Cuishan {2. Yi GU Sinopec petroleum Exploration & Production Research Institute Beijing 100083 China state key {2. of Organic Geochemistry Guangzhou 510640 China College of resources and Environment Yangtze UniversityWuhan 430100 China

Oil and gas breakthroughs have been achieved in the Zhongshen 1(ZS1) and 1 C(ZS1 C) wells in Cambrian pre-salt from the Tarim Basin in northwest china. However, Middle and Lower Cambrian reservoirs reveal substantial differences in the geochemistry and secondary alteration characteristics between the oils collected from the two wells. High concentrations of thiadiamondoids and diamondoidthiols, including thiatetramantanes, tetramantanethiols, thiapentamantanes, and pentamantanethiols, are detected in the organic sulfur compound fraction of concentrated oil collected from the ZS1 C well, which samples the Lower Cambrian Xiaoerbulake Formation. Higher diamondoids, such as tetramantanes, pentamantanes, hexamantanes, and cyclohexamantane, also occur in the saturate fractions of the concentrated ZS1 C oil. The presence of these compounds is verified by mass spectra analysis and comparison with previous studies. During thermochemical sulfate reduction(TSR), the cage of higher diamondoids is interpreted to open because of sulfur radicals forming open-cage higher diamondoid-like thiols, followed by cyclization that leads to the formation of high thiadiamondoids. Using D_(16)-adamantane as an internal standard, the concentrations of lower diamondoids and thiadiamondoids of non-concentrated Cambrian oil from well ZS1 C are 83874 and8578 μg/g, respectively, which are far higher than Cambrian oil from well ZS1 and most Ordovician oils in the Tarim Basin. The high concentrations of lower thiadiamondoids and occurrence of higher thiadiamondoids and diamondoidthiols support that the oil from well ZS1 C is a product of severe TSR alteration.

关键词： Tarim Basin Cambrian Well Zhongshen 1C Higher thiadiamondoid Higher diamondoidthiol Higher diamondoid,Therrnochemical sulfate reduction (TSR)

Effects of Deep Fluids on Hydrocarbon Generation and Accumulation in Chinese Petroliferous Basins

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Acta Geologica Sinica(English Edition) 2017年第1期91卷 301-319页

作者： zhu Dongya LIU Quanyou jin {2. MENG Qingqiang HU Wenxuan state key {2. of Shale Oil and Gas Enrichment Mechanisms and Effective Development Beijing 100083 China petroleum Exploration and Production Research Institute of SINOPEC Beijing 100083 China Department of Earth Sciences Nanjing University Nanjing 210093 Jiangsu China

Deep fluids in a petroliferous basin generally come from the deep crust or mantle beneath the basin basement, and they transport deep substances（gases and aqueous solutions） as well as heat to sedimentary strata through deep faults. These deep fluids not only lead to large-scale accumulations of CO2. CH4, H2. He and other gases, but also significantly impact hydrocarbon generation and accumulation through organic-inorganic interactions. With the development of deep faults and magmatic-volcanic activities in different periods, most Chinese petroliferous basins have experienced strong impacts associated with deep fluid activity. In the Songliao, Bohai Bay, Northern Jiangsu, Sanshui, Yinggehai and Pearl Mouth Basins in china, a series of CO2.reservoirs have been discovered. The CO2.content is up to 99%, with δ-（13）C（CO2. values ranging from-4.1‰ to-0.37‰ and -3He/-4He ratios of up to 5.5 Ra. The abiogenic hydrocarbon gas reservoirs with commercial reserves, such as the Changde, Wanjinta, Zhaozhou, and Chaoyanggou reservoirs, are mainly distributed in the Xujiaweizi faulted depression of the Songliao Basin. The δ-（13）CCH4 values of the abiogenic alkane gases are generally -30‰ and exhibit an inverse carbon isotope sequence of δ-（13）C（CH4）δ-（13）C（C2.6）δ-（13）C（C3H8）δ-（13）C（C4H10）. According to {2. experiments, introducing external H2.can improve the rate of hydrocarbon generation by up to 147% through the kerogen hydrogenation process. During the migration from deep to shallow depth, CO2.can significantly alter reservoir rocks. In clastic reservoirs, feldspar is easily altered by CO2.rich fluids, leading to the formation of dawsonite, a typical mineral in high CO2.partial pressure environments, as well as the creation of secondary porosity. In carbonate reservoirs, CO2.rich fluids predominately cause dissolution or precipitation of carbonate minerals. The minerals, e.g., calcite and dolomite, show some typical features, such as higher homogenization temperatures th

关键词： petroliferous basin deep fluids organic-inorganic interaction hydrogenation reservoir rock alteration hydrocarbon migration