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The effect of SiO2 nanoparticles derived from hydrothermal solutions on the performance of portland cement based materials

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Frontiers of Earth Science 2017年第4期11卷 436-445页

作者： ismaei flores-vivian Rani G.K PRADOTO Mohamadreza MOINI Marina KOZHUKHOVA Vadim POTAPOV Konstantin SOBOLEV Department of Civil Engineering and Mechanics Advanced and Nano Cement-Based Materials Laboratory University ofWisconsin-Milwaukee Milwaukee 53211 USA Universidad Aut6noma de Nuevo Le6n Av. Universidad s/n Cd. Universitaria San Nicoldts de los Garza 66455 Nuevo Le6nMExico The Belgorod State Technological University named after V.G. Shoukhov Belgorod Russia Geotechnological Research Center Far East Branch of Russian Academy of Science Petropavlovsk-Kamchatsky 683002 Russia

The nanoparticles of SiO2 were used in cement systems to modify the rheological behavior, to enhance the reactivity of supplementary cementitious materials, and also to improve the strength and durability. In this research, low-cost nano-SiO2 particles from natural hydrothermal solutions obtained by membrane ultrafiltration and, optionally, by cryochemical vacuum sublimation drying, were evaluated in portland cement based systems. The SiO2-rich solutions were obtained from the wells of Mutnovsky geothermal power station （Far East of Russia）. The constant nano-SiO2 dosage of 0.25% （as a solid material by weight of cementitious materials） was used to compare the cement systems with different nanoparticles against a reference mortar and a commercially available nano-SiO2. Nanoparticles were characterized by X-Ray Diffraction （XRD）, BET Surface Area, Scanning Electron Microscope （SEM） and Fourier Transform Infrared （FTIR） spectroscopy techniques. It was demonstrated that the addition of polycarboxylate ether superplasticizer and the dispersion treatment using an ultrasound processor can be used to facilitate the distribution ofnano-SiOz particles in the mixing water. The effect ofnano-SiO2 particles in portland cement mortars was investigated by evaluating the flow, heat of hydration and compressive strength development. It was demonstrated that the use ofnano- SiO2 particles can reduce the segregation and improve strength properties.

关键词： ultrafiltration cryochemical vacuum sublimation drying nanoparticles portland cement heat of hydration,surface area compressive slxength

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