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Unleashing the Power of Bio-based Thermotropic Liquid Crystal Modifiers:Toughening and Reinforcing Petroleum-based Epoxy Resin without Compromising Other Properties

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Chinese Journal of Polymer Science 2024年第8期42卷 1093-1102页

作者： Qing-Yun Lu hong-wei gu Jia-Hui Li Qian-Qian Fan Bei-Tao Liu Yan Kou Xi-Gao Jian Zhi-Huan Weng State Key Laboratory of Fine Chemicals Frontiers Science Center for Smart MaterialsLiaoning Technology Innovation Center of High Performance Resin MaterialsDepartment of Polymer Science&EngineeringDalian University of TechnologyDalian 116024China Thermochemistry Laboratory Liaoning Province Key Laboratory of Thermochemistry for Energy and MaterialsDalian National Laboratory for Clean EnergyDalian Institute of Chemical PhysicsChinese Academy of SciencesDalian 116023China

Toughening the petroleum-based epoxy resin blends with bio-based modifiers without compromising their modulus,mechanical strength,and other properties is still a big challenge in view of the *** this study,a bio-based liquid crystal epoxy resin(THMT-E P)with an s-triazine ring structure was utilized to modify a petroleum-based bisphenol A epoxy resin(E51)with 4,4'-diaminodiphenylsulfone(DDS)as a curing agent,and the blended systems were evaluated for their thermal stability,mechanical properties,and flame *** results showed that the impact strength of the blended system initially increased and then decreased with the increase in THMT-EP content,and it reached the a maximum value of 26.5 kJ/m^(2)when the THMT-EP content was 5%,which was 31.2%higher than that of E51/***,the flexural strength,modulus,and glass transition tem perature of the blended system were all simultaneously improved with the addition of *** the same time,the addition of THMT-EP enhanced the flame retardancy of the system by increasing the char yield at 700℃and decreasing the peak heat release rate and total heat release *** work paves the way for a more sustainable improvement in the comprehensive performance of epoxy resin.

关键词： Epoxy resin Toughening Bio-based Thermotropic liquid crystal

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Growth mechanism of CdS film prepared by chemical bath deposition

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Rare Metals 2014年第3期33卷 324-329页

作者： Xing-Yu Peng hong-wei gu Teng Zhang Fa-Zhu Ding Fei Qu hong-Yan Wang Key Laboratory of Applied Superconductivity Institute of Electrical Engineering Chinese Academy of Sciences University of Chinese Academy of Sciences

In this paper, sodium citrate was adopted as a complexing agent and ammonia merely served as pH adjustor to investigate the growth mechanism of CdS film The growth rate, structural properties, surface morphology microstructure, and optical properties of CdS films were studied by profilometer, X-ray diffractometer（XRD）scanning electron microscopy（SEM）, transmission elec tron microscopy（TEM）, and spectrophotometer, respec tively. The SEM images show that CdS films prepared with higher ammonia concentration have lower nucleation density on substrate. SEM and EDS results show that the formation of Cd（OH）2is not required in the growth of CdS film. As the ammonia concentration increases, the sites tha previously adsorbed S2-are taken by OH-which leads to lower S2-density on substrate. CdS film forms through direct reaction of Cd2？with the S2-which are adsorbed on the substrate. Lower S2-density on the substrate results in the decrease of particle density on the substrate. The as deposited CdS films have relatively high-average trans mittance（＊80 %） in the wavelength range from 500 to1,000 nm which makes them suitable to be used in sola cell.

关键词： CdS Chemical bath deposition Ammoniaconcentration Growth mechanism

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Morphological evolution of CdS films prepared by chemical bath deposition

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Rare Metals 2013年第4期32卷 380-389页

作者： Xing-Yu Peng hong-wei gu Teng Zhang Fei Qu Fa-Zhu Ding hong-Yan Wang Key Laboratory of Applied Superconductivity Institute of Electrical Engineering Chinese Academy of Sciences

In this article, the growth process of chemical bath deposited CdS films was systematically investigated. The structural, optical, and morphological properties were investigated by X-ray diffraction （XRD）, transmission electron microscope （TEM）, UV-Vis spectrophotometer, scanning electron microscope （SEM）, respectively. CdS nanocubes with size of less than 500 nm and nanocrystal-lites with diameter of less than 5 nm forming in reaction solution are observed. According to the TEM results and the SEM morphological evolution of CdS films, a crystal-lite-by-crystallite growth mechanism is proposed to eluci-date the growth process of chemical bath deposited CdS films based on the present growth mechanism.

关键词： CdS Chemical bath deposition Growthmechanism Crystallite-by-crystallite

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Microstructure and superconducting properties of (BaTiO3,Y2O3)-doped YBCO films under different firing temperatures

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Rare Metals 2017年第1期36卷 37-41页

作者： hong-Yan Wang Fa-Zhu Ding hong-wei gu Hui-Liang Zhang Ze-Bin Dong University of Chinese Academy of Sciences Beijing 100049China Key Laboratory of Applied Superconductivity Institute of Electrical Engineering Chinese Academy of SciencesBeijing 100190 China

YBaCuO(YBCO) films with co-doping of Ba Ti O(BTO) and YOnanostructures were successfully fabricated on La Al O(LAO) substrate by metal organic deposition using trifluoroacetates(TFA-MOD). The focus of this study was to optimize the process conditions during the firing heat treatment of high critical current density(J C)-co-doped YBCO films. The effect of the firing temperatures on both the surface morphology and the superconducting properties for the doped YBCO films was systematically studied. According to the X-ray diffraction(XRD) and scanning electron microscopy(SEM) results,the films prepared at 820 and 850 °C show poor electrical performance due to impurity phases and large pores. In contrast, the dense YBCO films prepared at 830 and840 °C with the critical current densities of 10 MA-cm(77 K, 0 T) are obtained.

关键词： YBa2Cu3O7-x BaTiO3 and Y2O3 nanostructures Firing temperature TFA-MOD

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Synthesis, characterization, and thermostability of bis(2,2,6,6-tetramethyl-3,5-heptanedionato)barium(Ⅱ)

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Rare Metals 2013年第1期32卷 67-74页

作者： Teng Zhang hong-wei gu Fa-Zhu Ding Fei Qu Shao-Tao Dai Key Laboratory of Applied Superconductivity Institute of Electrical Engineering Chinese Academy of Sciences

The metal-organic chemical vapor deposition （MOCVD） technique is a promising process for high-tem- perature superconductor YBa2Cu307_6（YBCO） preparation. In this technique, it is a challenge to obtain barium precursors with high volatility. In addition, the purity, evaporation characteristics, and thermostability of adopted precursors in whole process will decide the quality and reproducible results of YBCO film. In the present report, bis（2,2,6,6-tetramethyl- 3,5-heptanedionato）barium（II）（Ba（TMHD）2） was synthe- sized, and its structure was identified by PTIR, 1H NMR, 13C NMR, and ESI-MS spectroscopy. Subsequently, the thermal properties and the kinetics of decomposition were systemati- cally investigated by nonisothermal thermogravimetric anal- ysis methods. Based on the average apparent activation energy evaluated by the Ozawa, Kissinger, and Friedman methods, the volatilization process was discussed, and all results show that Ba（TMHD）2 is unstable and highly sensitive to the change of temperature during the whole evaporation process. There- fore, it is very important to choose suitable volatilization technology and conditions for avoiding Ba（TMHD）2 break- down （or thermal aging） during MOCVD process. Subse- quently, the possible conversion function is estimated through the Coats-Redfern method to characterize the evaporation patterns and follows a phase boundary reaction mechanism by the contracting surface equation with average activation energy of 118.7 ***1-1.

关键词： Ba(TMHD)2 Metal-organic chemical vapordeposition (MOCVD) Synthesis Thermostability

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Substrate angle-induced fully c-axis orientation of AlN films deposited by off-normal DC sputtering method

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Rare Metals 2021年第12期40卷 3668-3675页

作者： Bo-wei Xie Fa-Zhu Ding hong-Jing Shang Da-Xing Huang Tai-guang Li Qi Zou Ji-Liang Zhang hong-wei gu Key Laboratory of Applied Superconductivity Chinese Academy of SciencesBeijing 100190China Institute of Electrical Engineering Chinese Academy of SciencesBeijing 100190China University of Chinese Academy of Sciences Beijing 100049China Department of Materials Science and Engineering Korea UniversitySeoul 02841Republic of Korea

A highly c-axis-oriented aluminum nitride(Al N)thin film with smooth and crack-free surface was fabricated by an off-normal direct current(DC)sputtering method in a pure nitrogen atmosphere,in which the rotatable substrate holder positioned in the middle of four side targets was a key approach to guarantee the grain growth with no *** detailed effects of substrate angle on the c-axis orientation of Al N films were investigated by varying the substrate angle from 0°to 90°.Moreover,theoretical analysis and Monte Carlo(MC)simulation reveal that the oblique or even vertical angle could improve the lateral kinetic energy of sputtered atoms deposited on the growing film.A variety of examining techniques including X-ray diffraction(XRD),(002)peak rocking curve,scanning electron microscopy(SEM)were conducted to evaluate the angle dependence on the crystallographic *** test results indicate that larger substrate angle is beneficial to the(002)growth of Al N thin film,and a fully c-axis textured Al N thin film is obtained at 90°with small surface roughness(R_(a))of 3.32 nm.

关键词： AlN film c-axis orientation Off-normal DC sputtering Rotating substrate Side target

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Electrical and optical properties of ZnO:Al films with different hydrogen contents in sputtering gas

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Rare Metals 2015年第3期34卷 173-177页

作者： Fei Qu Teng Zhang hong-wei gu Qing-Quan Qiu Fa-Zhu Ding Xing-Yu Peng hong-Yan Wang Applied Superconductors Key Laboratory Institute of Electrical EngineeringChinese Academy Sciences

Aluminum-doped zinc oxide （ZnO：AI） films were deposited by direct current magnetron sputtering in incorporating hydrogen in sputtering gas at room temper- ature. The influences of hydrogen content in sputtering gas on the structural, optical, and electrical properties of ZnO：A1 films were systematically investigated. It is found that hydrogen incorporated into ZnO lattice forms shallow donors in ZnO：A1 films and plays an important role in the properties of ZnO：A1 films. The electrical conductivity and infrared （IR） reflectance are improved due to the increase of electron carrier concentration, and the average trans- mittance decreases, which is ascribed to the strong scat- tering from the hydrogen incorporated and oxygen vacancies in ZnO：A1 films. In this study, the resistivity of 5.5 × 10-4 Ω.cm is obtained, the average transmittance of the wavelength in the range of 400-900 nm is almost 86 %, and the IR reflectance reaches 75 % at 2,500 nm, which is higher than that of reported TCO films. The band gap determined by optical absorption is a result of com- petition between Burstein-Moss effect and many-body perturbation effect. However, the hydrogen content in sputtering gas is above 10 %, and the optical band gap shift is independent of hydrogen content in sputtering gas.

关键词： ZnO:A1 thin films Hydrogen Electricalresistivity Transmittance IR reflectance

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Effects of amniotic membrane transplantation on cytokines expression in chemically burned rat corneas

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International Journal of Ophthalmology(English edition) 2011年第1期4卷 33-36页

作者： hong-wei gu Dan-Mei Bian Nan Hu and Jun-Fang Zhang Department of Ophthalmology the Affiliated Hospital of Nantong University Nantong 226001 Jiangsu Province China

AIM: To investigate the effect of amniotic membrane transplantation (AMT) on the expressions of inflammatory-related, angiogenic-related and growth-related cytokines in rat corneas after chemical injury. METHODS: Alkali wounds were inflicted on the central corneas of rats by applying a round filter paper soaked in 1mol/L NaOH for 40 seconds. One week after alkali burn, 12 rats were randomly divided into 2 groups: the AMT group and the control group, and AMT was performed on the rats in the AMT group. Corneal opacity and neovascularization were observed by slit-lamp microscopy. The protein levels of interleukin (IL)-2, interferon (IFN)-gamma, IL-10 and transforming growth factor (TGF)-beta were determined by enzyme-linked immunosorbent assay 2 weeks after AMT. The mRNA levels of matrix metalloproteinase-2 (MMP-2), vascular endothelial growth factor (VEGF), epidermal growth factor (EGF) and basic fibroblast growth factor (bFGF) were evaluated by real-time quantitative PCR. RESULTS: In the AMT group, the corneal opacity was improved (P =0.011) and the area of corneal neovascularization was significantly decreased (P=0.005) compared with the control group. The amount of IL-2 and IFN-gamma secreted by Th1 cells were decreased after AMT, whereas the amount of IL-10 and TGF-beta secreted by Th2 cells were increased ( P gulated (P=0.013) at the nnRNA level in the AMT group, while the expression of EGF was significantly higher (P= 0.022) compared with the control. CONCLUSION: AMT may suppress corneal neovascularization after chemical injury by modulating the expressions of soluble factors.

关键词： amniotic membrane transplantation chemical injury cornea cytokine

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Effect of Nb on the dynamic recrystallization behavior of high-grade pipeline steels

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International Journal of Minerals,Metallurgy and Materials 2010年第6期17卷 742-747页

作者： Tao Niu Yong-lin Kang hong-wei gu Yu-qun Yin Ming-liang Qiao Jin-xing Jiang School of Materials Science and Engineering University of Science and Technology Beijing Beijing 100083 China State Key Laboratory for Advanced Metals and Materials University of Science and Technology Beijing Beijing 10083 China Nanjing Iron and Steel Co. Ltd. Nanjing 210035 China

The dynamic recrystallization （DRX） behavior of high-grade X80/X100 pipeline steels with different Nb contents was investi- gated through single pass compression experiment using a Gleeble 1500 thermomechanical simulator. By the regression of stress-sWain data obtained in the experiment, the deformation activation energy of DRX was identified, and the critical strain was calculated with the Po- liak-Jonas （P-J） method. Based on the analysis, the occurrence condition and kinetics of DRX were determined. The results show that as the Nb content increases from 0.08wt% to 0.095wt%, the activation energy of recrystallization raises from 365 to 395 kJ/mol. The critical swain of DRX can be determined more accurately by the P-J method, and the ratios of critical swain to peak sWain of XS0 and X100 pipeline steels are 0.51 and 0.49, respectively, which are similar to the results achieved by other researchers and calculated with empirical formulae.

关键词： pipeline steels niobium dynamic recrystallization activation energy retardation kinetics

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Myotonic Dystrophy Type 1 Associated with White Matter yperintense Lesions： Clinic, Imaging, and Genetic Analysis

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Chinese Medical Journal 2015年第10期128卷 1412-1414页

作者： Lei Liu Hui-Miao Liu Zun-Jing Liu Lin-wei Zhang wei-hong gu Ren-Bin Wang Department of Neurology China-Japan Friendship Hospital Beijing 100029 China Department of Neurology The First Hospital of Hebei Medical University Shijiazhuang Hebei 050031 China

Myotonic dystrophy （DM） is a chronic, slowly progressing, highly variable, inherited multisystemic disease, which includes two main types： DM type 1 （DM1） and DM type 2 （DM2）. Both DM 1 and DM2 are autosomal dominantly inherited disorder. DM1, also called Steinert disease, is characterized by myotonia, muscle weakness, muscular dystrophy, endocrinopathy, cataract, cardiac conduction defect, central nervous system （CNS） dysfunction, and so on.

关键词： Anterior Temporal White Matter Hyperintense Lesions Myotonic Dystrophy Type 1 White Matter Hyperintense Lesions

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