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Crystallization and Hardness of Melt Spun Fe_(73)Si_(13)B_9Nb_4Cu_1 Alloy

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journal of Materials Science & Technology 2009年第1期25卷 48-52页

作者： j.i. akhter M. iqbal M. Siddique M. Ahmad M.A. Haq M.A. Shaikh Z.Q. Hu Physics Division Pakistan Institute of Nuclear Science and Technology P. O. Nilore Islamabad Pakistan Shenyang National Laboratory for Materials Science Institute of Metal Research Chinese Academy of Sciences Shenyang 110016 China Department of Chemical and Materials Engineering Pakistan Institute of Engineering and Applied Sciences P.O. Nilore Islamabad Pakistan

An alloy having composition Fe73Si13B9Nb4Cu1 was synthesized by melt spinning to investigate the kinetics of crystallization. Techniques of differential scanning calorimetry （DSC）, X-ray diffraction （XRD） and Mossbauer spectroscopy were employed to characterize the phases produced due to annealing at various temperatures. High temperature DSC revealed two stage crystallization reactions. First stage, crystallization occurs at temperature around 514℃ with the production of α-Fe （bcc） and Fe3Si phases. in the second stage, Fe2B and α-Fe （Si,Nb） phases were produced. Mossbauer results revealed the formation of Fe3Si, Fe13Si3 and Fe7Si1 in the first stage and Fe3Si, Fe13Si3, Fe2B and α-Fe （Si,Nb） phases in the second stage of crystallization. An abrupt change in average internal magnetic field was observed at 500℃. The maximum hardness value was found for the sample heat-treated at 500℃.

关键词： Amorphous alloy Crystallization Mossbauer spectroscopy Hardness

Coupling metal-organic frameworks and wood-based carbon for water remediation

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Nano Research 2024年第6期17卷 5661-5669页

作者： akhter Zia Manish Neupane Aidan McGlone Rui He Ruikun Xin Yifeng Liu Qiangu Yan jinwu Wang Ling Li Zhiyong Cai Pei Dong Yingchao Yang Department of Mechanical Engineering University of MaineOronoME 04469USA Department of Mechanical and Aerospace Engineering University of MissouriColumbiaMO 65211USA Department of Mechanical Engineering George Mason UniversityFairfaxVA 22030USA Department of Civil and Environmental Engineering Rice UniversityHoustonTX 77005USA Department of Materials Science and NanoEngineering Rice UniversityHoustonTX 77005USA Forest Products Laboratory USDAMadisonWI 53726USA School of Forestry Resources University of MaineOronoME 04469USA

Fresh and clean water is highly demanded throughout the *** effectively address the need,nanomaterials enabled nanotechnology has been explored as a means of more efficient,reliable,and environmentally friendly approach towards water treatment *** concern in adopting nanomaterials is how to retrieve them from water body to avoid secondary *** this work,the earth abundant and sustainable wood,e.g.,basswood,was selected and carbonized into porous carbon as host skeleton,and metal-organic frameworks(MOFs),e.g.,MOF-199 with extremely high surface area,were grown throughout all channels in the porous basswood *** the traditional organic pollutant,methyl orange(MO),the combination of MOFs and basswood carbon(MOFs@carbon)demonstrates a remarkable adsorption capacity,which is 243%and 454%higher than basswood carbon and MOF-199,*** an outstanding adsorption performance originates from that the positively charged carbon pulls MO molecules close to carbon surface,leading to a high MO molecule concentration,and then the concentration gradient drives the MO molecules to be stored inside MOFs,functioning like *** findings highlight the potential application of coupled MOFs and biomass carbon in addressing water remediation.

关键词： metal-organic framework(MOF)-199 basswood carbon MOFs@carbon methyl orange

MXenes:A comprehensive review of synthesis,properties,and progress in supercapacitor applications

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journal of Materiomics 2023年第6期9卷 1196-1241页

作者： Raheela akhter Shrikant S.Maktedar Materials Chemistry&Engineering Research Laboratory Department of ChemistryNational Institute of TechnologySrinagar190006J&K(UT)India

MXenes,a class of two-dimensional materials,have garnered significant attention due to their unique properties and versatile applications in various *** review provides a comprehensive overview of MXene synthesis methods,highlighting their distinctive layered structure and tunable properties through surface *** focus then shifts to their remarkable role in supercapacitor *** exhibit high electrical conductivity,large surface areas,and tailored surface chemistry,making them promising candidates for energy storage in *** paper discusses the interplay of electric double-layer capacitance and pseudocapacitance mechanisms within MXenebased electrodes,detailing recent research efforts aimed at optimizing their energy storage *** a combination of theoretical insights and experimental findings,the potential of MXenes to revolutionize supercapacitor technology emerges,offering prospects for high-energy-density and long-lasting energy storage ***,this review highlights recent advances in MXenebased supercapacitors,including novel electrode designs,electrolyte engineering,and hybrid materials,showcasing the dynamic evolution of MXene-based supercapacitor *** comprehensive overview aims to provide a thorough understanding of MXenes'synthesis,properties,and their pivotal role in advancing supercapacitor technology,while also encompassing the latest breakthroughs in this rapidly evolving field.

关键词： MXenes Bimetallic MXenes Supercapacitor Charge storage mechanism Microsupercapacitor Prelithiation

Protein ubiquitination in plant peroxisomes

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journal of integrative Plant Biology 2023年第2期65卷 371-380页

作者： Delara akhter Yuchan Zhang jianping Hu Ronghui Pan State Key Laboratory of Rice Biology Zhejiang Provincial Key Laboratory of Crop Genetic ResourcesCollege of Agriculture and Biotechnology&ZJU-Hangzhou Global Scientific and Technological Innovation CenterZhejiang UniversityHangzhou 310058/311200China Zhejiang Laboratory Hangzhou 311121China Department of Genetics and Plant Breeding Sylhet Agricultural UniversitySylhet 3100Bangladesh Department of Energy Plant Research Laboratory and Plant Biology Department Michigan State UniversityEast LansingMichiganUSA Department of Plant Biology Michigan State UniversityEast LansingMichiganUSA

Protein ubiquitination regulates diverse cellular processes in eukaryotic organisms,from growth and development to stress *** subjected to ubiquitination can be found in virtually all subcellular locations and organelles,including peroxisomes,singlemembrane and highly dynamic organelles ubiquitous in *** contain metabolic functions essential to plants and animals such as lipid catabolism,detoxification of reactive oxygen species(ROS),biosynthesis of vital hormones and cofactors,and *** peroxisomes possess a complex proteome with functions varying among different tissue types and developmental stages,and during plant response to distinct environmental ***,how these diverse functions are regulated at the post-translational level is poorly understood,especially in *** this review,we summarized current knowledge of the involvement of protein ubiquitination in peroxisome protein import,remodeling,pexophagy,and metabolism,focusing on plants,and referencing discoveries from other eukaryotic systems when *** on previous ubiquitinomics studies,we compiled a list of 56 ubiquitinated Arabidopsis peroxisomal proteins whose functions are associated with all the major plant peroxisomal metabolic *** discovery suggests a broad impact of protein ubiquitination on plant peroxisome functions,therefore substantiating the need to investigate this significant regulatory mechanism in peroxisomes at more depths.

关键词： peroxins peroxisome peroxisome biogenesis peroxisome metabolism pexophagy ubiquitination

Crystallization Behaviour and Mechanical Properties of Zr65Cu18Ni9A18 Bulk Metallic Glass

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journal of Materials Science & Technology 2007年第5期23卷 693-696页

作者： M.iqbal j.i.akhter Haifeng ZHANG Zhuangqi HU Shenyang National Laboratory for Materials Science Institute of Metal Research Chinese Academy of Sciences 72 Wenhua Road Shenyang 110016 China Physics Division Pakistan Institute of Nuclear Science and Technology P.O. Nilore Islamabad Pakistan

Designing and synthesis of cost effective bulk metallic glasses （BMGs） has been of considerable interest during the last decade so that they can be made commercially viable. Among these, Zr-based BMGs have been reported extensively due to their attractive properties, An alloy having composition Zr65Cu18Ni9A18 was designed and synthesized using 2-3 N pure materials by Cu mould casting. The alloy was characterized by X- ray diffraction （XRD）, scanning electron microscopy （SEM）, energy dispersive X-ray spectroscopy （EDS） and high temperature differential scanning calorimetry （DSC）. Thermal parameters like supercooled liquid region △Tx, reduced glass transition temperature Trg, γ and δ parameters were evaluated. Mechanical properties like microhardness, nanohardness, elastic modulus and fracture strength were measured. The alloy showed wide supercooled liquid region of 129＋1 K with improved thermal stability. The alloy has considerable fracture strength along with fair amount of ductility.

关键词： Zr-based bulk amorphous alloys Mechanical properties Glass-forming ability Thermal parameters

Preparation and Characterization of Boron Thin Film on iron Substrate

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journal of Materials Science & Technology 2007年第4期23卷 481-486页

作者： ishrat REHANA D.Muhammad S.Ahmed j.i.akhter Central Analytical Facility Division Pakistan institute of Nuclear Science and Technology NiloreIslamabadPakistan Physics Radiation Division Pakistan institute of Nuclear Science and Technology NiloreIslamabadPakistan

The adherent thermal layering was undertaken by chemical vapor deposition （CVD） method using saturated solution of boric acid in ultra pure CH3OH. The influence of temperature was studied by varying temperature from 100 to 600℃ during the process of boron deposition. The most optimum temperature was found to be 200℃. The effect of time span was observed from 6 to 120 h. The generation of micro or nano-scale thickness could be achieved by reducing time span of the experiment. The behavior of CVD was characterized by using scanning electron microscope, absorbance spectrohotometer and atomic emission spectrograph.

关键词： Boron Chemical vapor deposition (CVD) Scanning electron microscopy (SEM) Atomic emission spectrograph (AES) Absorbance spectrophotometer Thin film

New Bi-metallic Single Source Precursors for the Deposition of Thin Films of Semiconductor Ceramics

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journal of Materials Science & Technology 2007年第2期23卷 196-200页

作者： U.Salma M.Mazhar j.i.akhter Z.Ali Department of Chemistry Quaid-i-Azam UniversityIslamabad 45320Pakistan Physics Division Pakistan Institute of Nuclear Science and TechnologyP.O.NiloreIslamabadPakistan

Stable binary single source precursors （SSP） for the deposition of thin films of ceramic semiconductors of composition SnO·GeO were synthesized by close circuit chemical vapour deposition （CCCVD） method. Elemental analysis and spectroscopic techniques were used to characterize the precursors. Scanning electron microscopy （SEM） and energy dispersive spectroscopy （EDS） were employed to characterize the thin films. Resistivity measurements were conducted to show that the films are of semiconducting nature.

关键词： Single source precursors CCCVD Organotin carboxylates

Antibacterial Characterization of Silver Nanoparticles against *** ATCC-15224

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journal of Materials Science & Technology 2008年第2期24卷 192-196页

作者： M.Raffi F.Hussain T.M.Bhatti j.i.akhter A.Hameed M.M.Hasan Department of Chemical and Materials Engineering Pakistan Institute of Engineering and Applied Sciences(PIEAS)Islamabad-45650Pakistan Department of Microbiology Faculty of Biological SciencesQuaid-i-Azam UniversityIslamabadPakistan Central Analytical Facility Division Pakistan Institute of Nuclear Science and Technology(PINSTECH)Islamabad-45650Pakistan Physics Division Pakistan Institute of Nuclear Science and Technology(PINSTECH)Islamabad-45650Pakistan

Silver nanoparticles of mean size 16 nm were synthesized by inert gas condensation （iGC） method. Crystalline structure, morphology and nanoparticles size estimation were conducted by X-ray diffraction （XRD） and transmission electron microscopy （TEM）. Antibacterial activity of these silver nanoparticles as a function of particles concentration against gram-negative bacterium Escherichia coli （E. coli） was carried out in liquid as well as solid growth media. Scanning electron microscopy （SEM） and TEM studies showed that silver nanoparticles after interaction with *** have adhered to and penetrated into the bacterial cells. Antibacterial properties of silver nanoparticles are attributed to their total surface area, as a larger surface to volume ratio of nanoparticles provides more efficient means for enhanced antibacterial activity.

关键词： Silver Nanoparticles Antibacterial Electron microscopy

The effect of tailing lipidation on the bioactivity of antimicrobial peptides and their aggregation tendency Special issue:Emerging investigators

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聚集体(英文)

聚集体(英文) 2023年第4期4卷 195-209页

作者： Bruce Lin Andrew Hung William Singleton Kevion K.Darmawan Rachael Moses Bicheng Yao Hongkang Wu Anders Barlow Marc-Antoine Sani Alastair j.Sloan Mohammed akhter Hossain john D.Wade Yuning Hong Neil M.O’Brien-Simpson Wenyi Li The Bio21 institute of Molecular Science and Biotechnology University of MelbourneMelbourneVictoriaAustralia ACTV Research group Melbourne Dental SchoolCentre for Oral Health ResearchUniversity of MelbourneMelbourneVictoriaAustralia School of Science RMIT UniversityMelbourneVictoriaAustralia Melbourne Dental School Division of Basic and Clinical Oral SciencesUniversity of MelbourneMelbourneVictoriaAustralia Department of Biochemistry and Chemistry La Trobe Institute for Molecular ScienceLa Trobe UniversityMelbourneVictoriaAustralia Florey institute of Neuroscience and Mental Health University of MelbourneMelbourneVictoriaAustralia School of Chemistry University of MelbourneMelbourneVictoriaAustralia Materials Characterisation and Fabrication Platform University of MelbourneMelbourneVictoriaAustralia

Antimicrobial peptides(AMPs)are potentially powerful alternatives to conven-tional antibiotics in combating multidrug resistance,given their broad spectrum of *** mainly interact with cell membranes through surface electrostatic potentials and the formation of secondary structures,resulting in permeability and destruction of target microorganism *** earlier work showed that two leading AMPs,MSi-78(4–20)and pardaxin(1–22),had potent antimicrobial activ-ity against a range of *** is known that the attachment of moderate-length lipid carbon chains to cationic peptides can further improve the functionality of these peptides through enhanced interactions with the membrane lipid bilayer,inducing membrane curvature,destabilization,and potential ***,in this work,we aimed to investigate the antimicrobial activity,oligomerization propensity,and lipid-membrane binding interactions of a range of N-terminal lipidated analogs of MSi-78(4–20)and pardaxin(1–22).Molecular modeling results suggest that aggregation of the N-lipidated AMPs may impart greater structural stability to the peptides in solu-tion and a greater depth of lipid bilayer insertion for the N-lipidated AMPs over the parental *** experimental and computationalfindings provide insights into how N-terminal lipidation of AMPs may alter their conformations,with subsequent effects on their functional properties in regard to their self-aggregation behavior,membrane interactions,and antimicrobial activity.

关键词： aggregation antimicrobial peptide lipidation membrane active peptide