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Production of high-purity Mg metal from dolomite through novel molten salt electrolysis and vacuum distillation

Journal of Magnesium and Alloys 2023年第4期11卷 1308-1320页

作者： hyeong-jun jeoung Tae-Hyuk Lee Jin-Young Lee Kyung-Woo Yi jungshin Kang Korea Institute of Geoscience and Mineral Resources 124 Gwahak-ro Yuseong-guDaejeon 34132Republic of Korea Department of Materials Science and Engineering Seoul National University1 Gwanak-roGwanak-guSeoul 08826Republic of Korea Department of Resources Engineering University of Science and Technology217 Gajeong-ro Yuseong-guDaejeon 34113Republic of Korea School of Materials Science and Engineering Pusan National University2 Busandaehak-roGeumjeong-guBusan 46241Republic of Korea

In this study,a novel Mg production process for producing high-purity Mg metal from dolomite was *** the electrolysis of calcined dolomite was conducted using Cu cathode and C anode in MgF_(2)–LiF molten salt at 1083–1173 K by applying an average current of 1.42–1.46 A for 9.50–21.0 h,the current efficiency of 66.4–88.6%was *** produced Mg alloys consisted of MgCu_(2)and Cu(Mg)or MgCu_(2)and CuMg_(2)phases,depending on the Mg concentration in the Mg *** the electrolysis of calcined dolomite was conducted in MgF_(2)–LiF–CaF_(2)molten salt at 1083 K,the current efficiency was 40.9–71.4%,owing to undesired reactions such as electroreduction of Ca^(2+)or/and CO_(3)^(2−)***,the current efficiency increased from 40.9%to 63.2%by utilizing a Pt anode,because the occurrence of CO_(3)^(2−)ions in the molten salt was *** vacuum distillation of the obtained Mg alloys at 1300 K for 10 h,Mg metal with a purity of 99.9996–99.9998%was ***,the feasibility of this novel process for the production of high-purity Mg metal from dolomite was demonstrated.

关键词： High-purity magnesium Dolomite Magnesium oxide Electrolytic process Copper metal cathode Vacuum distillation

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Use of various MgO resources for high-purity Mg metal production through molten salt electrolysis and vacuum distillation

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Journal of Magnesium and Alloys 2023年第2期11卷 562-579页

作者： hyeong-jun jeoung Tae-Hyuk Lee Youngjae Kim Jin-Young Lee Young Min Kim Toru HOkabe Kyung-Woo Yi jungshin Kang Korea Institute of Geoscience and Mineral Resources 124 Gwahak-ro Yuseong-guDaejeon 34132South Korea Department of Materials Science and Engineering Seoul National University1 Gwanak-roGwanak-guSeoul 08826South Korea Department of Resources Engineering University of Science and Technology217 Gajeong-ro Yuseong-guDaejeon 34113South Korea Korea Institute of Materials Science 797 Changwondae-roSeongsan-guChangwonGyeongnam 51508South Korea Institute of Industrial Science The University of Tokyo4-6-1 KomabaMeguro-kuTokyo 153-8505Japan School of Materials Science and Engineering Pusan National University2 Busandaehak-roGeumjeong-guBusan 44241South Korea

A green and effective electrolytic process was developed to produce high-purity Mg metal using primary and secondary resources containing Mg O as a feedstock. The electrolysis of various Mg O resources was conducted using a Cu cathode in MgF2– LiF – KCl molten salt at 1043 K by applying an average current of 1.44 A for 12.5 h. The electrolysis of calcined North Korean magnesite and seawater Mg O clinker yielded Mg alloys of MgCu2and(Cu) phases with current efficiencies of 89.6–92.4%. The electrolysis of oxidized Mg O-C refractory brick, aged ferronickel slag, and ferronickel slag yielded Mg alloys of MgCu2and(Cu) phases with current efficiencies of 59.3–92.3%. The vacuum distillation of Mg alloys obtained was conducted at 1300 K for 10 h to produce high-purity Mg metal. After vacuum distillation, Mg metal with a purity of above 99.994% was obtained. Therefore, this study demonstrates the feasibility of the production of high-purity Mg metal from various Mg O resources using a novel electrolytic process with a Cu cathode, followed by vacuum distillation.

关键词： High-purity magnesium Magnesium oxide resources Electrolytic process Metal cathode Vacuum distillation

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Analytic design of information granulation-based fuzzy radial basis function neural networks with the aid of multiobjective particle swarm optimization

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International Journal of Intelligent Computing and Cybernetics 2012年第1期5卷 4-35页

作者： Byoung-jun Park jeoung-Nae Choi Wook-Dong Kim Sung-Kwun Oh IT Convergence Technology Research Laboratory Electronics and Telecommunications Research Institute(ETRI)DaejeonSouth Korea Research Institute KDT Co.LtdBucheong-siSouth Korea Department of Electrical Engineering The University of SuwonHwaseong-siSouth Korea

Purpose–The purpose of this paper is to consider the concept of Fuzzy Radial Basis Function Neural Networks with Information Granulation(IG-FRBFNN)and their optimization realized by means of the Multiobjective Particle Swarm Optimization(MOPSO).Design/methodology/approach–In fuzzy modeling,complexity,interpretability(or simplicity)as well as accuracy of the obtained model are essential design *** the performance of the IG-RBFNN model is directly affected by some parameters,such as the fuzzification coefficient used in the FCM,the number of rules and the orders of the polynomials in the consequent parts of the rules,the authors carry out both structural as well as parametric optimization of the network.A multi-objective Particle Swarm Optimization using Crowding Distance(MOPSO-CD)as well as O/WLS learning-based optimization are exploited to carry out the structural and parametric optimization of the model,respectively,while the optimization is of multiobjective character as it is aimed at the simultaneous minimization of complexity and maximization of ***–The performance of the proposed model is illustrated with the aid of three *** proposed optimization method leads to an accurate and highly interpretable fuzzy ***/value–A MOPSO-CD as well as O/WLS learning-based optimization are exploited,respectively,to carry out the structural and parametric optimization of the *** a result,the proposed methodology is interesting for designing an accurate and highly interpretable fuzzy model.

关键词： Modelling Optimization techniques Neural nets Design calculations Fuzzy c-means clustering Multi-objective particle swarm optimization Information granulation-based fuzzy radial basis function neural network Ordinary least squaresmethod Weighted least square method

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Visceral hypersensitivity and altered colonic motility after subsidence of inflammation in a rat model of colitis

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World Journal of Gastroenterology 2003年第12期9卷 2791-2795页

作者： jun-Ho La Tae-Wan Kim Tae-Sik Sung jeoung-Woo Kang Hyun-Ju Kim ⅠI-Suk Yang Department of Physiology College of Veterinary MedicineSeoul National UniversitySeoulRepublic of Korea

AIM:Irritable bowel syndrome(IBS)is a functional bowel disorder characterized by visceral hypersensitivity and altered bowel *** is increasing evidence suggesting the role of inflammation in the pathogenesis of IBS,which addresses the possibility that formerly established rat model of colitis could be used as an IBS model after the inflammation subsided. METHODS:Colitis was induced by intracolonic instillation of 4% acetic acid in male Sprague-Dawley *** extent of inflammation was assessed by histological examination and myeloperoxidase(MPO)activity *** subsidence of colitis,the rats were subjected to rectal distension and restraint stress,then the abdominal withdrawal reflex and the number of stress-induced fecal output were measured, respectively. RESULTS:At 2 days post-induction of colitis,the colon showed characteristic inflammatory changes in histology and 8-fold increase in MPO *** 7 days post-induction of colitis,the histological features and MPO activity returned to *** rats at 7 days post-induction of colitis showed hypersensitive response to rectal distension without an accompaning change in rectal compliance,and defecated more stools than control animals when under ***: These results concur largely with the characteristic features of IBS, visceral hypersensitivity and altered defecation pattern in the absence of detectable disease, suggesting that this animal model is a methodologically convenient and useful model for studying a subset of IBS.

关键词： Acetic Acid Animals Biological Markers Colitis Disease Models, Animal Inflammation Irritable Bowel Syndrome Male Pain Peroxidase Rats Rats, Sprague-Dawley Research Support, Non-U.S. Gov't

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