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Towards the diffusion source cost reduction for NdFeB grain boundary diffusion process

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journal of Materials science & Technology 2020年第1期36卷 50-54页

作者： H.X.Zeng Z.W.Liu j.s.zhang X.F.Liao H.Y.Yu school of Materials science and Engineering South China University of TechnologyGuangzhou 510640China

Aiming at improving the performance/cost ratio in grain boundary diffusion process(GBDP),the critical RE containing Pr-Al-Cu alloy,less expensive RE containing La-Al-Cu alloy and non-RE Al-Cu alloy were employed as the diffusion *** preliminary results show that the coercivity was successfully enhanced from 1000 kA/m to 1695,1156 and 1125 kA/m by Pr70Al20Cu10,La70Al20Cu10 and Al75Cu25(at.%) alloys diffusion,respectively,due to the formation of(Nd,Pr)-Fe-B,La2 O3 and c-Nd2 O3 phases respectively,after *** is also found that the corrosion resistance can be improved by Al-Cu diffusion due to the positive effects of Al and Cu elements in grain *** present results demonstrated the various coercivity enhancement mechanisms for the GBDP based on different diffusion sources,and provided feasible solutions for cost reduction of GBDP and NdFeB production by saving RE resource.

关键词： Grain boundary diffusion Cost reduction Coercivity Microstructure Corrosion resistance

A novel Mg-Gd-Y-Zn-Cu-Ni alloy with excellent combination of strength and dissolution via peak-aging treatment

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journal of Magnesium and Alloys 2023年第2期11卷 720-734页

作者： Y.H.Liu Z.R.zhang j.Wang Y.Li H.X.Li L.Y.jia j.H.Wang j.s.zhang state Key Laboratory for Advanced Metals and Materials University of Science and Technology BeijingBeijing 100083China Dekai Intelligent Casting Co. Ltd.Hebei 072750China

Inferior absolute strength and dissolution properties are the main bottlenecks for the widespread application of dissolvable magnesium alloys in complex working environments for unconventional oil and gas ***,a novel functional peak-aged Mg-9.5Gd-2.7Y-0.9Zn-0.8Cu-0.4Ni(wt.%) alloy for fracturing tools is reported,and it possesses an ultimate tensile strength of 457.6 MPa,ultimate compressive strength of 620.7 MPa and dissolution rate of ~43.7 mg·cm^(-2)·h^(-1) in 3 wt.% KCl solutions at 93℃.The excellent strength of the agedalloy is primarily attributed to the combination of grain refinement,long-period stacking ordered(LPsO) strengthening,and precipitation strengthening induced by stacking fault and β’ phase,among which the precipitation strengthening is *** investigations confirm that the corrosion is triggered from the micro-galvanic coupling between the Mg matrix and the cathodic lamellar and block LPsO ***-shaped corrosion pits along with LPsO phases are subsequently formed,significantly accelerating *** β’ precipitates can effectively improve the strength without compromising the dissolution rate because of their nanoscale *** study provides an excellent material selection for dissolvable fracturing tools and presents a strategy by which a synergistic combination of strength and dissolution rate is achieved via peak-aging treatment.

关键词： Dissolvable magnesium alloy Peak-aging treatment Mechanical properties Micro-galvanic corrosion

Effect of trace Ni addition on microstructure,mechanical and corrosion properties of the extruded Mg-Gd-Y-Zr-Ni alloys for dissoluble fracturing tools

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journal of Magnesium and Alloys 2021年第5期9卷 1649-1660页

作者： j.Wang T.Li H.X.Li Y.Z.Ma K.N.Zhao C.L.Yang j.s.zhang state Key Laboratory for Advanced Metals and Materials University of Science and Technology BeijingBeijing 100083China Department of Petroleum Equipment of RIPED PetroChinaBeijing 100083China state Key Laboratory of solidification Processing Northwestern Polytechnical UniversityXi'an 710072China

Magnesium alloys,a novel functional material for the fabrication of fracturing tools,are being paid more and more attentions recently due to their relatively high mechanical properties and fast dissolubility ability after *** this study,the novel extruded Mg-10Gd-3Y-0.3Zr-xNi alloys will be reported and their microstructure,mechanical and corrosion behaviors will be also *** results show that Ni contents influence phase precipitation *** adding 0.2 wt%Ni,a large amount of Zr_(7)Ni_(10)phases will be precipitated insidesα-Mg matrix,directly leading to degradation of strength and large corrosion *** further increasing Ni contents,the precipitation phases can be changed from Mg_(5)RE to 18R-LPsO structure,resulting in higher mechanical properties and faster corrosion ***,adding Ni element also change the texture orientation by influencing the precipitation behavior of the *** alloys invented in this paper have attained the highest compressive and tensile properties among all the reported dissoluble magnesium *** work is beneficial in understanding the role of Ni in the magnesium alloys and provides more materials alternatives for the fabrication of dissoluble fracturing tools.

关键词： Dissoluble magnesium alloys Microstructure Mechanical properties Corrosion behaviors Fracturing tools

Double heterogeneous structures induced excellent strength-ductility synergy in Ni_(40)Co_(30)Cr_(20)Al_(5)Ti_(5)medium-entropy alloy

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journal of Materials science & Technology 2024年第14期181卷 176-188页

作者： A.X.Li X.s.Liu R.Li s.B.Yu M.H.jiang j.s.zhang C.N.Che D.Huang P.F.Yu G.Li state Key Laboratory of Metastable Materials science and Technology Yanshan UniversityQinhuangdao 066004China

The application of single-phase face-centered cubic(FCC)medium entropy alloys(MEAs)in the engi-neering industry is often hindered by the challenge of insufficient *** this study,a novel non-equiatomic ratio Ni_(40)Co_(30)Cr_(20)Al_(5)Ti_(5)MEA was successfully *** the well-designed mechan-ical heat treatment processing,we introduced a heterogeneous grain structure comprising 67.4%fine grain and 32.6%coarse ***,heterogeneous size L12 phases consisting of 18.7%submicron precip-itates and 11.7%nano-sized precipitates,were incorporated into the *** tests conducted at room temperature revealed that the double heterogeneous structure alloy demonstrated remarkable strength–ductility *** exhibited a yield strength of 1200 MPa,an ultimate tensile strength of 1560 MPa and a total elongation of 33.6%.The exceptional strength of the alloy can be primarily attributed to heteroge-neous deformation induced strengthening,grain boundary strengthening and precipitation *** excellent ductility is mainly attributed to the high-density stacking faults and Lomer–Cottrell *** study not only contributes to the clarification of the strengthening and deformation mechanism of double heterogeneous structure alloys but also provides an effective strategy for the development of high-performance alloys with high strength and ductility.

关键词： Medium entropy alloy Double heterogeneous structure HDI strengthening Remarkable tensile properties

Improving the hard magnetic properties by intragrain pinning for Ta doped nanocrystalline Ce-Fe-B alloys

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journal of Materials science & Technology 2019年第9期35卷 1877-1885页

作者： j.s.zhang W. Li X.F. Liao H.Y. Yu L.Z. Zhao H.X. Zeng D.R. Peng Z.W. Liu school of Materials science and Engineering South China University of TechnologyGuangzhou510640China Innovative Center for Advanced Materials (ICAM) Hangzhou Dianzi UniversityHangzhou310012China

To develop Ce based permanent magnets with high performance/cost ratio, Ta doping is was employed to enhance the magnetic performance of Ce-Fe-B alloys. For melt spun Cei7Fe78-xTaxB6 (x = 0-1) alloys, the coercivity Hc increases from 439 to 553 kA/m with increasing x value from 0 to 0.75. Microstructure characterizations indicate that Ta doping is helpful for grain refinement. A second phase of TaB2 is observed in Ce17Fe77.25Tao.75B6 alloy, which acts as the pinning center of the magnetic domains, resulting in the change of coercivity mechanism from nucleation type to nucleation +pinning type. The micromagnetic simulation confirms that non-magnetic particles within hard magnetic phase can increase the demagnetization field around them and it is crucial for preventing the further magnetization reverse by pinning effect. Take the advantage of Ta doping for enhancing the coercivity, Ce content of Ce-Fe-B alloy can be further cut down to increase the remanence jr due to the reduced volume fraction of CeFe2 phase and increased Fe/Ce ratio. As a result, a good combination of magnetic properties with Hc = 514 kA/m, jr = 0.49 T, and the maximum energy product (BH)max = 36 kj/m^3 have been obtained in Ce15Fe79.25Tao.75B6 alloy. It is expected that the present work can serve as a useful reference for designing new permanent magnetic materials with low-cost.

关键词： Melt-spinning Permanent magnets second phase Coercivity mechanism Thermal stability

Tailoring precipitation/properties and related mechanisms for a high-strength aluminum alloy plate via low-temperature retrogression and re-aging processes

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journal of Materials science & Technology 2022年第25期120卷 15-35页

作者： L.G.Hou H.Yu Y.W.Wang L.You Z.B.He C.M.Wu D.G.Eskin L.Katgerman L.Z.Zhuang j.s.zhang state Key Laboratory for Advanced Metals&Materials University of Science&Technology BeijingBeijing 100083China BCAsT Brunel University LondonKingston LaneUxbidge Middlesex UB83PHUnited Kingdom Institute of mineral resources Chinese Academy of Geological SciencesBeijing 100037China Nanjing Advanced Transportation Equipment New Technology Research Institute Nanjing 211800China Tomsk state University Tomsk634050Russian Federation Katgerman Aluminium Technology van Beuningenlaan 102334CC LeidenNetherlands Department of Materials science and Engineering Delft University of TechnologyMekelweg 22628CD Delftthe Netherlands

The retrogression and re-aging(RRA)processes,aimed mainly at tailoring intergranular precipitates,could significantly improve the corrosion resistance(i.e.,stress corrosion cracking resistance)without considerably decreasing the strength,which signifies that an efficient control of the size,distribution and evolution of intergranular and intragranular precipitates becomes critical for the integrated properties of the(mid-)thick high-strength Al alloy *** to RRA process with retrogression at200℃ (T77),this study investigated the impact of a modified RRA process(MT77)with lower retrogression temperatures(155-175℃ )and first-stage under-aging on the properties of a high-strength AA7050 Al alloy,in combination with detailed precipitate *** study showed that the strength/microhardness of the RRA-treated alloys decreased with raising retrogression temperature and/or prolonging retrogression time,along with the increased electrical *** rapid responsiveness of microstructure/property typical of retrogression at 200℃ was obviously postponed or decreased by using MT77 process with longer retrogression time that was more suitable for treating the(mid-)thick *** the other hand,higher retrogression temperature facilitated more intragranularηprecipitates,coarse intergranular precipitates and wide precipitate free zones,which prominently increased the electrical conductivity alongside a considerable strength loss as compared to the MT77-treated *** the preferred MT77 process,the high strength approaching T6 level as well as good corrosion resistance was ***,though a relatively homogeneous through-thickness strength was obtained,some small discrepancies of properties between the central and surface areas of an 86-mm thick 7050 Al alloy plate were observed,possibly related to the quenching *** precipitate evolution and mechanistic connection to the properties were discussed and reviewed for high-strengt

关键词： Aluminum alloy Heat treatment Precipitation strength Grain boundary

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急性脊髓创伤多次激发扩散加权MRI的特征

国际医学放射学杂志 2014年第3期 296-297页

作者： j.s.zhang Y.Huan 唐光健 Department of Radiology Xijing HospitalFourth Military Medical UniversityNo.127 Changle xiluXi’an 710032People’s Republic of China

摘要目的分析急性脊髓创伤的扩散MRI,评价其诊断价值。方法采用1.5 T MR设备,对20例急性脊髓创伤病人在创伤72 h内行常规MRI与多次激发导航校准DWI检查。

关键词： MRI 脊髓创伤高信号区

REsEARCH ON sURFACE CONTACT FATIGUE FAILURE OF HARDENED GEARs

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RESEARCH ON SURFACE CONTACT FATIGUE FAILURE OF HARDENED GEAR...

Determination of the number ofψ(3686)events taken at BEsⅢ

第三届摩擦疲劳学国际会议

作者： j.s.zhang X.L.WU W. Z. QI X.H. GU C.H.zhang Zhengzhou Research Institute of Mechanical Engineering 450052 Zhengzhou China jiaoZao AEs WanFANG Power Company Limited China

＜正＞In this paper, the fatigue test results of two different types of hardened gears were reported. The tests were carried out with two kinds of gear oils on the FZG gear test machine. The surface fatigue features and the anti-wear effect of oils were carefully studied by means of scanning electron microscope （sEM）, x-ray photoelectron spectroscopy （XPs）, auger electron spectroscopy （AEs） and scanning auger microprobe （sAM）.

关键词： Gear Fatigue test Pitting surface analysis

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Chinese Physics C 2024年第9期48卷 8-20页

作者： M.Ablikim M.N.Achasov P.Adlarson O.Afedulidis X.C.Ai R.Aliberti A.Amoroso Q.An Y.Bai O.Bakina I.Balossino Y.Ban H.-R.Bao V.Batozskaya K.Begzsuren N.Berger M.Berlowski M.Bertani D.Bettoni F.Bianchi E.Bianco A.Bortone I.Boyko R.A.Briere A.Brueggemann H.Cai X.Cai A.Calcaterra G.F.Cao N.Cao s.A.Cetin j.F.Chang G.R.Che G.Chelkov C.Chen C.H.Chen Chao Chen G.Chen H.s.Chen H.Y.Chen M.L.Chen s.j.Chen s.L.Chen s.M.Chen T.Chen X.R.Chen X.T.Chen Y.B.Chen Y.Q.Chen Z.j.Chen Z.Y.Chen s.K.Choi G.Cibinetto F.Cossio j.j.Cui H.L.Dai j.P.Dai A.Dbeyssi R.E.de Boer D.Dedovich C.Q.Deng Z.Y.Deng A.Denig I.Denysenko M.Destefanis F.De Mori B.Ding X.X.Ding Y.Ding Y.Ding j.Dong L.Y.Dong M.Y.Dong X.Dong M.C.Du s.X.Du Y.Y.Duan Z.H.Duan P.Egorov Y.H.Fan j.Fang j.Fang s.s.Fang W.X.Fang Y.Fang Y.Q.Fang R.Farinelli L.Fava F.Feldbauer G.Felici C.Q.Feng j.H.Feng Y.T.Feng M.Fritsch C.D.Fu j.L.Fu Y.W.Fu H.Gao X.B.Gao Y.N.Gao Yang Gao s.Garbolino I.Garzia L.Ge P.T.Ge Z.W.Ge C.Geng E.M.Gersabeck A.Gilman K.Goetzen L.Gong W.X.Gong W.Gradl s.Gramigna M.Greco M.H.Gu Y.T.Gu C.Y.Guan Z.L.Guan A.Q.Guo L.B.Guo M.j.Guo R.P.Guo Y.P.Guo A.Guskov j.Gutierrez K.L.Han T.T.Han F.Hanisch X.Q.Hao F.A.Harris K.K.He K.L.He F.H.Heinsius C.H.Heinz Y.K.Heng C.Herold T.Holtmann P.C.Hong G.Y.Hou X.T.Hou Y.R.Hou Z.L.Hou B.Y.Hu H.M.Hu j.F.Hu s.L.Hu T.Hu Y.Hu G.s.Huang K.X.Huang L.Q.Huang X.T.Huang Y.P.Huang T.Hussain F.Hölzken N.Hüsken N.in der Wiesche j.jackson s.janchiv j.H.jeong Q.ji Q.P.ji W.ji X.B.ji X.L.ji Y.Y.ji X.Q.jia Z.K.jia D.jiang H.B.jiang P.C.jiang s.s.jiang T.j.jiang X.s.jiang Y.jiang j.B.jiao j.K.jiao Z.jiao s.jin Y.jin M.Q.jing X.M.jing T.johansson s.Kabana N.Kalantar-Nayestanaki X.L.Kang X.s.Kang M.Kavatsyuk B.C.Ke V.Khachatryan A.Khoukaz R.Kiuchi O.B.Kolcu B.Kopf M.Kuessner X.Kui N.Kumar A.Kupsc W.Kühn j.j.Lane P.Larin L.Lavezzi T.T.Lei Z.H.Lei M.Lellmann T.Lenz C.Li C.Li C.H.Li Cheng Li D.M.Li F.Li G.Li H.B.Li H.j.Li H.N.Li Hui Li j.R.Li j.s.Li Ke Li L.j.Li L.K.Li Lei Li M.H.Li P.R.Li Q.M.Li Q.X.Li R.Li s.X.Li T.Li W.D.Li W.G.Li X.Li X.H.Li X.L.Li X.Z.Li Xi Institute of High Energy Physics Beijing 100049China Beihang University Beijing 100191China Bochum Ruhr-University D-44780BochumGermany Budker Institute of Nuclear Physics sB RAs(BINP) Novosibirsk 630090Russia Carnegie Mellon University PittsburghPennsylvania 15213USA Central China Normal University Wuhan 430079China Central south University Changsha 410083China China Center of Advanced science and Technology Beijing 100190China China University of Geosciences Wuhan 430074China Chung-Ang University Seoul06974Republic of Korea COMsATs University Islamabad Lahore CampusDefence RoadOff Raiwind Road54000LahorePakistan Fudan University Shanghai 200433China GsI Helmholtzcentre for Heavy Ion Research GmbH D-64291DarmstadtGermany Guangxi Normal University Guilin 541004China Guangxi University Nanning 530004China Hangzhou Normal University Hangzhou 310036China Hebei University Baoding 071002China Helmholtz Institute Mainz Staudinger Weg 18D-55099MainzGermany Henan Normal University Xinxiang 453007China Henan University Kaifeng 475004China Henan University of science and Technology Luoyang 471003China Henan University of Technology Zhengzhou 450001China Huangshan College Huangshan 245000China Hunan Normal University Changsha 410081China Hunan University Changsha 410082China Indian Institute of Technology Madras Chennai 600036India Indiana University BloomingtonIndiana 47405USA INFN Laboratori Nazionali di Frascati (A)INFN Laboratori Nazionali di FrascatiI-00044FrascatiItaly(B)INFN Sezione di PerugiaI-06100PerugiaItaly(C)University of PerugiaI-06100PerugiaItaly INFN sezione di Ferrara (A)INFN Sezione di FerraraI-44122FerraraItaly(B)University of FerraraI-44122FerraraItaly Inner Mongolia University Hohhot 010021China Institute of Modern Physics Lanzhou 730000China Institute of Physics and Technology Peace Avenue 54BUlaanbaatar 13330Mongolia Instituto de Alta Investigación Universidad de TarapacáCasilla 7DArica 1000000Chile jilin University Changchun 130012China joha

The number ofψ(3686)events collected by the BEsⅢdetector during the 2021 run period is determined to be(2259.3±11.1)×10~6 by counting inclusiveψ(3686)hadronic *** uncertainty is systematic and the statistical uncertainty is ***,the numbers ofψ(3686)events collected during the 2009 and 2012run periods are updated to be(107.7±0.6)×10~6 and(345.4±2.6)×10~6,*** numbers are consistent with the previous measurements within one standard *** total number ofψ(3686)events in the three data samples is(2712.4±14.3)×10~6.

关键词： ψ(3686) inclusive process Hadronic events BEsⅢdetector